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Diels Alder Lab Results

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Diels Alder Lab Results
Peppermint:
Chemical Name
Caryophyllene
4H‐1,4‐Epoxy‐4a,7‐ methanonaphthalene, 1,5,6,7,8,8a‐hexahydro‐
, (1α,4α,4aα,7α,7aβ)‐

Cis‐Hydrindane
6‐Methyl‐
bicyclo[4.2.0]octa n‐7‐ol Acetic Acid,
Chloro‐, Decyl
Ester
3‐
Heptafluorobytyr
yloxy‐6‐
Ethyldecane

Cornmint:
Chemical Name
1,5‐Dimethyl‐1,5‐
cyclooctadiene D‐Limonene
3‐Heptene, 2‐
Methyl‐. (E)‐
3‐Heptene, 4‐
Methyl‐
Cycloheanol, 5‐
Methyl‐2‐(1‐
Methylethyl)‐
Cyclohexanol, 1‐ methyl‐4‐(1‐ methylethyl)‐
(1.alpha.,2.beta.,5.
alpha.)‐

Retention
Structural
Time
Formula
(Mins)
9.312
C15H24
9.312
C11H14O

CAS
Number

87‐44‐5
129‐130 N/A
32763‐64‐7 251.775 N/A

0.901
1.178

7.407
7.407

C9H16
C9H16O

4551‐51‐3 160.999 N/A
900193‐87‐ 209.252 N/A

0.883
1.041

5.666

C12H23O2Cl

6974‐05‐6

0.972

5.666

C16H25O2F7

900215‐97‐ 296.979 N/A

CAS
Number

Boiling
Point

Melting
Point

274.482 35‐36

Boiling
Point

Density
(g/mL)

1.141

Retention
Structural
Time
Formula
(mins)
3.870
C10H16

Melting Density
Point
(g/mL)

3760‐14‐3

74

N/A

0.867

3.870
5.506

C10H16
C8H16

3760‐14‐3
692‐96‐6

176‐177
115.241

‐75‐ ‐73
N/A

0.842
0.726

5.506

C8H16

4485‐16‐9

119.969

N/A

0.729

5.836

C10H20O

15356‐70‐4 103‐104

43‐44

0.890

5.836

C10H20O

21129‐27‐1 208.453

N/A

0.898

Fragmentation:
Peppermint:
Possible Fragments
Compound Caryophylle ne 4H‐1,4‐Epoxy‐
4a,7‐
methanonapht halene… Retention
Time

Possible
Fragment

Cis‐
6‐Methyl‐
Acetic Acid,
Hydrindane bicyclo[4.2.0 Chloro‐,
]octan‐7‐ol Decyl Ester

3‐
Heptafluorob
ytyryloxy‐6‐
Ethyldecane

9.312

9.312

7.407

7.407

5.666

5.666

Cornmint:

Possible Fragments
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