Preview

Synthesis of Strontium Hexaferrite

Powerful Essays
Open Document
Open Document
14109 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
Synthesis of Strontium Hexaferrite
SYNTHESIS OF STRONTIUM HEXAFERRITE SUBSTITUTED WITH TITANIUM AND ZINC NANOPARTICLES BY SOL-GEL METHOD AND ITS CHARACTERIZATION

BY PAVITRA THIRUCHELVAM

SCHOOL OF ARTS AND SCIENCE TUNKU ABDUL RAHMAN COLLEGE KUALA LUMPUR

2012/2013

SYNTHESIS OF STRONTIUM HEXAFERRITE SUBSTITUTED WITH TITANIUM AND ZINC NANOPARTICLES BY SOL-GEL METHOD AND ITS CHARACTERIZATION

BY PAVITRA THIRUCHELVAM

A project report submitted to the School of Arts and Science in partial fulfilment of the requirement for the Bachelor of Science, Campbell University, U.S.A. and Advanced Diploma in Science, Tunku Abdul Rahman College

2012/2013

i

DECLARATION ON PLAGIARISM

Name: …Pavitra Thiruchelvam……………. Student’s ID:…11WAB08632…………

Title of Thesis: Synthesis of Strontium Hexaferrite Substituted with Titanium and Zinc (SrZnxTixFe12-2x O19) nanoparticles by Sol-gel method and its characterization

Declaration

1. I confirm that I understand what plagiarism entails and am aware of the College’s policy in this regard. 2. I confirm that I have not committed plagiarism when completing the attached piece of work. 3. I did not make use of another student’s previous work and submitted it as my own. 4. I did not allow and will not allow anyone to copy my work with the intention of presenting it as his or her own work. 5. I declare that this thesis is my own, original work.

Signature: ……………………………………...

Date: …22.03.2013…………………………

ii

ACKNOWLEDGEMENT

Foremost, I would like to express my gratitude to my advisor, Dr. Teh Geok Bee for her guidance to complete my Degree study and research. Under her supervision, I have gained more knowledge especially on chemistry (material science). Besides that, she has also inspired me to think critical to solve the scientific problem faced during the research. Besides my advisor, I would like to thank the other lectures especially Ms. Chia and Dr. Banumathi at Tunku Abdul Rahman College for their motivation and guidance. I thank my thesis team mates, Chan Chun lam,



References: 56 Weissleder R, Elizondo G, Wittenburg J, Rabito CA, Bengele HH, Josephson L: Ultrasmall superparamagnetic iron oxide: characterization of a new class of contrast agents for MR imaging, (1990)

You May Also Find These Documents Helpful

  • Good Essays

    i. Place a few single small crystal of Fe(OH2)6(H4N)2(SO4)2 in a shallow watch glass. Cover the crystals with the unknown solution. Then immediately add excess drops of 18 M H2SO4 .…

    • 889 Words
    • 4 Pages
    Good Essays
  • Good Essays

    Syllabus AP chem

    • 2072 Words
    • 9 Pages

    SYLLABUS – ADVANCED PLACEMENT CHEMISTRY Required Texts 1. Chemistry: The Central Science by Brown, LeMay and Bursten, 10th ed., Pearson Education. Inc., Upper Saddle River, NJ, 2006, ISBN: 0­13­146489­2 Includes: Text book, Laboratory Manual, Student Study Guide, AP Test Prep Series, Solutions to Practice Problems 2. Barrons AP Chemistry, Jespersen, Neil D, 4th ed., Barron’s Educational Series, Inc, 250 Wireless Boulevard, Hauppauge, New York 11788, ISBN: 978­0­7641­9329­3 Topics and Concepts Covered Topics covered are suggested by the College Board.…

    • 2072 Words
    • 9 Pages
    Good Essays
  • Powerful Essays

    Tsuzuki, T. (2009). Commercial scale production of inorganic nanoparticles. International Journal of Nanotechnology, Volume 6(5), 567-578. Retrieved August 19, 2014, from http://inderscience.metapress.com/content/Y4R5747447762895…

    • 2034 Words
    • 7 Pages
    Powerful Essays
  • Good Essays

    An ionic Iron solution with a known concentration of 4.047x10-3 M was obtained. A 250-mL sample of a 10-fold dilution of this ionic iron solution and 5 drops of concentrated HNO3 was made. This solution served as the source of ionic Iron for the remainder of the lab and was labeled “stock ionic Iron solution.” Next, a 50-mL aqueous ionic Iron and FerroZine® complex solution was prepared by adding 5.00mL stock ionic Iron, 3-mL of acetic acid buffer, 2-mL of 5% hydroxylamine hydrochloride, allowing five minutes for hydroxylamine to reduce Fe3+ to Fe2+, adding 2.5-mL of 0.01 M FerroZine® solution, and mixing well. A single beam Agilent technologies CARY60-UV-Vis Spectrophotometer was then employed to determine the optimum wavelength in the visible spectrum of the ionic Iron and FerroZine® complex.…

    • 458 Words
    • 2 Pages
    Good Essays
  • Good Essays

    The electron transfer reaction between hexacyanoferrate (III) and sodium borohydride resulted in the formation of hexacyanoferrate (II) ion and dihydrogen borate ion which was strongly catalyzed by AuNPs. The redox reaction is described as BH4- + 8 [Fe (CN)6]3- + 3H2O 8 [Fe(CN)6]4- + H2 BO3- + 8H+ The advantage of hexacyanoferrate ion for this redox study is that both oxidation states of iron (+2 and +3) are quite stable with respect to dissociation and hydrolysis and possess the same chemical composition and geometry. The redox potential corresponding to the reaction being studied, Eo (Fe2+/Fe3+) is +0.44 V versus a normal hydrogen electrode (NHE).…

    • 523 Words
    • 3 Pages
    Good Essays
  • Better Essays

    • Types of Catalysts • Examples of Heterogeneous Catalysis  Nanocatalysis • Preparation • Size Effects • Shape Effect • Support Materials…

    • 2251 Words
    • 10 Pages
    Better Essays
  • Powerful Essays

    formal lab

    • 904 Words
    • 4 Pages

    Abstract: In this two-part lab, we will learn about coordination compounds and their uses with stoiciometry. We will also find out about how theoretical yield is calculated from a reaction we will create. We will also synthesize Potassium Ferric Oxalate Trihydrate (K_3 [〖Fe(C_2 O_4)〗_3]•3H_2 O) using a two step reaction. In the second part of this lab we will calculate how much Oxalate Ion is present in the K_3 [〖Fe(C_2 O_4)〗_3]•3H_2 O using tirtimetry. This process is called quantitative chemical analysis and will be very helpful.…

    • 904 Words
    • 4 Pages
    Powerful Essays
  • Good Essays

    In this lab, 0.010 M purple-colored potassium permanganate solution was standardized by redox titration with iron (II) ammonium sulfate hexahydrate (FAS). The average mass of the three flasks of FAS was 0.483 grams. Once the concentration of the standard solution of KMnO4 (aq) was determined, it was used to determine the concentration of Fe2+ in iron pills. On average, there was 0.01813 L of solution used. With this information and the balanced net-ionic equation 10Fe(NH4)2(SO4)2*6H2O+2KMnO4+H2SO4 --> 5Fe2(SO4)3+(NH4)2SO4+K2SO4+2MnSO4+H2O, the average percentage by mass composition of Fe2+ in iron pill samples was 16.99%. (103)…

    • 1687 Words
    • 7 Pages
    Good Essays
  • Good Essays

    The photocatalytic activity obtained indicates that the HCC-TiO2 activity is attributed to the increased phenol adsorption by hydrotalcite transferring it to the active photocatalytic phase of the impregnated TiO2 particle, while better results are obtained in HSC-TiO2 due to greater impregnation of the catalyst on the surface of the calcined hydrotalcite, reducing the screening phenomenon, achieving HSC-TiO2 degradation up to (21.0%) at 8 w. The reuse of both compounds indicated the synergy between HCC and HSC with TiO2, since in four successive separation cycles there was little reduction of activity associated primarily with the loss of material…

    • 1105 Words
    • 5 Pages
    Good Essays
  • Better Essays

    References: 1. G.R. Odette, G. E. L. (2001). "Embrittlement of Nuclear Reactor Pressure Vessels." JOM 53(7): 18-22. 2. Gulyaev A.P. “Physical Metallurgy” 3. Wikipedia (25 October 2011). "Control rod." from http://en.wikipedia.org/wiki/Control_rod 4. Francois Thévenot, Boron carbide—A comprehensive review, Journal of the European Ceramic Society, Volume 6, Issue 4, 1990, Pages 205-225, ISSN 0955-2219, 10.1016/0955-2219(90)90048-K. 5. Wikipedia (2 January 2012). "Hafnium." from http://en.wikipedia.org/wiki/Hafnium 6. Chen, L. Y., Y. L. Gu, et al. (2004). "Synthesis and oxidation of nanocrystalline HfB2." Journal of Alloys and Compounds 368(1-2): 353-356. 7. C.R.F. Azevedo, Selection of fuel cladding material for nuclear fission reactors, Engineering Failure Analysis, Volume 18, Issue 8, December 2011, Pages 1943-1962, ISSN 1350-6307, 10.1016/j.engfailanal.2011.06.010. 8. Wikipedia (23 October 2011). "Zirconium alloy." from http://en.wikipedia.org/wiki/Zircaloy 9. Archer, S. (2010). Metallurgy: austenite vs. ferrite. Nuclear Archer. 10. Takeji, K. (2006). Method for producing oxide dispersion strengthened ferritic steel tube. J. N. C. D. Institute. Japan. 11. Wikipedia (5 January 2012). "Uranium." from http://en.wikipedia.org/wiki/Uranium. 12. Wieland (2009). Nuclear fusion as alternative energy source: Wieland supplies high performance copper alloys for the ITER research reactor.…

    • 3080 Words
    • 13 Pages
    Better Essays
  • Powerful Essays

    Diels Alder Experiment

    • 1208 Words
    • 5 Pages

    3 Lide, David R. CRC handbook of chemistry and physics: a ready-reference book of chemical and physical data. 75th ed. (1994-95 ed. Boca Raton, FL: CRC Press, 1994. Print.…

    • 1208 Words
    • 5 Pages
    Powerful Essays
  • Better Essays

    The compound, tris(acetylacetonano)lron(lll) (Fe(acac)3), was synthesized by reacting hydrated ferric chloride + acetyl acetone in ethanol and sodium acetate in water. The formed crystals were then recrystallized by dissolving in ethanol and washing with water. This synthesized compound and hexacyanoferrate(lll) (K3[Fe(CN)6]), which was already synthesized, were individually taken to the Sherwood Magnetic Susceptibility Balance (M.S.B) for measurements of calculating their individual magnetic susceptibilities and hence the magnetic moments.…

    • 1310 Words
    • 6 Pages
    Better Essays
  • Powerful Essays

    Dead

    • 3573 Words
    • 15 Pages

    A crystalline solid: atomic resolution image of strontium titanate. Brighter atoms are Sr and darker ones are Ti.…

    • 3573 Words
    • 15 Pages
    Powerful Essays
  • Powerful Essays

    ZnS exists in two polymorphs, namely sphalerite and wurzite. Analysis of its symmetry and crystal structure using ATOMS will be used to deduce its possible polytypic stacking sequences as well as the orientation relationship between these two structures. Sphalerite is a face centered cubic structure with each sulphur bonded with four zinc atoms is observed. The four interior sulphur atoms are located at 0.25, 0.25, 0.25 away from the nearest unit cell corners. There are 4 formula units of ZnS per unit cell.…

    • 1286 Words
    • 4 Pages
    Powerful Essays
  • Good Essays

    The present study, considering Barium strontium titanate due to its important applications in the electronic device as the piezoelectric material due to excellent performance as sensing and actuation. Barium strontium titanate nanocrystalline ceramic have been synthesized from mechanical alloying of commercially available BaCO3, SrCO3 and TiO2 by high energy ball milling. This method has produced nano-sized particles as well as highly reactive surface, can cause structural relaxation of surface atom and produce inhomogeneous strain by producing defect in crystalline solids and that defect can influence powder properties. The milled powders are characterized at different stages of milling by XRD, particle size analyzer, FESEM…

    • 935 Words
    • 4 Pages
    Good Essays