Preview

Unknown Acid Titration

Good Essays
Open Document
Open Document
1249 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
Unknown Acid Titration
Titration Lab

A Titration is a process of the concentration of one solution being determined by its reaction with either a standard solution or a known quantity of solid dissolved in solution. It may also be used to calculate the molar mass of an unknown acid or base.
Purpose:
I. Prepare a standard solution of sodium hydroxide II. Standardize a sodium hydroxide solution by using potassium hydrogen phthalate (KHP) III. When given whether the acid is monoprotic, diprotic, or triprotic , determine the molar mass of the unknown organic acid. IV. Calculate the Molarity of the Soft drink.

Materials: * 50 mL Buret * Beaker * Erlenmeyer Flask * Sodium Hydroxide * Water * Balance * Unknown Acids
…show more content…
Repeat the same steps 1-4 from Section B to prepare for the titration of the unknown acid solution.
2. Repeat the same steps 5-7 substituting the unknown acid for KHP. The unknown acids are in labeled jars A, B, and C. It will be indicated whether the acids are monoprotic, diprotic, or triprotic. 10 titrations should be completed for each unknown acid.
3. From the equation on the first page, calculate the molar mass of the acid using your average molarity.
Find the molar mass based on the number of protons in each acid.
4. Accept the values that are within 1.0 of each other. Calculate the average of all the acceptable values and then repeat for the remaining acids.
5. When back in the classroom, you will receive the correct molar mass of the acids so you can calculate the percent error.

D- Calculation of Molarity of a soft drink solution
1. Repeat steps 1-4 from Section B to prepare for the titration of the soft drink solution.
2. Take the soft drink solution from a buret on the back lab table recording the initial and final volume from the soft drink buret. Add approximately 40 mL of the soft drink to your flask. Make sure you record the exact volume to the 100ths place. Do not add water to your
…show more content…
The concentration of one solution was determined by its reaction with a standard solution. The molar mass of unknown acids were also calculated. While learning to titrate, I learned several other skills in the process. I learned how to prepare a standard solution of sodium hydroxide, how to standardize a sodium hydroxide solution by using potassium hydrogen phthalate (KHP), how to find the molar masses of unknown organic acids when given whether the acid is monoprotic, diprotic, or triprotic, and how to calculate the molarity of a soft drink. At the same time, other skills were practiced. Skills such as calculating molarity, molar mass and percent error were exercised.
The molarity was calculated for part B, the standardization of sodium hydroxide. After all of the molarities were calculated, five of them were accepted and the average came out to be 0.0935, which was the number that would be used throughout the lab to help calculate the molar masses of the unknown acids and the molarity of a soft

You May Also Find These Documents Helpful

  • Powerful Essays

    Diprotic Acid Lab Report

    • 1283 Words
    • 6 Pages

    The mole ratio needed to be used to compare the food acid and sodium hydroxide. We worked out that there was a three to one ratio as shown above. Due to being a three to one ratio, this means that the unknown supplied food acid is critic acid as it is a triprotic…

    • 1283 Words
    • 6 Pages
    Powerful Essays
  • Satisfactory Essays

    6.03 Calorimetry Lab

    • 301 Words
    • 2 Pages

    Once divided by two, that value ended up being 6.815 milliliters of NaOH added at the ½ equivalence point pH. In order to estimate the pH at that volume of NaOH being added, two data points around the volume of 6.815 milliliters were…

    • 301 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    Devry week five chem Ilab

    • 496 Words
    • 2 Pages

    Step 5 repeat steps 1-4 using pH meter, add a pH meter to the acid solution. Record numerous points of pH and NaOH added (especially near equivalence point) to be used later to prepare a titration curve.…

    • 496 Words
    • 2 Pages
    Good Essays
  • Good Essays

    2. To titrate a hydrochloric acid solution of “known” concentration with standardized 0.5M sodium hydroxide.…

    • 1882 Words
    • 12 Pages
    Good Essays
  • Satisfactory Essays

    Lab 4 Weak Acid Unknown

    • 304 Words
    • 2 Pages

    When testing the acid, use only between 0.2 g and 0.3 g for each trial (get as precise a measurement as you can). The general procedure is to weigh out your acid, dissolve it in water, add a couple drops of the indicator (phenolphthalein), and then add the sodium hydroxide until you note a color change (from clear to pink). When the color change occurs, you have added enough base to completely react with the acid (the endpoint). You are allowed three trials, and will be graded on accuracy.…

    • 304 Words
    • 2 Pages
    Satisfactory Essays
  • Better Essays

    Titration is a method, which is meant to find the concentration of either an acid or a base by adding a measured amount of it to a known volume and concentration of an acid or base1. Titration starts with a beaker or Erlenmeyer flask containing a very precise volume of the known concentration solution and a small amount of indicator, which is put underneath a burette containing the solution with unknown concentration1. Small drops of the titrant are then added to the known solution and indicator until the indicator changes which means the endpoint has been reached. Single drops of the titrant can sometimes make a permanent or temporary change in the indicator2.…

    • 2337 Words
    • 10 Pages
    Better Essays
  • Satisfactory Essays

    CHEM120 W5 Lab Template 1

    • 414 Words
    • 3 Pages

    Step 5 repeat steps 1-4 using pH meter, add a pH meter to the acid solution. Record numerous points of pH and NaOH added (especially near equivalence point) to be used later to prepare a titration curve.…

    • 414 Words
    • 3 Pages
    Satisfactory Essays
  • Good Essays

    Chem Lab.

    • 520 Words
    • 3 Pages

    3. Determine the mass of the clean dry vial and record your mass to 2 decimal places on your lab sheet.…

    • 520 Words
    • 3 Pages
    Good Essays
  • Satisfactory Essays

    Titrations Lan

    • 413 Words
    • 2 Pages

    C. Calculate the mass of the acetic acid in grams using the previously given equation.…

    • 413 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    Labs

    • 3297 Words
    • 14 Pages

    The second part of the experiment is the reaction of acid/base through titration. The acid, KHP, was placed in one burette while 100 mL of base, stock solution of NaOH, was placed in another burette. 25 mL of KHP was placed into the Erlenmeyer flask, which was also recorded as the volume of acid in the flask. A total of 19 mL of base, NaOH, was required for the endpoint, which was indicated by a very pale pink color. To calculate the molarity of NaOH, the following equation was used MNaOH x VNaOH = MKHP x VKHP therefore the molarity was .125 M.…

    • 3297 Words
    • 14 Pages
    Good Essays
  • Satisfactory Essays

    2.) Make a mass determination for 10.00 mL of each known and unknown solution, using a balance and a graduated cylinder. Record.…

    • 463 Words
    • 4 Pages
    Satisfactory Essays
  • Good Essays

    Determination of Khp

    • 907 Words
    • 4 Pages

    Acid – base titration is typical method of determining unknown figures. Acid – base titration means that by using neutralization between acid and base. Abrupt changing of pH says whether procedure is done or not. pH indicators are tools for determining neutralization is reaching end point. When reaction reaches equivalent point, one of species, titrant or analyte is used up completely and there is no more neutralization. But By pH indicator, there is very few possibility to distinguish equivalent point. When, neutralization reaches at that point, changing pH is too sensitive to distinguish that. Blank titration is one of way to decrease interval between equivalent and end point. Blank titration is executed in solution with no analyte, it involves same volume of diluted water with final volume of mixture of actual titration, pH indicator and titrant. From this titrant, interval is obvious. Before doing titration, standardization of titrant is first step. If concentration of titrant is not exact, final result is not exact. And then, doing titration by standardized titrant is going to be second.…

    • 907 Words
    • 4 Pages
    Good Essays
  • Powerful Essays

    Acid-Base Lab

    • 1339 Words
    • 6 Pages

    II.Purpose: The purpose of this experiment is to standardize a sodium hydroxide solution and use the standard solution to titrate an unknown solid acid. The equivalent mass of the solid acid will be determined from the volume of sodium hydroxide added at the equivalence point. The equilibrium constant, Ks, of the solid acid will be calculated from the titration curve obtained by plotting the pH of the solution versus the volume of sodium hydroxide added.…

    • 1339 Words
    • 6 Pages
    Powerful Essays
  • Good Essays

    Titration can be traced to the origins of volumetric analysis, which began in the late eighteenth century. Study of analytical chemistry began in France and the first burette was made by Francois Antoine Henri Descroizilles. The field began to spread to neighboring countries and eventually to the whole world. Titration can be defined as the gradual addition of one solution to another until the chemical amount of one reactant being added matches stoichiometrically the amount of another reactant in the solution initially present. Learning the right technique of Titration is essential because of its wide applications in all areas of science, it is used in laboratory medicine to determine unknown concentrations of chemicals of interest in blood and urine. Pharmacists also use titration in the development of new pharmaceuticals. Titration may also be used to determine the amount of a certain chemical in food. Often, titration is used to determine fat content, water content, and concentrations of vitamins. It is also used to tell if cheeses and wines have aged enough for distribution to supermarkets and shops. Scientists of different disciplines use titrations for a variety of different reason. [1]…

    • 735 Words
    • 3 Pages
    Good Essays
  • Good Essays

    Ester Hydrolysis

    • 1098 Words
    • 5 Pages

    First begin by mixing up and standardizing a 500mL solution of NaOH to titrate. For each of the six bottles, measure the directed amounts of ester, water, alcohol, and HCl. The bottles of different solutions will be left to come to equilibrium for two weeks. Once the NaOH is standardized, the solutions in the bottles have come to equilibrium, and a molarity is calculated, use the molarity of NaOH to discover how many mols were used to neutralize the solutions in each bottle. Once all of the calculations are complete, use an ICE chart to discover the mols of ester, water, acid, and alcohol at equilibrium to then calculate the Kc for each bottle. After a Kc has been calculated for all bottles, the last step is to determine an average Kc for all of the solutions.…

    • 1098 Words
    • 5 Pages
    Good Essays