Name C.W. Lab Section 1 GTA N.C. Station 30 5. Acylation of Ferrocene Post-lab report Fill out the appropriate sections below. Show all work. Your calculated answers need to match the answers in the table and be consistent with significant figures. Results Amounts and units Initial weight of Ferrocene 0.225 g Moles of Ferrocene 1.21 * 10 ^ -3 mol Initial volume of acetic anhydride 1.00 mL Moles of acetic anhydride 0.0110
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Experiment 42: Ferrocene Preparation Introduction: The purpose of the lab is to prepare ferrocene from ferrous chloride and cyclopentadiene. Ferrocene‚ an organometallic‚ is a combination of two cyclopentadienide ions with a ferrous cation‚ such that the six pi electrons binds every carbon equally to the metal forming a sandwich type structure. Ferrocene has the properties of both an activated benzene (undergoes electrophilic substitution reactions) and a ferrous ion (oxidation reaction). Glyme
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Jessica Zebracki Organic Chem II Lab 2/15/15 Friedel-Crafts Acylation of Ferrocene and Column Chromatography Introduction: The intention of this lab is to analyze the formation of acetylferrocene using column chromatography. The Friedel-Crafts acylation reaction created acetylferrocene and diacetylferrocene‚ using phosphoric acid as a catalyst for the reaction between acetic anhydride and ferrocene (once applying heat). During column chromatography‚ a solution is passed through a filtration system
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Separating Ferrocene and Acetylferrocene by Adsorption Chromatography Separating Ferrocene and Acetylferrocene by Adsorption Chromatography Dry Pack Method Leah Monroe February 27‚ 2003 Organic Chemistry Lab II Experiment performed on February 18 and 20‚ 2003 Abstract: Adsorption column chromatography is one way to separate compounds out of a mixture. In this technique‚ a solid stationary phase called the adsorbent is packed in a glass column and an eluent‚ which is the mobile phase‚ moves
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BioLab3 Lab Report 5 Enzymes Student Name: Cooper Lyon I. Enzyme Structure and Function EXERCISE 1 – Preparation of an enzyme activity standard At five minute intervals over the next fifteen minute period‚ record the color intensity of the solution of each test tube. Time (min) Tube S1 Potato Extract + Catechol Tube S2 Potato Extract + Water Tube S3 Catechol + Water 0 Shade of Yellow Clear/Milky Clear/Milky 5 Shade of Yellow Clear/Milky Clear/Milky 10 Orange Clear/Milky Clear/Milky 15
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root tip of a plant spend a comparatively long time in the mitotic phase‚ whereas those cells comprising slow-growing tissues would spend most of their lives in interphase. Non-dividing cells remain in interphase and never enter the mitotic phase. (Lab Manual 64) Interphase is the synthesis of biological molecules including DNA and duplicated DNA with associated proteins. These comprise the chromatin that begin to condense toward the end of this phase‚ but are not yet visible. The nucleoplasm
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Acetylation of Ferrocene 17. October 1996 Experiment #7 Introduction In this lab we will be utilizing the Friedel Crafts process of acetylation of ferrocene. Ferrocene is an atom of iron bounded by two aromatic rings. We will use some reagents that will cause the ferrocene to add either one acetyl group to an aromatic ring or add two acetyl groups to each of the aromatic rings. In order to determine how well this process had worked we employed: IR spectra analysis‚ column chromatography‚
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Solubility‚ Crystallization and Melting Point Determination Post-Lab Discussion Guidelines: Part 2A and 2C: Draw tables (as in textbook) showing which combinations were soluble/miscible and which were insoluble/immiscible. Explain why this is so. Why are certain chemicals soluble/miscible when others are not? Part 3A: Calculate % recovery (this is not the same as % yield – see handout from the first day of lab if you’re confused)‚ and determine melting point of your product. Discuss % recovery
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Taki Simadiris p1 Brierly Post-lab a. If you did not wash all of the Calcium Carbonate out of the beaker and into the filter during step 5‚ would your percent yield be larger or smaller? If you do not wash all of the Calcium Carbonate out‚ then the percent yield would be smaller because there is enough calcium carbonate left in the beaker that would have attributed to the final yield. b. If you used tap water instead of DI water what do you think would happen? Why? If you used tap water‚ the coffee
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Biology 160 Lab Manual Tacoma Community College Last update 06/03/2013 This page left intentionally blank Table of Contents Table of Contents i Laboratory 1: Principles of the Scientific Method 4 In-Lab Report Sheet 12 This page has been left intentionally blank 27 Laboratory 2: Scientific Methodology & Enzyme Activity 28 In-Lab Report Sheet 28 Objectives 33 Introduction 33 Parts of the Swift M5 Microscope 33
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