supplemental material from Zubrick‚ The Organic Chem Lab Survival Manual. (2) Draw the structure of acetanilide and report relevant physical data. Be sure to cite the source of the data. You should be able to figure out what’s relevant by reading the procedure. (3) Find and report the boiling points of the solvents you will be using for this experiment. (4) Outline the steps in the recrystallization of acetanilide. Recrystallization involves dissolving a solid in a solvent and crystallizing it again‚ taking
Premium Chemistry Experiment Oxygen
to be present in your sample of Panacetin (aspirin‚ acetanilide‚ and starch)‚ only starch is insoluble in the organic solvent dichloromethane (or methylene chloride)‚ CH2 Cl2. If a sample of Panacetin is dissolved as completely as possible in dichloromethane‚ the insoluble starch can be filtered out‚ leaving acetanilide and aspirin in solution. The purpose of this experiment is to extract the components of Panacetin. Although the acetanilide and aspirin are both quite insoluble in water at room
Premium Hydrochloric acid Solvent Acid
last part of the experiment I observed the melting point of Unknown E. After finding the melting point of Unknown E‚ I used 2-Chloroacetemide with a known melting point between 116-118 degrees Celsius and mixed it with Unknown E. I also took Acetanilide with a known melting point of 114.4 degrees Celsius and mixed it with Unknown E. I then observed these melting points to try and determine the identity of Unknown E. Results: Our first known was 100 % Biphenyl. We did three trials. The following
Premium
Name: Bhumiben Shah Date: 31st Jan ‘13 EXPERIMENT # 2 RECRYSTALLIZATION; FILTRATION OBJECTIVES: 1. To perform recrystallization and filtration of given impure organic compound. 2. To purify impure acetanilide using reflux condenser apparatus and Hirsch funnel filtration. 3. To determine percentage recovery of pure material (which is)‚ purified by recrystallization and filtration. SAFETY PRECAUTIONS: 1. Operate the aspirator with the maximum water-flow using a stop cock to
Premium Distillation Filter paper Laboratory glassware
placed in its own capillary tube‚ and then a 3rd capillary tube contained a 50/50 mixture of both ingredients. The results of their melting points occurred as is what the table says below. Data of MP’s (Celsius) Table 1 Trial #1 Unknown *Acetanilide 50/50 mixtures Shininess Occurred 114 114 114 MP 115.5 115.5 115.5 Trial #2
Premium Solubility Chemistry Separation process
2):  During this experiment‚ we used recrystallization methods in order to help in the purification of the unknown solid‚ as well as drying and vacuum filtration. We then ground the unknown and combined it with different chemicals (such as acetanilide or phenacetin) and used the melting point ranges to determine the identity. We used the Mel-Temp method in order to measure the melting points. (It is important to remember that if a chemical is mixed with a differing chemical‚ the melting point
Premium Temperature Solid Water
Introduction:The purpose of this lab was to determine the activating effect of aniline‚ phenol‚ anisole and acetanilide after reacting with pyridinum tribromide in order to undergo electrophilic aromatic substitution. The melting point of the isolated products were measured against the standards in order to determine how strong of an ortho/para activator the compound was based on the product(s) and melting point obtained. Theory: Electrophilic aromatic substitution is an organic reaction that takes
Premium Chemistry Electrophilic aromatic substitution Benzene
Kate Kirby June 6‚ 2013 Title: Extraction of an Unknown Compound Purpose: The purpose of this experiment was to separate a mixture of two or more unknown compounds and identify them based on their melting point and reactivity with an acid or a base. Compound studied/Reactions: The organic solvent used in this experiment was methyl t-butyl ether (MTBE‚ 2-methoxy-2-methylpropane). The unknown that dissolved in the MTBE‚ but was insoluble in water. MBTE is very volatile and flammable. It was
Free Chemistry Solvent Laboratory glassware
13‚ 2015 Answers to Questions: 1.) Arrangement of Reactivity: (fastest to slowest) - Phenol‚ Nitrophenol‚ Acetanilide‚ Benzene‚ Chlorobenzene‚ Aniline - A reaction has occurred if there’s a change in color. The nature of the substituent‚ whether electron-donating to the ring or electron-withdrawing from the ring‚ was responsible for the reactivity of the benzene. Aniline and acetanilide contain amine groups‚ which are electron-donating. Chlorobenzene contains chlorine‚ which is electron-withdrawing
Premium Benzene Functional group
different substituted benzenes towards bromination will be determined‚ where bromine is dissolved in acetic acid. Materials and apparatus Test solutions: 0.2 M solutions in ethyl acetate: Benzene‚ chlorobenzene‚ phenol‚ nitrophenol‚ aniline and acetanilide. Measuring pipettes (5 mL) micro test tubes 0.05 M Br2 in 90% CH3COOH Pasteur pipettes 0.05 M Br2 in cyclohexane II. Schematic Diagram of the Procedure Relative Rates of Bromination Add 2 drops of 0
Premium Solvent Benzene Acetic acid