Introduction: This experiment focuses on carrying out a Perkin Reaction to synthesize (E) and (Z) isomers of α-phenylcinnamic acid. This was accomplished by refluxing benzaldehyde‚ phenylacetic acid‚ acetic anhydride and triethylamine as a base. The chemical equation of a Perkin Reaction can be seen below. The reaction mechanism for the synthesis of α-phenylcinnamic acid is shown below: Results: Theoretical Yield Therefore‚ phenylacetic acid is the limiting reagent. Table
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Preparation of 4-bromoaniline Introduction Aromatic compounds tend to undergo electrophilic aromatic substitutions rather than addition reactions. Substitution of a new group for a hydrogen atom takes place via a resonance-stabilized carbocation. As the benzene ring is quite electron-rich‚ it almost always behaves as a nucleophile in a reaction which means the substitution on benzene occurs by the addition of an electrophile. Substituted benzenes tend to react at predictable positions. Alkyl groups
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filter paper. This process can be slow to drain leave only the remaining insoluble impurities in the filter. Once the pure sample is collected the crystallization process begins. Sodium acetate buffer‚ to maintain a relatively constant pH and acetic anhydride is added to the solution of p-phenetidine in HCl. After mixing and boiling‚ the solution is placed on Ice where the Crystallization process begins. The crystals are collected in a vacuum filtration using a Buchner funnel. This is a faster
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For the first part of the experiment‚ it began by weighing 4.0ml of methyl salicylate into a flask—a stir bar was added. While stirring‚ 40ml of 6M sodium hydroxide was added and the solution was heated and boiled for about 15 minutes. After the 15 minutes‚ a bit of water was used to wash down the sides of the flask and the solution was cooled. It was boiled for another 15 minutes‚ after this the solution was cooled for 5 minutes in an ice water bath. While the flaks was in the ice bath‚ 50ml of
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Preliminary Test and Solubility Classification of Organic Compound Keene Louise Topacio‚ Christopher Jay Robidillo Abstract The experiment focuses on how to classify organic compounds by its functional groups. It is done by preliminary test and with the solubility test. Preliminary test used two known compounds also the unknowns. Physical state‚ color‚ odor‚ and ignition test were noted. The known compounds are inorganic and organic compounds. A comparison is made from the observation in the unknown
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EXPERIMENT NO. 6 LIPIDS I NUR 4 GROUP 9 POLICARPIO‚ JOHN PAUL (A & B) QUERUBIN‚ KIMBERLY (C & D) QUILALA‚ REGENE (E & F1) RAMOS‚ PRACCEDES (F2a & F2b) SABALDICCA‚ VENZ (F2c & F2d) INTRODUCTION Lipids are organic compounds found in living organisms that are insoluble or slightly soluble in water but soluble in non-polar organic solvents. Lipids can be classified into four groups which are -fats‚ oils‚ and waxes‚ -compound lipids‚ -steroids‚ and -derived lipids. Various
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EXPERIMENT NO. 5 LIPIDS Sheena Grace Abainza (12-8116) Agatha Abella (12-8046) Danielle Quigao (12-8051) Jessa Mae Ramos (12-8049) February 15‚ 2013 CHEM42 (Biochemistry) Laboratory ABSTRACT This experiment was performed to enlighten the researcher about the different properties and characteristics of lipids including its solubility and its complexity with regards to its components. The test for solubility tagged along the aphorism “like dissolves
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SYNTHESIS OF ESTERS USING GREEN AND NON-GREEN CHEMISTRY Abstract Esters are a class of organic compounds with the general formula RCOOR’. Ester also contributes the flavor and aromas in fruits and flowers. The esterification reactions will use in the procedure‚ which are the interaction of a carboxylic acid with an alcohol‚ aided by an inorganic acid catalyst (H2SO4). Moreover‚ the green method will not use any catalyst but using heating source instead (microwave). Based on the comparison of
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Experimental Procedure and Interpretation of Data Collection and Preparation of Materials The bark of Santol (Sandoricum koetjape (Burm.f.) merr.) were collected at the researchers backyard on Rosales‚ Province of Pangasinan. The collection was done in the month of August to September 1999. The bark was collected through the used of a knife. The bark were dried under the sun. And were placed into container and tightly closed ready for expression. Preliminary Test for the Determination of Plant
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