Journal of Pharmaceutical & Biomedical Analysis Vol. I 1‚ No. 3‚ pp. 191-196‚ 1993 Printed in Great Britain 0731-7085/93 $6.00 + 0.00 ~) 1993 Pergamon Press Ltd The study of the differential pulse voltammetric behaviour of ergot alkaloids and their determination by DC amperometric detection in a FIA system* JUDIT INCZEFFY‚t$ ZSUZSA BERTHA SOMODI‚$ ZSOFIA PAP-SZIKLAY$ and GYORGY FARSANG§ $ Chemical Works of Gedeon Richter Ltd‚ P.O.B. 27‚ H-1475 Budapest‚ Hungary § Institute of Inorganic and
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Topic 8a – Carbonyl compounds Revision Notes 1. Introduction • Aldehydes and ketones are carbonyl compounds • They contain the carbonyl group C=O • The functional group in aldehydes is –CHO on the end of a chain e.g. ethanal CH3CHO • The functional group in ketones is C=O not at the end of a chain e.g. propanone CH3COCH3 2. AS Recap • Primary alcohols are oxidised by acidified potassium dichromate. An aldehyde is produced first and this can be further oxidised
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Thornton James Keel 7/20/13 Title: Titration for Acetic Acid in Vinegar Purpose: The objectives in this lab were to develop familiarity with the concepts and techniques of titration and to determine the concentration of an acetic acid solution in vinegar. Procedure: Data Tables: Data Table 1: Quantity of NaOH needed to Neutralize 5 mL of Acetic Acid Brand of Vinegar Used: heinz Label Notes: none | | Initial NaOH reading(Interpolate to 0.1 mL) | Final NaOH reading(Interpolate
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of different concentration of acetic acid (a weak acid which partially dissociated in water) with a PH probe. After we got the PH‚ we could find out the concentration of H+ by applying the relationship pH = -log [H+]. Having the determined value of [H+] of a weak acid with a known molar concentration [HA]‚ The acid dissociation constant‚ Ka‚ can be determined according to Ka = [H+][A-] /[HA]. In “Part B” experiment‚ we use a strong acid (HCl) and a weak acid (acetic acid) titrates with a strong base
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amount concentration of acetic acid in a sample of vinegar is 0.83 mol/L. VCH3COOH (aq) = 10.00 mL VNaOH (aq) = ? CCH3COOH = 0.83 mol/L CNaOH (aq) = 0.145 mol/L Materials: Sodium hydroxide 100 mL Acetic acid 50 mL 250 mL beaker x 2 Distilled water x 1 bottle Erlenmeyer flask x 1 Burette x 1 Pipette x 1 Pipette bulb x 1 Volumetric pipette x 1 Phenolphalein Procedure: Step 1- Gather materials‚ put on eyeglasses and apron. Step 2- Pour 50 mL of acetic acid into one 250 beaker
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Experiment 1: "A cis to trans conversion" Saturday‚ June 25‚ 2005 4:19 PM Notes on Theory • Alkenes o They are hydrocarbons with a C=C double bond • Double bonds are stronger and more reactive than single bonds o Hydrocarbons with double bonds used to be known as "olefins"‚ because they had an oily appearance • "Oleum" means oil • "Ficare" means make • Isomers o Geometric isomers have the same molecular formula‚ but a different geometric arrangement • They also have different physical properties
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FOUNDATION IN SCIENCE INTRODUCTION TO PRACTICAL ORGANIC CHEMISTRY – MAKING AND PURIFYING ORGANIC COMPOUNDS Stage 1 – Deciding how much reagent to use Most organic reactions do not go to completion; most reach an equilibrium position with significant quantities of reactants still remaining. In addition‚ separating the desired product from the rest of the reaction mixture‚ and then purifying it‚ will result in the loss of more of the product. The amount of product obtained expressed as a percentage
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FDA Vinegar / Acetic Acid Analysis Objective- Determine the Acetic acid level contained within the vinegar sample Background- Per the FDA regulation which states that consumer vinegar may contain no less than four percent and no more than five percent Acetic Acid‚ we will determine the Acetic Acid content of a sample of the vinegar in question through titration. After standardization of our titrant‚ which in this case will be NaOH‚ we will use this along with the indicator Phenolphthalein
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hydrogen-bonding from other protic groups on citric acid. Citric acid has a sour taste. Ethanoic acid also known as acetic acid and also commonly known as vinegar: is an organic compound with the chemical formula CH3COOH. It is a colourless liquid that when undiluted is also called glacial acetic acid. Acetic acid is the main component of vinegar (apart from water; vinegar is roughly 8% acetic acid by volume)‚ and has a distinctive sour taste and pungent smell. Besides its production as household vinegar
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Experiment 4 SOLUTION STOICHIOMETRY ACID-BASE TITRATIONS Determination of the Percent Acetic Acid in Vinegar Objectives: (1) To introduce and use the concept of solution stoichiometry (2) To specifically use solution stoichiometry to determine the percent of acetic acid in vinegar. (3) To prepare a standard solution by the method of titration. Consider the following balanced chemical equations: (1) HCl + NaOH ------> NaCl + HOH (2) H2SO4
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