Experiment 2: Centrifugation Title Centrifugation of fresh milk and Acetic Acid Objective(s): 1. To separate coagulated milk from mixture of fresh milk and Acetic Acid by centrifugation 2. To determine the relationship of speed of centrifugation with the coagulation of milk which separate from mixture. 3. To study the process of centrifugation Introduction Centrifugation is a process which materials suspended in a liquid medium undergo separation or concentrate due to the effect of gravity
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Glacial acetic acid‚ Ethylic acid‚ Vinegar acid‚ Acetic acid‚ glacial‚ Methanecarboxylic acid‚ Acetasol‚ Essigsaeure Molecular Formula: C2H4O2 Molecular Weight: 60.05196 Acetic acid is a weak acid which is probably most famous for being the primary acid in vinegar. In fact‚ acetic acid has a wide range of uses beyond sprinkling on salads‚ and it is produced in large volumes all over the world. People have been working with this acid in a number of contexts for centuries‚ with acetic acid being
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Percent Acetic Acid in Vinegar Introduction: Acetic acid is reactive when combined with calcium carbonate. In this lab‚ we will use vinegar for its acetic acid and egg shells for their calcium carbonate. Marketable vinegar differs in its acetic acid concentration from 4-6%. Calcium carbonate reacts with the acetic acid in vinegar to produce carbon dioxide‚ water‚ and calcium acetate as represented by the equation: CaCO3 + 2HC2H3O2 CO2 + H2O + Ca(C2H3O2)2. The calcium carbonate reacts with
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Procedure 8 Results 10 Calculations 14 Discussion 20 Conclusion 21 Recommendations 21 References 22 Appendices 22 Abstract This experiment was performed in order to determine the molarity of a solution and the percent by mass of acetic acid‚ CH3COOH in vinegar. Acetic acid is monoprotic and belongs to the carboxyl family of organic compounds. The titration method is used to neutralize the acids by using the standardized sodium hydroxide solution. It reacts with bases which is sodium hydroxide‚ NaOH
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2013 VI. RESULTS AND DISCUSSION Aspirin is prepared by the esterification of salicylic acid with acetic anhydride under acidic conditions. The phenol group in salicylic acid is replaced by a carboxyl group through electrophilic substitution. The mechanism for the reaction can be summarized as follows: Figure 11.4. Mechanism for the reaction of salicylic acid and acetic anhydride to form acetylsalicylic acid (aspirin) In this experiment‚ 85% phosphoric acid (H3PO4)‚ a strong acid
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[1]‚ commonly known as aspirin‚ through the reaction of salicylic acid with acetic anhydride under acidic conditions provided by sulphuric acid. Once the reaction was completed the samples’ yield and melting point were determined for comparison to industrial perimeters. The equation below outlines the overall reaction between salicylic acid and acetic anhydride. Note that acetyl salicylate is a synonym of aspirin and acetic acid is a by-product. Aspirin is one of the safest pain relievers
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acid and acetic anhydride; in the presence of sulfuric acid. After fully dissolving the salicylic acid with acetic anhydride‚ the solution is cooled and cold water is then added. Once the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction: Purpose: The aim of this experiment is to synthesize the common pain killer aspirin through an esterification reaction between Salicylic Acid and Acetic Anhydride; using
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salicylic acid to acetic anhydride‚ the starting materials. Instead of using acetic acid‚ acetic anhydride was used as solvent since the anhydride reacting with water to form acetic acid tends to drive the reaction to the right. It results from the elimination of a molecule of water from two molecules of acetic acid (see Fig. 11.2). Figure 11.3 below shows the balanced chemical reaction of the synthesis of acetylsalicylic acid. Figure 11.2. Structure of Acetic Anhydride
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acid reacts with acetic anhydride to form an ester‚ and to make aspirin. Synthesis of Acetylsalicylic Acid occurs by protonation of carbonyl (C=O) group‚ and a nucleophilic attack of OH on the acetic anhydride. The ferric chloride test and melting point were used to test the purity of the results. A hypothesized recovery rater of above 50% was expected. salicylic acid acetic anhydride Acetylsalicylic acid Acetic acid Procedure
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of HCl via nucleophilic substitution. Cellulose triacetate was generated by mixing cotton balls and acetic anhydride with acidic condition under heating. Materials: Styrene‚ 1 M NaOH solution‚ CaCl2(s)‚ xylene‚ t-butyl peroxybenzoate‚ methanol‚ 5% aqueous solution of 1‚ 6-hexanediamine‚ NaOH(s)‚ 5% sebacoyl chloride in hexane‚ glacial acetic acid‚ concentrated H2SO4‚ cotton balls‚ acetic anhydride‚ CH2Cl2 Procedure: For the synthesis of polystyrene‚ 10 ml styrene and 20 ml of 1 M NaOH solution
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