Figure 2 Figure 3 Figure 1 show the crystallisation reaction when the saturated sodium chloride solution was added to the cool reaction mixture. The salt of p-Toluenesulphonic acid started forming. Figure 2 show the wet crystal after the precipitated salt was being filtered by suction. The wet crystal was light purple in colour. Figure 3 show the end product after drying the wet crystal at 105°C in the drying cabinet (oven)
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Abandoned Acid Mine Drainage at Shoup’s Run Introduction Acid mine drainage (AMD) is an industrial waste which is the result of the extraction process of the mineral coal from the ground. It causes widespread pollution in the streams above and below the coals fields. AMD is caused when water flows through sulfur-bearing materials forming acidic solutions. It is formed when pyrite (FeS2)‚ an iron sulfide‚ is exposed and then reacts with air (O2) and water (H2O) to form sulfuric acid. 2FeS2 (s)
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EXERCISE 11 Synthesis of Aspirin (Acetylsalicylic Acid from Salicylic Acid) RAQUID‚ Rency J Group 5 18L I. Introduction Due to the demand of certain reagents in the laboratory in order to perform and conduct further experiments or produce essential compounds‚ chemists continuously develop organic synthesis. This process aims to prepare and synthesize desired organic compounds from commercially or readily available ones by providing the simplest route in synthesizing the compound
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Conclusion: The purpose of this lab was to synthesize and purify aspirin. The theoretical yield was calculated to 3.766g. The actual yield of pure aspirin was 2.863g with a yield of 76%. The percent yield indicates that our synthesis was a success but the yield is low and indicates that some of the aspirin was lost during synthesis. Some reasons for loss can result from human error such as loosing product from sticking on the spatula and the Buchner funnel and several weighings. Also‚ when transferring
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LAB 6. ACIDS AND BASES: PH AND BUFFERS PURPOSE: To determine the pH of common acids and bases using a pH meter‚ pH paper‚ and red cabbage indicator. To test the effect of adding an acid or base to a buffer solution. SAFETY CONCERNS: Always wear safety goggles. Wash with soap and water if skin contacts acids or bases. ACIDS: An Acid is a substance that when dissolved in water will produce hydrogen ions‚ H+‚ in the solution. An acid that does not contain carbon is called an inorganic
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Thermochemistry (((CLASS INFORMATION)) INTRODUCTION Thermal chemistry was intended to display that chemical reaction and phase changes involve energy. The energy of heat was presented when a change in temperature difference was evaluated. Chemical reactions in a calorimeter were used to determine the amount of heat produced by a reaction. Reactions that absorb heat were noted as endothermic‚ and reactions that release heat were noted as exothermic
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Experiment # 3 Acetylsalicylic Acid Introduction: The purpose of this experiment is to create and isolate pure acetylsalicylic acid from the substances salicylic acid and acetic anhydride. Then one will find the melting point to determine purity. Procedure: Make a hot bath. Weigh some salicylic acid and place in conical vial. Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in
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Post Lab Report Experiment 3 - Chromatography – Analyzing Analgesics by TLC and Isolation of β–Carotene by Column Chromatography Chemicals 1. Acetaminophen (C8H9NO2) 2. Aspirin (C9H8O4) 3. Caffeine (C8H10N4O2) 4. Ibuprofen (C13hH18O2) Introduction In this experiment‚ several analgesics were analyzed by Thin Layer Chromatography (TLC) and the composition of an unknown tablet was identified. We define chromatography as the separation of two or more compounds or ions by
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Introduction: Acid rain has proven to be a big problem for Connecticut. It has had a great impact on builders‚ wildlife‚ and the water sources. Acid rain has many components in it such as pollutants from plants to sulfuric acid from burning coal. Problem: Which stone is the most resistant against acid rain? Hypothesis: If we test the different stones against acid rain then red sand stone would be the best because it is heavier and cannot be easily broken. Independent variable: Type of stones
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Experiment 4: ACIDS AND BASES: PH Measurements and Macroscale Titration CHM023L – A12 Group no. 6 Members: | Contributions: | | Conclusion | | Recommendation | | Tables and figures with analysis | | Principles‚ Equation | | Abstract‚ tables | Date Performed: February 28‚ 2012 - Tuesday Date Submitted: March 6‚ 2012 - Tuesday Submitted to: ------------------------------------------------- ABSTRACT: This experiment introduces us the pH measurement and application of macroscale titration
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