and fever. Aspirin were made using a combination of salicylic acid and acetic anhydride.The goal of this experiment was to determined the purity of aspirin using different methods. These methods included‚ reacting salicylic acid with FeCl3‚ finding its melting points‚ and by doing Thin-layer chromatography. When you reacted salicylic acid with FeCl3‚ changes in color will occur. Pure Aspirin has a melting point around 135°C and a pure salicylic acid has 158 °C. TLC is used to separate compounds based
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Standard Solution (Part A and B) ABSTRACT The purpose of this experiment is to prepare a standard solution of potassium hydrogen phthalate and use titration to perform an acid/base reaction between the potassium hydrogen phthalate and sodium hydroxide to standardize approximately 0.10 M sodium hydroxide solution. To prepare the Potassium Hydrogen phthalate‚ a 2.00 grams of KHP was measured to an accurate measurement of 1.980 grams. A total of 100 mL of water was mixed with the KHP solution
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Acid-Base Titration Pre-Lab Discussion In the chemistry laboratory‚ it is sometimes necessary to experimentally determine the concentration of an acid solution or a base solution. A procedure for making this kind of determination is called an acid-base titration. In this procedure‚ a solution of known concentration‚ called the standard solution‚ is used to neutralize a precisely measured volume of the solution of unknown concentration to which one or two drops of an appropriate acid-base
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Amino acid present in the lumen of the small intestine The goal is to cross through the epithelial cell membrane to enter into the epithelial cell’s cytoplasm – its charged cuz of side chains To get through the membrane the amino acid must cross the Simple columnar epithelial cells lining the apical surface of the small intestinal tract. These cells are impermeable to any harmful bacteria that may be ingested by the body‚ but permeable to necessary ions. Absorption of amino acids occurs through
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Lysergic Acid Diethylamide (LSD) was created by chemist Albert Hofmann in Switzerland while attempting to create a blood stimulant. The drug was utilized for psychological experiments for many years and this even led to the military experimenting with it as a biological weapon in the 1960’s. During the 1960’s‚ as a result to the wide dispensing of the drug for experimental purposes‚ it wound up being the “…counterculture used the drug to escape the problems of society…” (LSD: A Short History). Due
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| Alex University Faculty of Commerce English EMBA Program Cohort 5 | | Case Analysis: Kim Park (B): Liabilities By: Khaled M. Motawie Introduction As part of her plan to explore interesting accounting questions with her study group‚ Kim Park prepared a set of short case studies dealing with the recognition and measurement of liabilities. Kim knew from her earlier study group discussions that
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High Performance Liquid Chromatography Analysis of Aspirin Problem: Was aspirin (acetylsalicylic acid) successfully synthesized? Are there impurities or by-products present in the synthesized aspirin? How pure is the synthesized aspirin? Introduction: In the last experiment‚ aspirin was synthesized followed by characterization of the product using several different techniques. Melting point was a test that provided information about the identity and purity of the aspirin product. The iron(III)chloride
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Abstract The bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure and its mechanism. After the addition of bromine to trans-cinnamic acid‚ the product was identified by its melting point and infrared spectrum resulting in erythro-2‚3-Dibromo-3-phenylpropanoic acid after comparing similar properties. Introduction In this lab‚ the bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure‚ and from there determine
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butanols with hydrobromic acid. Before the lab began we discussed and proposed mechanisms. (see “Mechanisms”) To begin this experiment we calculated how much of each material we were going to be using‚ and the numbers we chose to use differed from our reference text slightly. We used 6.5 mL of our assigned butanol and only 4 mL of sulfuric acid. Going back to our reaction mechanisms‚ we were looking at SN1 and SN2 reactions‚ so we of course used the hydrobromic acid as our acid catalyst which would be
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Sulfuric Acid is one of the the important chemical compounds. A Great amount of sulfur is mined all around the world and is used to produce sulfuric acid. Sulfuric acids being produced Sulfuric acid may seem like something to find in a lab‚ perhaps under the label “corrosive‚” and in some kind of tube that isn’t affected by it. But‚ in reality‚ it’s quite common‚ and is used often in the industrial business‚ for many different objects. Because of this‚ many places can often be judged upon their
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