Introduction: The theory behind the extraction of a solution containing benzoic acid‚ cellulose‚ and methyl orange involves many components pertaining to the fundamental ideas of solubility and polarity. Using the concepts of like dissolving like and acid base reactions‚ a solution of organic acid (benzoic acid)‚ a water soluble compound cellulose‚ and an organic soluble compound methyl orange‚ can be separated and benzoic acid can be isolated by a method of extraction. At the fundamental level‚
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The purpose of this experiment is to separate a solution of an acidic and organic compound and purify its respective acidic product through the techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through
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Conclusion Guidelines A good conclusion should contain all of the following parts a) You should state what experiment was performed‚ and show any necessary reaction schemes. The reaction schemes should include molecular weights and any other important physical data for the reagents and products. Ex. Cyclohexanol was oxidized to cyclohexanone using sodium dichromate in the presence of sulfuric acid. * Note: you can download a free version of a structure editor from ACD labs‚ the PC version is called
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Mabel M. Kimble September 21‚ 2014 Chemistry 234 Recrystallization of Benzoic Acid ABSTRACT The recrystallization of Benzoic Acid was performed to fully master the ability to purify a solid compound. This form of purification technique is especially important in chemical identification‚ where the melting point of the compound is taken to confirm its purity. In order to perform recrystallization a solubility test much be completed. Four solvents (95% Ethanol‚ Petroleum Ether‚ Acetone and distilled
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Abstract In this experiment paper chromatography was used in order to identify two unknown amino acids using eight known amino ones. The two unknown ones were identified by comparing the distance they travelled up the chromatography paper and their Rf values to the corresponding values of the other eight known amino acids. The unknown amino acids identified were Glycine and Methionine. Introduction Proteins in cells are important in many ways. There are different types of proteins such as
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Titration Lab How Much Citric Acid is in Your Soda? PURPOSE To determine the molarity (concentration) of citric acid (H3C6H5O7) in various different citrus flavored sodas. BACKGROUND PRINCIPLES Popular sodas all strive for a somewhat sour (’tart’) flavor and manufacturers utilize acids to impart this taste. While there are a vast variety of different brands of sodas on the market‚ they can be broken into two main categories: dark or clear. This differentiation is not only a simple color
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are several purposes to the amino acid lab experiment. One reason is to help us understand the concept of acids and bases and how they interact with one another. Another purpose is to understand what occurs when placed with the existence of buffers. Lastly‚ the experiment is to help us understand the applications of titrations and how it can be used in a real world setting‚ in this case‚ the identification of an amino acid. One must understand that amino acids all have special characteristics
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Title: Estimation of Ascorbic acid Aim: To determine the ascorbic acid content of canned apple and orange juice To determine the volume of canned juice necessary to provide 75mg of Vitamin C Introduction: For the estimation of ascorbic acid‚ the method used involved the titration of the ascorbic acid‚ in the presence of a redox indicator 2‚6-dichlorophenol-indophenol (DCPIP) which acts as both an oxidant so as to oxidise the ascorbic acid to dehydroascorbic acid‚ and it acts as an indicator
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Anna Powell 2nd I.Title: Acid-Base Titrations AP Chemistry Laboratory #6 II.Purpose: The purpose of this experiment is to standardize a sodium hydroxide solution and use the standard solution to titrate an unknown solid acid. The equivalent mass of the solid acid will be determined from the volume of sodium hydroxide added at the equivalence point. The equilibrium constant‚ Ks‚ of the solid acid will be calculated from the titration curve obtained by plotting the pH of the solution versus
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5% and 21
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