EXP-10 CHEM 233L SYNTHESIS OF p-BROMOANILINE Introduction: In this experiment‚ p-bromoaniline was synthesized in three steps starting from aniline. Since the amino group of aniline is a strong activator of aromatic ring‚ direct bromination is impractical (equation 1). In order to make a desired product‚ amino group needed to be protected as the acetamide which also maintained ortho and para position but slowed down the rate of reaction (equation 2). Slow reaction rate would increase
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Grignard reaction. As the reaction was to set up to produce a Grignard reagent and then recrystallize it to obtain pure sample. The percentage yield obtained was 55% and its melting point was 161 co which is within the literature value 160-163 co. In addition to that the IR spectroscopy confirmed the molecule structure to be triphenylmethanol. Introduction: The Grignard reagents are alkyl magnesium halides‚ R-Mg-X were first introduced in 1900. These reagents are usually prepared by reacting one atom
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Vegetative reproduction (vegetative propagation‚ vegetative multiplication‚ vegetative cloning) is a form of asexual reproduction in plants. It is a process by which new individuals arise without production of seeds or spores. It can occur naturally or be induced by horticulturists. Although most plants normally reproduce sexually‚ many have the ability for vegetative propagation‚ or can be vegetatively propagated if small pieces are subjected to chemical (hormonal) treatments. This is because meristematic
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Jr.‚ 2013). This reaction is best used for making six membered rings with different functional groups. The reaction is called a 4+2 cycloaddition because a ring is formed by four pi electrons in the diene interacting with two pi electrons of the alkene or alkyne (Wade‚ Jr.‚ 2013). In this experiment anthracene was used as the diene and considered to be electron rich in the reaction. Maleic anhydride was the electron poor dienophile used in the reaction. The reaction converted two pi bonds into two
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positive result for the chloride test. Bromine Br2 (l or aq) A dark red liquid - orange-brown fumes‚ yellow-orange aqueous solution. The other common orange-brown gas is nitrogen dioxide (i) Shake with a liquid alkene. (ii) Mix with silver nitrate solution. (ii) Decolourised. See alkene test. (ii) Cream ppt. of silver bromide as in the test for bromide. (i) Forms a colourless organic dibromo-compound >C=C< + Br2 ==> >CBr-CBr< (ii) Ag+(aq) + Br-(aq) ==> AgBr(s) Any soluble bromide gives
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This lab will allows the comparison between elimination reactions under acidic and basic conditions through an analysis of two separate reactions: an acid-catalyzed dehydration of 1-butanol and 2-butanol using sulfuric acid and a dehydrobromination under basic conditions using potassium tert-butoxide of 1-bromobutane and 2-bromobutane. The products of all four reactions will be analyzed with gas chromatography‚ which separates organic compounds to see how each reaction’s product are formed under
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bond between two Carbon atoms‚ they are "unsaturated" hydrocarbons. Their names follow a similar pattern: ethene‚ propene‚ butene‚ pentene‚ etc..It is not possible to have "methene" because there have to be TWO atoms of Carbon in a molecule of an alkene. Think about it. Here is a general formula for the alkenes:By now you will have realised that the spelling of chemical names is very important. |
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conditions‚ involves the nucleophilic addition of an enolate ion to another carbonyl group. The resulting product‚ a beta-hydroxy ketone or aldehyde‚ is called an aldol because it contains both and aldehyde group and the hydroxy group of alcohol. Condensations‚ including aldol condensation‚ combine two or more molecules‚ typically with a loss of a smaller molecule (including water or alcohol). In the presence of a base‚ the aldol condensation occurs by a nucleophilic addition of the enolate ion (a strong
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contains four sections‚ SECTION A to SECTION D. Instructions: Answer all questions in SECTION A - SECTION D. Make sure that the section heading is included and your answers are correctly numbered. The assignment must have a completed cover sheet. It must be placed in the drop-box on or before the deadline. st SECTION A ELECTRONIC STRUCTURE & IONIZATION ENERGY 1. 2. Write the electronic structure in s‚p‚d notation of the following: O‚ Na‚ Na+‚ Al‚ Cl- and Co
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SYLLABUS – ADVANCED PLACEMENT CHEMISTRY Required Texts 1. Chemistry: The Central Science by Brown‚ LeMay and Bursten‚ 10th ed.‚ Pearson Education. Inc.‚ Upper Saddle River‚ NJ‚ 2006‚ ISBN: 0131464892 Includes: Text book‚ Laboratory Manual‚ Student Study Guide‚ AP Test Prep Series‚ Solutions to Practice Problems 2. Barrons AP Chemistry‚ Jespersen‚ Neil D‚ 4th ed.‚ Barron’s Educational Series‚ Inc‚ 250 Wireless Boulevard‚ Hauppauge‚ New York 11788
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