2.4.General procedure for the synthesis of 2‚3-dihydriquinazolin-4(1H) ones derivatives: A stirred mixture of isatoic anhydride (1 mmol)‚ amines containing 2-aminobenzothiazole or 2-amino benzimidazole (1.1mmol)‚ aromatic aldehydes (1 mmol) and 0.045 g of H-ZSM-5 nanozeolite was reacted in an oil bath at 100 oC for the appropriated times. Completion of the reaction was indicated by TLC. After completion of reaction‚ the mixture was cooled to room temperature. The solid residue was dissolved in hot
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Methylprednisolone sodium succinate 1) Structure: 2) Name: Methylprednisolone sodium succinate 3) A-Methapred is a sterile powder used as an anti-inflammatory glucocorticoid‚ which contains methylprednisolone sodium succinate as the active ingredient. A-METHAPRED™ is available in several strengths and packages for intravenous or intramuscular administration. It is used as replacement therapy in adrenocortical deficiency states. Their synthetic analogs are primarily used for their anti-inflammatory
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Ambrose Bierce’s writing style and choice of structure. Ambrose Bierce uses a very unique writing style he makes things sound happy and joyful but at the same time dark and depressing. In An Occurrence at Owl Creek Bridge‚ we are told the story of Peyton Farquhar’s hanging and escape. In the story we are led to believe he escapes the noose last second but as the story continues it hints more and more towards his death. As the story continues it tells how he is drifting down the river spinning hinting
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Biochemistry Lecture Exam 1 Study Guide Chapter 1: Biochemistry: An Introduction I. Introduction a. Biochemistry: the study of molecules and chemical reactions of life b. Divided into 3 principal areas: 1. Structural chemistry of components of living matter & relationship of biological function to chemical structure 2. Metabolism – total chem reactions that occur in living matter; building & breaking down of molecules 3. Chemistry of processes & substances that store & transmit biological
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A carbohydrate is an organic compound that consists only of carbon‚ hydrogen‚ and oxygen‚ usually with a hydrogen:oxygen atom ratio of 2:1 (as in water); in other words‚ with the empirical formula Cm(H2O)n. The carbohydrates (saccharides) are divided into four chemical groupings: monosaccharides‚ disaccharides‚ oligosaccharides‚ and polysaccharides. In general‚ the monosaccharides and disaccharides‚ which are smaller (lower molecular weight) carbohydrates‚ are commonly referred to as sugars.
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backbone tends to resist degradation‚ whereas heteroatom-containing polymer backbones confer biodegradability. Biodegradability can‚ therefore‚ be engineered into polymers by the judicious addition of chemical linkages such as anhydride‚ ester‚ or amide bonds‚ among others. The usual mechanism for degradation is by hydrolysis or enzymatic cleavage of the labile heteroatom bonds‚ resulting in a scission of the polymer backbone. Macroorganisms can eat and‚ sometimes‚ digest polymers‚ and also initiate
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*substitution (of a carboxylic/acid derivative) = addition + elimination - substitution at the tetrahedral intermediate from the addition of an organometallic to an aldehyde/ketone will not (usually) work as R- (i.e. H- or CH3-) is a bad leaving group - addition of a Grignard reagent to an aldehyde/ketone = stable tetrahedral intermediate (alkoxide) - addition of an alcohol to a carbonyl group in the presence of a base = unstable intermediate (hemiacetal/hydrate) - nucleophiles with good
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Organic Chemistry Basic Ideas: Carbon chains: Straight chains and branched chains‚ Numbering of chains and branches. Carbon Rings: Cyclic Molecules‚ Aromatic Compounds Types of Organic reactions: Combustion Addition Substitution Condensation Oxidation What is organic chemistry? Carbon compounds. Methane CH4 Hexane C6 H14 Ethane C2H 6 Heptane C7 H16 Propane C3H 8 Octane C8 H18 Butane C4H10 Nonane C9H20 Pentane C 5 H12 Decane C1 0 H22 Alkanes: Saturated Hydrocarbons
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had already existed in the leaf itself but needed to be separated from the other chemicals. Caffeine’s chemical structure is relatively similar to the nucleic acid purine in that they use nitrogen and is bicyclic but lacks an alkene‚ amine and an amide. Caffeine has a solubility of 67.0 g/100 mL in boiling water but tannins also boil in hot water to form catechin. Catechin cannot react with water but it can with calcium carbonate. The calcium carbonate was added into the reflux beforehand so the
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ACYL COMPOUNDS: SOAPS AND DETERGENTS Experiment # 8 I. Objectives To observe the general properties of carboxylic acids. To compare the acidity of carboxylic acids and phenols. To verify experimentally the interconversion among acyl compounds. To become familiar with the physical and chemical properties of fats and oils and to understand the chemical basis of these properties. To learn how to prepare soap. To compare the properties of soap and synthetic detergents. II. Data and
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