Separation of a Carboxylic Acid from a Neutral Compound by Extraction Reference: Smith‚ Chapter 2 (Acids and Bases) Introduction Carboxylic acids and phenols are two families of organic compounds that contain carbon‚ hydrogen and oxygen‚ and also react with water to yield an excess of hydronium ions over hydroxide ions. Pure water has a pH of 7‚ which means it has a hydronium ion concentration‚ [H3O+] of 10-7 M (M = molarity‚ moles/Liter). The hydronium ions in pure water come from the self-ionization
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Title:Extraction:Extraction with acid and alkaline Objective: 1. To recover benzoic acid and p-dichlorobenzene from its mixture using acid-alkaline extraction. 2. To determine the percentage recovery and melting point of benzoic acid and p-diclorobenzene. Apparatus:Separatory funnel(250mL)‚Buchner funnel‚beaker. Materials:Benzoic acid‚p-dichlorobenzene‚ether‚10% NaOH‚conc.HCl‚distilled water‚ anhydrous CaCl2. Introduction: Organic compounds in an aqueous mixture can be separated
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Determination of Calcium ions in milk using titration. Background Calcium is a mineral which is essential to the human body. In fact 1.5% of the human body is made up of calcium‚ and not just the obvious uses such as bone and teeth formation but it is also a vital factor in many enzyme reactions‚ for example blood clotting. It also partakes in the regulation of the hearts rhythm. Lack of the crucial mineral can result in the build up of cadmium and lead‚ both of which are toxic. along
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ACID BASE IMBALENCE INTRODUCTION The body normally maintains a steady balance between acids‚ produced during metabolism and bases that neutralize and promote the excretion of the acids.Many health problems may lead to acid base imbalance.Patients with Diabetis mellitus ‚COPD‚and kidney disease frequently frequently develop acid base imbalences. Vomiting and diarrhea may also cause acid base imbalance.The kidneys are an essential buffer system for
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concentration I have choose three volumes form my results table which I have added them and then divided by three to get an average results. Describe the stages you followed in collecting the primary data and any secondary data. Titration Steps: • Firstly we weighed the solid sample of sodium hydrogen carbonate with an accurate balance; then dissolved in distilled water up to 250ml to make a
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activity of sodium butyldithiocarbamate pentahydrate‚ C5H20NNaO5S2 Ayodele T. Odularu a‚ Peter A. Ajibade a‚ Bolhuis‚ A. b a. Department of Chemistry‚ University of Fort Hare‚ Private Bag X1314‚ Alice 5700‚ South Africa. b. Department of Pharmacy and Pharmacology‚ University of Bath‚ United Kingdom. Abstract Synthesis of sodium butyldithiocarbamate pentahydrate‚ C5H20NNaO5S2‚ entailed a one-pot synthesis. The process of synthesis involved the use of butyl amine‚ carbon(IV) sulfide and sodium hydroxide
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INTRODUCTION Sodium hypochlorite is considered one of the most efficient irrigant in endodontics 1-4. Due to its antimicrobial‚ tissue dissolving properties and low cost‚ it is one of the most widely accepted irrigant in Endodontic practice 5-8. Sodium hypochlorite as a solution is relatively an unstable compound. On exposure to organic compounds‚ heat‚ light‚ air and metals‚ the available chlorine ions reduce and there is subsequent loss of tissue dissolving and antimicrobial properties 9-10. Recent
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Determination of the Concentration of Acetic Acid in Vinegar Lab Exercise 4 CHEM 1106 9/19/12 Purpose: Standardize a sodium hydroxide solution using a primary standard acid. Determine the molarity and the percent by mass of acetic acid in vinegar by titration with the standardized sodium hydroxide solution. Introduction: Vinegar is a dilute solution containing acetic acid. Since vinegar has a low pH‚ it can be titrated with a base. Titration is a method used in order to ascertain the
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Prof. David B. Henthorn September 25‚ 2012 Summary The goal of this project was to determine the pre-exponential factor‚ k o ‚ the activation energy‚ E‚ and the reaction rate constants‚ k‚ of the saponification process of ethyl acetate using sodium hydroxide (NaOH) at 5 temperature between 15 and 25 degrees Celsius. Two trails were performed at temperatures 16‚ 18‚ 20‚ 22‚ and 24 degrees Celsius. The main equipment of the project were the jacketed beaker batch reactor and the LabPro conductivity
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Part A: Table 1: Fractionation of amino acid Fraction No | Response to Ninhydrin test(level of blue colour change) | Response to Sakaguchi test (colour change) | 1 | X | yellow | 2 | Dark blue | yellow | 3 | Dark blue | Pale orange | 4 | Blue | Pale orange | 5 | Pale blue | Pale orange | 6 | Blue | Pale orange | 7 | Pale blue | Pale orange | Discussion Part A In the separation and purification of a single protein or amino acids‚ a solution containing the desired analyte
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