Introduction Titration is a volumetric analysis technique used to find the concentration of an unknown substance. There are several types of titration but the one used for this experiment is called acid-base titration as the substance we are titrating is acidic. Acid-base titrations are based on the neutralisation reaction between the analyte and the acidic or basic titrant. The analyte is the solution of unknown concentration and the titrant is the solution of accurately known concentration used
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Experiment 4 SOLUTION STOICHIOMETRY ACID-BASE TITRATIONS Determination of the Percent Acetic Acid in Vinegar Objectives: (1) To introduce and use the concept of solution stoichiometry (2) To specifically use solution stoichiometry to determine the percent of acetic acid in vinegar. (3) To prepare a standard solution by the method of titration. Consider the following balanced chemical equations: (1) HCl + NaOH ------> NaCl + HOH (2) H2SO4
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CHM 3120L ANALYTICAL CHEMISTRY I LABORATORY REPORT EXPERIMENT: DETERMINATION OF ASCORBIC ACID BY REDOX TITRATION Name: Section: Date Experiment Completed: 2.0008 g KIO3 x (1 mol/214 g KIO3) = 0.0093495327 mol KIO3 0.0093495327 mol KIO3 / 0.500 L = 0.0186990654 M KIO3 6 Na2S2O3 + KIO3 + 6 H+ → I-+ 3 H2O + 3 S4O62- + K+ + 12 Na+ 0.0187 M KIO3 × 0.025 L = 4.675 x 10-4 mol KIO3 4.675 x 10-4 mol KIO3 x (6 mol Na2S2O3 / 1 mol KIO3) = 0.002805 mol Na2S2O3 0.002805 mol Na2S2O3
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INTRODUCTION Differences between acids and bases An acid-base reaction is based on the reaction involving the ionization of water H2O -> H+ + OH- This means that water can break apart into a hydrogen ion and a hydroxide ion. These two ions can also join together to form a water molecule. When a strong acid is placed in water‚ it will ionize completely‚ and break down into its constituent ions in which one of it a hydrogen ion. When a strong base is placed in water‚ it will ionize
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Vitamin C Introduction: The lab consists in determining the vitamin C concentration in a solution by a redox titration using iodine. Vitamin C (ascorbic acid) is a water-soluble‚ essential oxidant that plays a vital role in the protection of the body from infections and disease it is acquired from primary fruits and vegetables. With the use of different materials as natural orange juice‚ Tampico (chemical orange juice) and other solutions that contain vitamin C we will find the amount of vitamin
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OXIDATION-REDUCTION TITRATIONS REDOX TITRATION • involves oxidizing agents and reducing agents titrants and analytes • oxidizing agents used as standard solutions: potassium permanganate‚ KMnO4 potassium dichromate‚ K2Cr2O7 iodine‚ I2 ceric sulfate‚ Ce(SO4) 2 potassium iodate‚ KIO3 REDOX TITRATION • reducing agents used as standard solutions: ferrous sulfate‚ FeSO4 oxalic acid‚ H2C2O4 sodium oxalate‚ Na2C2O4 sodium thiosulfate‚ Na2S2O3 titanous chloride
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IUPUI October 12‚ 2012 Titration of Acids and Bases Introduction According to Arrhenius definition‚ acid is substance that produces H3O+ ion while base is substance that produces OH- ions. The reaction between acid and base often yields the products of salt and water. The formation of water in this neutralization reaction is caused by the combination of H3O+ and OH- ions. In order to determine the concentration of an unknown acid and base‚ a method called acid-base titration is used. The end of
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SODIUM gSodium is a chemical element with the symbol Na (from Latin: natrium) and atomic number 11. It is a soft‚ silver-white‚ highly reactive metal and is a member of the alkali metals; its only stable isotope is 23Na. The free metal does not occur in nature‚ but instead must be prepared from its compounds; it was first isolated by Humphry Davy in 1807 by the electrolysis of sodium hydroxide. Sodium is the sixth most abundant element in the Earth’s crust‚ and exists in numerous minerals such
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thereby ensure the solution is of uniform concentration throughout. Standardisation of Sodium Hydroxide 1. Prepare the burette and fill with the sodium hydroxide solution to 50ml. 2. Pipette the KH(C8H4O4) solution into a conical flask. Use three drops of phenolphthalein as the indicator. 3. Titrate carefully until a colour change from colourless to pink is observed. 4. Perform a rough titration first‚ then repeat until 3 concordant
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Abstract By using acid-base titration‚ we determined the suitability of phenolphthalein and methyl red as acid base indicators. We found that the equivalence point of the titration of hydrochloric acid with sodium hydroxide was not within the ph range of phenolphthalein’s color range. The titration of acetic acid with sodium hydroxide resulted in an equivalence point out of the range of methyl red. And the titration of ammonia with hydrochloric acid had an equivalence point that was also out of
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