Determination of Fe by Redox Titration Matt Cuff Quant 320L October 21‚ 2011 Abstract In this experiment the percent of iron in an unknown sample will be determined by using a redox titration and then compared to a different method. A primary standard which in this case is ferrous ammonium sulfate will be used to standardize potassium dichromate. The standardized potassium dichromate will then be used to titrate the unknown iron sample using the indicator p-diphenylamine sulfonate.
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Acid-Base Titration Background Information A titration is a controlled addition of one substance into another substance. In an acid-base titration‚ the experimenter will add a base of known concentration to an acid of unknown concentration (or vice-versa). The goal of the titration is usually to use the substance of known concentration to determine the concentration of the other substance. In order to run a titration‚ the following materials are needed: • A buret filled with the base (or acid) of
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Titration is a method used to help determine the concentration of an unknown solution (the analyte) by using a solution of known concentration (the titrant).1 In medicine‚ titration helps doctors determine unknown concentrations of substances in the blood or urine‚ and it is useful in determining the proper dosage of medication. Titration can determine fat and water contents‚ and unknown concentrations of vitamins. With food‚ titration can be used to determine whether cheese or wine is adequately
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Acid-Base Titration and Volumetric Analysis The purpose of this experiment is to determine the [NaOH] of a solution by titrating it with standard HCl solution‚ to neutralize a known mass of an unknown acid using the NaOH solution as a standard‚ to determine the moles of NaOH required to neutralize the unknown acid‚ and to calculate the molecular mass of the unknown acid. Procedure: Part A: Standarized 0.10M HCl solution and unknown NaOH solution were poured into two beakers. The burets
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Aim: To calculate the concentration of acid in a sulphuric acid solution. Introduction: A titration is a method of analysis that will allow you to determine the precise endpoint of a reaction and the precise quantity of reactant in the titration flask. A burette is used to deliver the second reactant to the flask and an indicator is used to detect the endpoint of the reaction. So a chemical reaction is set up between a known volume of a solution of unknown concentration and a known volume of
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Precipitation Titration Mohr Method Experimental The chloride ion (Cl-) is an important anion found in solids and solutions. In this experiment‚ the amount of chloride ion in an unknown sample J (NaCl + KCl mixture) of water using the Mohr method is determined‚ which relies on the solubility differences of two anions and the titration endpoint of a precipitate. The net ionic reaction during the titration is as follows: Ag+ + Cl- → AgCl(s) The Ksp for AgCl is 1.8 x 10-10 and
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added the solution will quickly start to turn yellow due to formation of MnO2. If this happens anyway‚ add some more sulphuric acid to reverse the process. The solution should be clear with a slight green tinge. Chapter 15 – Volumetric analysis (Redox titrations) To prepare a standard solution of ammonium iron sulphate and use this solution to standardise a solution of potassium permanganate. Potassium permanganate (KMnO 4 ) is a powerful oxidizing agent and is a deep purple colour. It cannot be
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Acid/ Base Titration Lab Design III Materials: Goggles HCl NaOH Distilled Water Label Beaker Graduated Cylinder Pipet Stirring rod Buret with clamp Stopper Ring Stand Utility Clamp Computer Computer Program pH probe Procedure: 1) 2) Goggles were put on. 3) 0.1 M NaOH solution was made using 0.4 g NaOH and 100 mL distilled water. The ingredients were added together in a beaker and stirred. 4) The buret was standardized by adding 10 mL of distilled water‚ rolling
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a chelating ligand. The base‚ EDTA‚ will bind to the metal ions‚ which serve as the Lewis acid‚ thus playing a role as a ligand. The indicators used in EDTA titrations are metal ion indicators. Metal ion indicators work by the presence of absence of metal ions. Just like EDTA‚ the metal ion indicators will bind with metals. When the titrations begin‚ Mg2+ will be formed in a complex with the indicator. Once EDTA is added‚ it binds to the free Mg2+ ions‚ and then it reacts with the Mg2+ ions that
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Weak Acid Titration Abstract: Our method for determining the unknown weak acid was to determine the equilibrium constant K from the molecular weight of the weak acid from our titration data. In this lab the acid Potassium hydrogen phthalate and two unknown acids were titrated. We determined the molar mass of the Potassium hydrogen phthalate‚ for the unknown acids we calculated the molar mass and the Ka values. We used NaOH as the known base for titrating in all three of the titrations. Our ka
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