CHEMISTRY 101.1 Intermediate Chemistry Laboratory I Institute of Chemistry University of the Philippines‚ Diliman I. Synthesis of Salicylic Acid Purpose: Part I of the experiment illustrates the base hydrolysis of an ester‚ methyl salicylate‚ to form salicylic acid through nucleophilic acyl substitution. Procedure: Dissolve 12 g NaOH in 70 mL water in a 150 mL round bottom flask. Add 5.0 mL methyl salicylate and reflux the reaction mixture at its boiling point for 15 minutes using a stirrer
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In modern day‚ man does not truly think about how much the earth means to life. On the contrary‚ humans aspire to cease Mother Nature’s beauty with the replacement of modern day cities made up of synthetic nature. Since the dawn of the twentieth century‚ a major theme in the American Arts has been the protest against man’s destruction of the natural world. With this in mind‚ as very well argued in Chief Seattle’s article “Respect”‚ humans fail to be conscious of the physical and sentimental value
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aqueous solution of formaldehyde is called formalin. The commercially available formalin has 10 to 12% methanol with a few impurities like aluminum and copper. Almost 21 million tonnes of formaldehyde is produced annually all around the world. Synthesis of Formaldehyde Formaldehyde is produced by catalytic oxidation of methanol. A mixture of molybdenum and iron or silver is used as a catalyst in such a reaction. But a more commonly used process is FORMAX. In this process‚ methanol and oxygen
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ApEnglish Language and Composition Reading Time: 15 minutes Suggested Writing Time: 40 minutes Directions : The following prompt is based on the accompanying seven sources This question requires you to synthesize a variety of sources into a coherent‚ wellwritten essay. Synthesis refers to combining the sources and your positions to form a cohesive‚ supported argument and accurately citing sources. Your argument should be central; the sources should support this argument. Avoid merely summarizing sources. Introduction
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Explanatory Synthesis A countless number of children in the United States were taught to believe that you could accomplish anything if you worked hard. This American dream has now become an American nightmare. According to the information in the Hart Research Associations titled “Raising the Bar‚” “ How the Rich are getting Richer and Poor are getting Poorer‚” and the Workforce Commission powerpoint‚ Americans are faced with many obstacles to learn how to survive in the economy. The main discussion
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Gringard Synthesis detailed procedure and scheme of the apparatus any changes to the original procedure‚ actual masses‚ and obs yield calculations and mp Discussion outline Grignard rxn (what is it used for‚ why important‚ the mechanism) Reaction set up (important details) How can the rxn be activated Second step: rxn of the Grignard reagent with acetophenone‚ quenching with ammonium chloride Isolation of the product‚ identification Possible or actual sources of error Part one of our experiment
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Experiment 2 and 3: Synthesis of Aspirin and Determination of Melting Point A. Abstract Aspirin is the common name for the compound acetylsalicylic acid‚ widely used as a fever reducer and as a pain killer. The first part of the experiment aims to synthesize aspirin from the reaction of salicylic acid with acetic anhydride with the aid of phosphoric acid as a catalyst. The second part of the experiment aims to assess the purity of aspirin through the determination of its melting point and
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Synthesis of DEET Abstract: For this experiment m-toluic acid was reacted with thionyl chloride resulting in a nucleophilic acyl substitution which could then be used to create DEET with excess diethyl amine (Figure 1). This was done by adding diethyl amine drop wise using a seperatory funnel which resulted in a gas formation which was controlled with a condenser attached to a gas vacuum. The resulting mixture was then washed to remove excess acids and bases and rotovapped. DEET was synthesized
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Experiment 23: Synthesis of an Alkene April 5‚ 2013 Purpose: Results and Discussion The weight of our n-Butyl Bromide sample (actual yield) was 0.09g. The percent yield was found to be 4.38%. Only 0.09g of the theoretical 2.055g yield was obtained. The boiling point was 104° C‚ which is higher than the literature value of 101° C. This is due to the sample being somewhat impure‚ as impurities tend to increase boiling point. When IR spectroscopy was performed‚ there were no OH stretches
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replication in a eukaryotic cell is more difficult. DNA of an eukaryotic cell is in chromatin form to fit into the small nucleus for the replication to occur‚ first the DNA should open. This is because it is harder for eukaryotes to carry out DNA synthesis. Replication of DNA in a prokaryote is different from a eukaryote. In a prokaryote they have a single origin where the replication process starts. Also eukaryotes synthesize the same time they are being transcribed‚ and ribosomes will be active
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