FOUNDATION IN SCIENCE INTRODUCTION TO PRACTICAL ORGANIC CHEMISTRY – MAKING AND PURIFYING ORGANIC COMPOUNDS Stage 1 – Deciding how much reagent to use Most organic reactions do not go to completion; most reach an equilibrium position with significant quantities of reactants still remaining. In addition‚ separating the desired product from the rest of the reaction mixture‚ and then purifying it‚ will result in the loss of more of the product. The amount of product obtained expressed as a percentage
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CH4300/PY5140 - EXPERIMENT 2 – Answer Sheet SYNTHESIS OF THE PHARMACEUTICAL ASPIRIN (ACETYLSALICYLIC ACID) Aim: The aim of this experiment was to react salicylic acid with ethanoic anhydride to produce Aspirin. CH3CO)2O + HOC6H4COOH → CH3CO2C6H4CO2H + CH3COOH i Mass: 5g Volume: 7.5 cm3 Mass: 6.52g RMM: 138g/mol RMM: 180g/mol Moles: 5/138 = 0.0362 RMM: 102g/mol Moles: 0.0362 OBSERVATIONS – First‚ Ethanoic acid was added to the salicylic acid which resulted
Free Aspirin Acetic acid Acetic anhydride
Liquid Chromatography Analysis of Aspirin Problem: Was aspirin (acetylsalicylic acid) successfully synthesized? Are there impurities or by-products present in the synthesized aspirin? How pure is the synthesized aspirin? Introduction: In the last experiment‚ aspirin was synthesized followed by characterization of the product using several different techniques. Melting point was a test that provided information about the identity and purity of the aspirin product. The iron(III)chloride test
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Aspirin Synthesis Introduction Out of all the pharmaceutical drugs in the worlds‚ aspirin is made the most. Any potential pharmacist must be familiar with synthesizing the drug. The goal of this lab is to synthesize as much pure aspirin as possible. The reactants‚ acetyl anhydride and salicylic acid‚ must react in phosphoric acid. With phosphoric acid as a catalyst‚ the reaction yields aspirin and acetic acid. The equation for the reaction is as follows: “(CH3CO)2O + HOC6H4COOH □(→┴yields ) CH3CO2C6H4CO2H
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Synthesis of Aspirin (Acetylsalicylic Acid) Abstract: This experiment is about the synthesis of aspirin under laboratory conditions. Aspirin is prepared by reacting salicylic acid and acetic anhydride; in the presence of sulfuric acid. After fully dissolving the salicylic acid with acetic anhydride‚ the solution is cooled and cold water is then added. Once the crystals form they are then filtered and left to dry out. There mass is measured and recorded then the yield is calculated. Introduction:
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ATLANTIC COLLEGE CHEMISTRY DEPARTMENT (Written by Dr Geoffrey Neuss) CONTENTS Page Introduction 1 Assessment of Practical Work 3 Error and uncertainty 7 Significant figures 8 Title 1. Some common chemical reactions. 9 2. A traditional acid-alkali titration. 10 3. Analysis of aspirin tablets
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Chemistry 121 Colligative Properties Lab Demonstration of Selected Calculations from Choice I Determination of Kf for Naphthalene To determine the Kf for naphthalene‚ we need to find the difference in the freezing point of pure naphthalene and the solution of 1‚4-dichlorobenzene in naphthalene. Let’s say that we did this experiment‚ used 1.00 g 1‚4-dichlorobenzene in 10.00 g naphthalene‚ and found that the freezing temperature of pure naphthalene was 78.2°C‚ while that of the solution was 75
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purpose of this lab is to synthesise acetylsalicylic acid (aspirin) by creating a reaction between acetic anhydride and salicylic acid. This was be accomplished through the use of recrystallization. Acetic anhydride and salicylic acid are mixed together‚ and then acidified by the addition of a few drops of concentrated sulfuric acid‚ which catalyzed the reaction. The percent yield is calculated to determine the effectiveness of the reaction in preparing the desired product (aspirin). The limiting
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The purpose of this lab was to see which solutions are soluble and which are not. We were able to see this by mixing certain solutions together and observing changes that occurred. The procedure for this experiment included a few different steps. The first steps were to add the nitrate solutions into the lettered parts of the 96-well plate. Once you were done with that‚ you were supposed to add the sodium solutions to the numbered parts of the 96-well plate‚ so that the solutions were added together
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Rebecca Boreham 7/1/14 Chem 2423 Experiment #5 Synthesis of Aspirin Elizabeth Ajasa Kaylee Seymour Lauren Hatfield Suveda Perikala Introduction/ Purpose Aspirin is the most commonly used drug in the United States. Forty million pounds are produced each year. The chemical name for aspirin is Acetylsalicylic acid. Aspirin is a pain reliever and a fever reducer. Aspirin originated from the bark of a White Willow Tree. Chewing the bark however is extremely acidicand irritates the mucous membranes
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