Synthesis of Aspirin Name: Xuanyi Li Teaching assistant: Deirdre Zwilling November 15‚ 2009 Purpose: To synthesize aspirin‚ a common analgesic drug‚ via nucleophilic acid-catalyzed substitution reaction of salicyclic acid with acetic anhydride. The whole reaction is catalyzed by phosphoric acid. (The experiment involved three parts: The synthesis of aspirin‚ the isolation and purification of aspirin‚ and the estimation of the purity of the final product.) [pic] Procedure[1]: A mixture
Free Aspirin Carboxylic acid Salicylic acid
Maggie Mitchell IB Chemistry Prd. 5 THE HALOGENS LAB Date: 9/11/13 Purpose: The purpose of this experiment was to observe and record the halogens’ (NaF‚ NaCl‚ NaBr‚ and KI) reactions with the chemicals Ca(NO3)2‚ AgNO3‚ and NH4OH and use these observations to identify an unknown halogen. Data: (see next page) TABLE 1: REACTIONS OF HALOGENS WITH CA(NO3)2‚ AGNO3‚ AND NH4OH REACTION NAF NACL NABR KI REACTION W/ CA(NO3)2 solution turns cloudy and precipitate forms clear precipitate
Premium Chlorine Periodic table Chemical element
Synthesis of Aspirin Chemistry Standard Level Lab Report Data Collection and Processing and Conclusion and Evaluation Date: December 8th‚ 2011 Purpose: The purpose of this lab was to synthesize aspirin‚ determine the theoretical yield‚ compare the percent yield to the theoretical yield and test the purity of aspirin by adding Iron (III) chloride to the product. Hypothesis: I hypothesize that salicylic acid will react with acetic anhydride to produce acetylsalicylic acid (aspirin) and
Premium Aspirin Acetic anhydride Acetic acid
Being able to extract a compound or substance from a product or object will encourage us in being able to do the same in a similar manner with a tea solution. Extracting compounds is an important step in any kind of organic chemistry lab and will help us be better at accomplishing the experiment in a much faster and accurate rate than from before. Experimental To begin the experiment‚ a tea solution must be made by incorporating a tea bag into a beaker filled with almost boiling water and the
Premium Caffeine Tea Water
conduct the synthesis of aspirin‚ acquire the skills of recrystallisation using normal filtration and reinforce the technique of the melting point determination. The method used to synthesize aspirin was esterification by reacting salicylic acid with acetic anhydride with the presence of dehydrating agent‚ conc. sulphuric acid‚ to speed up the reaction. Having obtained the crude aspirin which was still impure‚ recrystallisation was conducted to remove the impurities. The aspirin harvested at the end
Free Aspirin Carboxylic acid Salicylic acid
Lab 1: Synthesis of Aspirin Introduction: The purpose of this lab was to demonstrate the ability to easily alter the molecular structure of a compound to greatly increase its utility. In this case‚ an acetyl group was added to salicylic acid‚ a naturally occurring compound with significant pharmaceutical value. Without the addition of the acetyl group‚ salicylic acid is an irritant to the gastro-intestinal (GI) tract. Once the acetyl group is added via a simple reaction‚ acetylsalicylic
Premium Oxygen Aspirin Acetic acid
EXPERIMENT A PREPARATION OF ASPIRIN Abstract This report gives a detailed account of the experimental preparation of aspirin in a laboratory environment as well as some basic industrial background on the product. It also contains information about safety precautions put in place to ensure the safety of the team who carried out the experiment. All results obtained have been included as well as a detailed analysis of what they represent alongside any improvements to the method used. Introduction
Premium Acetic acid Aspirin Acetic anhydride
Jennie K. Daniels Organic Chemistry 2121 11 February 2014 Synthesis of Aspirin Salicylic acid derivatives‚ or salicin‚ are found in the bark of the willow tree. In the 5th century B.C.‚ Hippocrates ground the bark into a powder‚ and later‚ the Natives Americans chewed on the bark to alleviate fever and pain1. In the 19th century‚ a German chemist by the name of Felix Hoffman wanted to find a medication that would ease
Premium Aspirin
CHEM/ENCH 212 EXPERIMENT II: KINETICS OF NUCLEOPHILIC SUBSTITUTION DATE OF SUBMISSION: Table of Contents Experimental Table : Hazardous properties of chemicals used in the experiment.[1] Acetone Irritant. Do not inhale vapors. Highly flammable. 2 chloro‚ 2 methyl propane Flammable. Equipment 1. Conductivity probe 2. Constant temperature water circulation bath 3. Stir-plate with stirring magnets
Premium Chemistry Chemical reaction Oxygen
Alka-Seltzer Rocket Formal Lab Report Abstract In the Alka-Seltzer Rocket lab one was to experimentally determine how much (grams) Alka-Seltzer and water in mL‚ is needed to launch the rocket the highest/longest distance in cm. Also to experimentally determine the % NaHCO3 in the tablet using the information from the highest/longest distance. Calculate the error and % error of NaHCO3 in an Alka-Seltzer tablet and to determine the limiting reagent for the highest/longest distance traveled. Alka-Seltzer
Free Acetic acid Sodium bicarbonate Vinegar