Multistep Synthesis of Tetraphenylcyclopentadienone Author: Instructor: Date work performed: 10.18.2012--10.25.2012 Date work submitted: 11.01.2012 Abstract: The aim of this experiment was to perform a multistep synthesis to form tetraphenylcyclopentadienone. The first step of the reactions was to synthesize benzoin from the condensation of benzaldehyde. A yield of 28.91% benzoin was obtained. The MP of benzoin was 127O-130O C and the IR spectra displayed a carbonyl peak at 3415 cm-1
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Synthesis of 1-bromobutane from 1-Butanol using the SN2 Reaction Abstract: The objective of this experiment is designed to study the synthesis of 1-bromobutane from 1 butanol using a SN2 reaction.. The product will then be analyzed using a flamed loop test by use of fire. Reaction Mechanism: CH3CH2CH2CH2—OH H+ CH3CH2CH2CH2— +OH2 Br- CH3CH2CH2CH2—Br + H2O 1-butanol
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Synthesis of benzilic acid from benzoin utilizing a multi-step reaction. Names: Arian Karim TA Name: Sayantan Das Lab Day & Time: Thursday 7:30-11:40 Lab Section #: Abstract The main purpose of this experiment was to synthesize benzilic acid from benzoin. This requires a multistep synthesis with benzyl as an intermediate product. The first step required HNO3 as an oxidizing agent and the second step required KOH and HCl. The percentage yields of benzil and benzilic acid were 59.5%
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Affects of Hydrogen Peroxide Equivalents on Green Synthesis of Adipic Acid. Andrew R. Glessman*‚ Chase W. Turner‚ Audra Cokain‚ Jacob Kindred‚ Darryl Watkins Department of Chemistry and Chemical Biology‚ IUPU‚ 402 N. Blackford St‚ Indianapolis‚ IN 46202 aglessma@umail.iu.edu April 25‚ 2014 Figure _______________________________________________________________Abstract- The synthesis of adipic acid has been a growing topic of discussion due to the harmful impact it has on the environment
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http://www.chem-toddler.com/chemical-equilibrium/chromatedichromate.html http://ibchem.com/IB/ibnotes/full/aab_htm/18.3.htm In the experiment part (i) (a)‚ the solid copper(II) nitrate is used to dissolve in a test tube filled with half distilled water. The solid copper(II) nitrate ionize in water to form copper(II) ions and nitrate ion. Hence‚ a blue solution is formed due to the blue copper(II) ion present in the solution. When excess solid is added‚ the solution will become saturated and
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We measured its relative mass and recorded in our lab notebook. The liquid was consequently poured into the cylinder and the volume measured. To finish off the experiment‚ section three was conducted in order to compare samples of known liquids. Samples of olive oil‚ isopropyl‚ and water were obtained
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Video 1: how to be mkt orientated ch 1 3 The Success of a firm is not only determined by the mkt plan but also by growth and profits and mainly depends by two basic pillars: the 1st one is the business core competences i.e the technical skills‚ indusrty knowledge and manifacturing experience which allow to develop excellent products or services. The other pillar is the drive and commitment to organization. Successful firms are driven by leaders which can inspire the firm with the vision of being
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Scale Size Analysis What’s it like to be as small as a fly? What’s it like to be as big as an elephant? In a matter of scale‚ the perspective of life differs dramatically between the large and the small. The things we see in nature every day‚ sometimes it makes me think we live in a strange world. The similarities between “Joyas Volardores” and “A Matter of Scale” are that they both go in depth with nature. In “Joyas Volardores‚” Doyle talks about the heart of a hummingbird and a blue whale
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Synthesis Paper Focus Question: What role do the Harry Potter books play in children’s education? In my freshman year in high school‚ Mr. Mehta‚ the Head of the English department‚ made some changes to our school’s English curriculum. One of these changes included introducing the fifth book of the Harry Potter series‚ Harry Potter and the Order of Phoenix‚ to our reading list. Mr. Mehta’s simple action attracted more attention than ever before! While students lauded his decision‚ most parents
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Abstract: The purpose of this lab is to prepare phenylmagnesium bromide‚ a Grignard reagent‚ and react it with benzophenone to give triphenylmethanol. Once made‚ the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone‚ benzophenone. The result is an alkoxide that is then protonated to give the alcohol‚ triphenylmethanol. The purity of the final product will then be considered by melting point and IR spectroscopy. Final purified triphenylmethanol weighed 8.02 grams
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