Synthesis of Salicylic Acid and Potentiometric Determination of its Purity and Dissociation Constant ------------------------------------------------- Abstract The purpose of the study is to synthesize salicylic acid from the ester‚ methyl salicylate‚ and determine the acid’s dissociation constant and purity. The ester was converted to salicylic acid by base hydrolysis. The products were refluxed and recrystallized‚ to ensure maximum purity‚ and filtered‚ dried‚ and weighed. The melting point
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VASAMID U~ A C R Co.‚ PBARLIVER‚X. Y . ] &Butyl Esters of Amino Acids and Peptides and their Use in Peptide Synthesis1 BY GEORGEv. ANDERSON i A ND FRANCIS. C.4LLAHAN M R ECEIVED NOVEMBER 1959 30‚ T he s ynthesis of t-but)-1 esters of amino acids and peptides and their use in peptide synthesis is described. T h e most convenient method was the acid-catalyzed reaction of isobutylene with benzyloxycarbonylamino acids or peptides followed by catalytic hydrogenation to produce the basic
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by everyday pollution from houses‚ factories‚ cars‚ and etc. This is the concept of acid rain‚ which according to EPA.gov is a broad term referring to a mixture of wet and dry deposition from the atmosphere containing higher than normal amounts of nitric and sulfuric acids. Acid rain isn’t just rain‚ its forms like hail or snow‚ which is wet deposition‚ and smoke or dust‚ which is dry deposition. The effects of acid rain are quite terrifying bringing all types of problems to the Earth‚ for example
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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of this experiment are to determine if the products derived from amide synthesis and Williamson Ether Synthesis are identical‚ and if one of the synthetic routes is more advantageous than the other. In Part 1‚ an attempt to synthesize acteophenetidin crystals by amide synthesis was made. We began by removing the colored impurities from the p-Phenetidine (reddish-brown) by placing 2g of the sample in 38 mL of hydrochloric acid and heating the solution to boiling point. Upon reaching just below boiling
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Multistep Synthesis of Benzilic Acid The synthesis of several complex organic compounds follows a multistep synthesis. "Multistep synthesis" refers to the procedure in which the product of one reaction serves as the starting material in the subsequent reaction. The multistep synthesis of benzilic acid begins with a conversion benzaldehyde to benzoin through a condensation reaction. The benzoin then oxidizes into benzil‚ which undergoes rearrangement to give benzilic acid. Benzoin Synthesis * When
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In the reaction mechanism‚ the alpha hydroxyketone’s hydroxylic group attacks the positively charged nitrogen from nitric acid attaching it to the molecule. The nitrogen’s electrons are then kicked off on to the oxygen bearing a positive charge‚ creating water. This process formed an organic nitrate. Next‚ water is used to abstract hydrogen from the positively charged oxygen‚ forming hydronium. A carbonyl is formed as well as nitrogen dioxide gas. Simultaneously the oxygen separates itself from nitrogen
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II. Synthesis This activity helps me to understand myself better by knowing what people think of me. It aims to foster self-awareness and self-improvement. I found out that my family thinks that I am a responsible person in terms of sense of responsibility. But my brother thinks I’m immature. In terms of duties at home‚ my mother and father understand that I don’t perform my duties because I’m busy with my studies. My sister thinks it too but she justified that I perform when I’m not busy. When
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NUCLEIC ACIDS I.BASIC CONCEPTS II.CLASSES III.CHEMICAL NATURE IV.FUNCTION I.BASIC CONCEPTS NUCLEIC ACIDS polymeric macromolecules‚ or large biological molecules‚ essential for all known forms of life are made from monomers known as nucleotides Each nucleotide has three components: a 5-carbon sugar‚ a phosphate group‚ and a nitrogenous base If the sugar is deoxyribose‚ the polymer is DNA. If the sugar is ribose‚ the polymer is RNA. Together with proteins‚ nucleic acids are the most
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Formic acid is known to be the simplest carboxylic acid‚ and it is an important factor in chemical synthesis and occurs naturally. The chemical formula for Formic Acid is CH202‚ and is mostly found in the venom of bee and ant stings. Formic acid is clear and colorless with a pungent odor. Formic acid is used in many ways; Formic acid is used to preserve livestock. It is also sprayed on animal food and fresh hay to reduce the decay rate. It can also be used as a pesticide to protect bee
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