solution of an acidic and organic compound and purify its respective acidic product through the techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through the Hirsch funnel into separate beakers of an aqueous
Premium Chemistry Acid Chlorine
Experiment 2: Acid- Base Extraction Separation of an Organic Acid‚ a Base and a Neutral Compound Introduction: The extraction technique is often used in the organic lab to separate organic compounds from mixtures. One type of an extraction technique is the acid-base extraction‚ which is used to separate organic compounds from a mixture based on their acid-base properties.1 There are certain principles that must be taken into account when choosing a solvent system to perform an extraction. The solvents
Premium Chemistry Acid
The obtained mass of benzocaine and benzoic acid mixture was measured to be 2.075 grams. Following being dried for a week the mass of benzocaine was recorded to be 0.250 grams‚ and benzoic acid was recorded to be 0.600 grams. The melting point range of benzocaine was measured to be 89.5°C-91.5°C‚ while benzoic acid’s melting point range was measured to be 129°C-131.3°C. The percent mass recovered was calculated to be 40.96% for the experiment. Table 1 illustrates the collected information. Starting
Premium Chemistry Oxygen Solvent
THE EXTRACTION OF DNA THE EXTRACTION OF DNA 07/02/2013 | By Laura Green‚ Tasnim Rahman and Sandra Strammiello | Table of Contents DNA………………………………………………………………………………………..………… 2 The Discovery of DNA…………………………………………………………………………...…………..…………. 4 The Steps for Extracting DNA…………………………………………………………………………………………….…..… 5 Experiment: Which Product Can the Most Visible Amount of DNA Be Extracted From?..............................................................................................
Free DNA
Wang Experiment #4 Recrystallization of Pure Phthalic Acid‚ Benzoic Acid and Napthalene Introduction Recrystallization is a important method in purifying organic compounds which are solid. It is an effective method that is important to be familiar with that is essential in the industrial chemical world. This experiment will allow students to be familiarized with the technique of recrystallization by working with phtalic acid‚ benzoic acid and naphthalene from appropriate organic solvents. Experimental
Premium Chemistry
necessary reaction schemes. The reaction schemes should include molecular weights and any other important physical data for the reagents and products. Ex. Cyclohexanol was oxidized to cyclohexanone using sodium dichromate in the presence of sulfuric acid. * Note: you can download a free version of a structure editor from ACD labs‚ the PC version is called chemsketch‚ the Mac version is called marvinsketch. You should learn how to draw structures using these programs. Lab reports should look professional
Premium Mathematics Phosphoric acid Carbon dioxide
from Benzoic Acid October 28‚ 2010 Abstract: This experiment was conducted to synthesize methyl benzoate from benzoic acid and methanol by using the Fischer esterification method. Methanol (12.5ml) and Benzoic acid (4.9 grams) are heated together in the presence of concentrated sulfuric acid (1.5ml) until equilibrium is achieved. A reflux apparatus is set up for 1 hour to carry out the reaction at the boiling point of the solvent (Methanol‚ 2.5ml). Then‚ separation though an extraction apparatus
Premium Distillation Benzene Oxygen
Unit 4 Assessment 2-Benzoic Acid Synthesis Synthesis and Investigation of Benzoic Acid Our aims: Create benzoic acid using benzaldehyde and hydrogen peroxide. Then remove some impurities from the benzoic acid crystals. Apparatus: Titration Pipette (25 cm3) Burette (50 cm3) Retort stand Clamp Conical flask (250 cm3) Volumetric flask (250 cm3) and stopper White tile Beakers (250 cm3) Dropping pipette Filter funnel Deionised water Phenolphthalein indicator Volumetric flask
Premium Chemistry Water Sodium hydroxide
Experiment 2&3 Recrystallization and Melting Points Determinantion of Benzoic Acid Abstract In experiment 2‚ recrystallization was used to purify the crude benzoic acid extracted from a mixture during experiment 1. Then a percent recovery for this recrystallization process was calculated. In experiment 3‚ the melting point ranges of the crude and purified benzoic acid were both determined by using Melt Temp Apparatus. Introduction Recrystallization is a purification technique for non-volatile
Premium Chemistry Liquid Water
A. Title – Acid-Base Extraction with Separatory Funnel B. Introduction – The main objective of the experiment was the extract an acid‚ a base‚ and a neutral compound from a 2:1:1 compound of benzoic acid‚ p-nitroaniline‚ and azobenzene. In theory‚ an extraction technique based on phase distribution should allow two immiscible solvents to separate with a portion of the solute distributed into each. Using a separatory funnel‚ acids were extracted with bases (NaOH)‚ and bases were extracted
Premium Chlorine Sodium chloride Acid