54.4% 15.765 g Melting Point of Intermediate (Benzoin) Melting Point of Product (Benzil) Trial 1 – 129-131°C Trial 2 – 133-135°C Trial 3 – 132-135°C Trial 1 – 92-93°C Trial 2 – 92-94°C Trial 3 – 93-95°C Average Melting Point Observed (Intermediate): 131.3-133.6°C Average Melting Point Observed (Product): 92.3-94°C Theoretical Melting Point of Benzoin: 132°C Theoretical Melting Point of Benzil: 94.5°C Discussion and Conclusions:
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Pat 1 Synthesis of 4-aryl-6-indolylpyridine-2-carbonitriles and evaluation of their biological activity Synthesis of 6-indolyl-4-aryl-3-cyanopyridine-2-one (1a-e) Employing the MCRs approach and microwave irradiation‚ an equimolar amounts of aromatic aldehyde‚ 3-acetylindole‚ ethyl cyanoacetate were reacted with excess of ammonium acetate in one-pot‚ reaction‚ under the microwave irradiation‚ afforded a novel series of 4-aryl-6-indolyl-nicotinonitrile-2-one derivatives 1a-e. Ethylene glycol was
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Available online at www.sciencedirect.com Nanomedicine: Nanotechnology‚ Biology‚ and Medicine xx (2011) xxx – xxx www.nanomedjournal.com Review Article Upconversion nanoparticles: synthesis‚ surface modification and biological applications Meng Wang‚ PhDa‚c ‚ Gopal Abbineni‚ MSb ‚ April Clevenger‚ MSb ‚ Chuanbin Mao‚ PhDb ‚ Shukun Xu‚ MSa‚⁎ a College of Sciences‚ Northeastern University‚ Shenyang‚ People’s Republic of China Department of Chemistry and Biochemistry‚ University of Oklahoma
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Microwave Synthesis of Benchmark Organo-iron complexes Chem 347/447 “Microwave synthesis of benchmark Organo-iron complexes” is an interesting article by Sean M. Garringer ‚ Andrew J. Hesse ‚ John R. Magers ‚ Kristopher R. Pugh ‚ Stacy A. O’Reilly and Anne M. Wilson which describes microwave- assisted technique in chemical synthesis. The authors detail the formation of various organo-iron species with the aid of a microwave. Using microwaves in chemical
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Aim Synthesis of Meso-1‚2-diphenyl-1‚2-ethanediol with focus on stereoselectivity Method Please refer to the CEM3005W practical manual for details on experimental procedure. Results and Analysis {Limiting reagent} Mass benzoin = 2.0050g (0.00945 mole) Mass sodium borohydride = 0.4059g (0.0107 mole) Mass compound A used to form compound B = 1.0647g Results Mass (g) moles Molecular formula Yield (%) Mp (pure) Compound A 1.7458 0.00815 C14H14O2 86.22 138-139 Compound C 0.4255
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the resin exuded from the bark of several species of Styrax trees. The fragrant resin smells like vanilla and is sometimes known as “gum benzoin”. It’s used to make incense and to slow fragrance release in perfumes. Benzoates are derived from benzoic acid. Today benzoic acid is made in the laboratory from other chemicals instead of being extracted from gum benzoin. Cinnamon contains benzoic acid. Source: AliciaC Benzoic Acid and Sodium Benzoate Pure benzoic acid is a white to colorless solid
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The synthesis of meso-1‚2-dibromo-1‚2-diphenylethane was successful as the final product of the experiment had the same physical properties of the theoretical properties‚ which were determined by TLC and melting point. The synthesis of diphenylacetylene was also successful‚ as TLC and the melting point both proved its identity‚ however the UV-vis analysis went awry due
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-APPLICATION OF ENZYMES IN ORGANIC CHEMISTRY Why enzymes in organic synthesis? | Alternative to chemical methods: * High region- and stereoselectivity * Milder reaction conditions * Environmentally more friendly | Which enzyme(s)? | OxidoreductasesHydrolasesLyasesIsomerases | Which reaction system? | AqueousAqueous and water-miscible organic solventAqueous and water-immiscible organic solventPure organic solventOther solvents (supercritical fluids‚ ionic liquids) | Which ‘chemistry’
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some amount of intelligence built-in [1]. Speech synthesis system has wide range of applications in our daily life. Speech synthesis plays an important role in signal processing. The natural‚ intelligible synthetic voices in the expanding field of speech technology had a lot of demand [4]. Speech was the natural form of human communication. Automatic speech signal generation on computers is commonly called speech synthesis. Speech synthesis was the artificial production of human speech [2]. Speech
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October 17 & October 24‚ 2012 How is Aspirin Made? This lab is about synthesizing aspirin using a hotplate to heat the reaction. It involved vacuum filtration‚ recrystallization‚ and comparing the properties of aspirin with salicylic aspirin. The first thing we did in this lab was make a hot-water bath by putting a beaker with water on a hot plate. After measuring out 2.1 grams of salicylic acid and 3 ml of acetic anhydride‚ we mixed the two together‚ along with 3 drops of sulfuric acid. We
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