Determination of Vanillin in Imitation Vanilla Essence Chloe Nolan 14832679 Introduction 4-hydroxy-3-methoxybenzaldehyde or as it is better known‚ vanillin is most commonly used to create imitation vanilla essence (Southam‚ 2013). Figure 1: vanillin structure Vanillin was first synthesised from eugenol from 1874 – 2001‚ from where it was later made from lignin- containing sulphite liquor which is a by-product of wood pulp processing in paper pulp manufacturing‚ most recently it is
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Once the 50 mL of CaCl2 solution from the other group is received‚ combine the two solutions in a beaker and stir until it is mixed. Set up the the filtering flask by attaching the buchner funnel in the opening top whole and the vacuum pump onto(over) the neck of the flask. Place filter on the buchner funnel‚ making sure it is not flat on top because the solution will
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soda * Funnel or piece of paper Hypothesis: * Yes‚ the higher the temperature‚ the faster the balloon fills up. * Yes‚ when the bottle is very big‚ it is the time where the balloon fills-up slowly because gasses need a lot of room spread out. * Yes‚ because the amount of vinegar or baking soda affects the production of carbon dioxide. Procedure: 1. Carefully pour the vinegar into the bottle. 2. Loosen up the balloon by stretching it a few times and then use the funnel to fill
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coffee cup. b. Fold a sheet of paper in half and then in half again. c. Open one section of the folded filter paper. d. Place the opened filter paper into the funnel‚ and the funnel into the paper cup. 7. Swirl the contents of the beaker. 8. Pour the contents of the beaker into the funnel. 9. After there is no more liquid in the funnel‚ take the filter paper and lay it somewhere to air dry. 10. When the contents are completely dry‚ weigh it. 11. Subtract the original weight of the filter
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0 grams of sawdust‚ - 300mL of water (H20)‚ - Beakers -a funnel -scale -a hot plate -dishes -tweezers * Procedure: 1) Gather and weigh materials. 2) Pour water into beaker. 3) Measure amount of water. 4) Mix salt‚ sand‚ sawdust and beads into water. 5) Use tweezers to separate beads from water and put them in a dish. 6) Put funnel in separate beaker and a filter in the funnel. 7) Pour mixture into the funnel to filter the sand and sawdust. 8) Separate the sand and sawdust
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Maleic anhydride underwent the Dials-Alder reaction with distilled cyclopentadiene as the dienophile. The reaction was a cycloaddition which produced cis-Norbornene-5‚6-endo-dicarboxylic Anhydride surface. (1) Product one had a mass of 9.351 grams and product two had a mass of 9.572 grams. The theoretical yield was found to be 10.047 grams‚ which makes the percent yield to be 93.07%. Melting Points were found to confirm the purity of the product. Product one had a melting point of 163.7-164
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PbNO3 and 1.44g of KI were acquired. 2) Assemble filtration system. The filter paper was to be folded and inserted into the funnel. Seal the filter paper to the funnel by using water. The funnel was set into the flask. 3) The substances were dissolved in 25 ml of water in beakers. 4) The solutions were thoroughly mixed together and then poured through the funnel. This separated the precipitate from the filter. 5) Separate the precipitate from the filter and place into beaker. 6)
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Quinn Kelly Kevin Hoover 9/12/12 PURPOSE The purpose of this lab was to analyze the amount of silver in an alloy using quantitative and qualitative observations. PROCEDURE 1. Prepare the Funnel and Filter Paper • Place the filter paper in the Buchner funnel‚ turn the water on and wet the filter paper with the acid wash. 2. Find the Mass of the Alloy • Find the mass of the empty beaker and then place the silver alloy in the beaker and weigh that. Subtract the
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LS Separation of Mixtures and Solids Purpose: To become familiar with the separation of mixtures of solids Hypothesis: I will be able to separate the materials using a variety of different methods. First‚ separate the iron fillings using a magnet. Second‚ I will put the rest of the solution into water and separate the insoluble sand from the soluble salt and benzoic acid. Third‚ I will filter out the benzoic acid when crystalized. Lastly‚ I will evaporate the water away leaving crystallized
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set of people‚ high upfront spending on online media is critical * Online media is also very successful in ensuring that an individual can see advertisements / displays multiple times. This would help in the subsequent stages of the brand check funnel. Multiple touch points
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