The Purity and Purification of Solids Recrystallization ABSTRACT In this experiment‚ impure adipic acid is purified though recrystallization. The impure adipic acid is dissolved in a solvent. After cooling it is ran through a vacuum filter to separate any moisture. The dry crystals are then weight for percent yield and the melting point range is taken to test the purity. There were two different trials ran in this experiment. The difference between the two was the addition of charcoal in
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PREPARATION OF ASPIRIN AND DETERMINATION OF THE MELTING POINT Ferrer‚ Lara Melissa V. Faculty of Engineering University of Santo Tomas Manila‚ Philippines ABSTRACT This experiment involved three steps: synthesis of aspirin‚ isolation and purification‚ and the estimation of purity of the final product. The synthesis involved the reaction of salicylic acid and acetic anhydride in the presence of a catalyst‚ phosphoric acid‚ H3PO4. When the aspirin was prepared‚ it was isolated and filtered. The percentage
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BOILING AND CONDENSATION BOILING • Phase change phenomenon where in transformation of liquid to vapour occurs at the saturation temperature of the fluid. It occurs at a solid/liquid interface due to convection heat transfer from the solid and usually occurs at surface temperatures higher than the saturation temperature of the fluid Agitation of fluid by vapor bubbles provides large convection coefficients Modified Newton’s law of cooling qs’’ h Ts Tsat Te • • • BOILING – CLASSIFICATON
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On Saturday‚ December 2nd‚ I saw the Live Newspaper Production of: BOILING POINT! Water‚ Politics‚ and Power. Boiling Point is production directed by Tom Harryman that gave a voice‚ while using satire‚ to show the flaws of how people of power in America deal with problems revolved around water. In this essay‚ I will analyze the audience‚ design‚ theme‚ acting‚ and the spectacle of the play. The audience had a mixed group of people. Even though I did not see anyone under that age of 17‚ I heard a
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the esterification of p-aminobenzoic acid with ethanol. The percent yield of crude product was determined to be 21% and the melting point was recorded at 86.2°C ± 0.2°C‚ with a 6.3% error from 92°C‚ the literature melting point of pure benzocaine. The crude product was then recrystallized to improve the purity of benzocaine and 57.4% was recovered. The new melting point range was measured at 89.1°C ± 0.3°C‚ which has a 3.15% error. The infrared spectrum of the recrystallized product was measured
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Title: Liquids and Solids Purpose: The experiment will help determine two important physical properties‚ boiling and melting point‚ of liquids and solids. Procedure: Before starting the experiment I gathered all materials appropriate for the experiment and prepare a safe environment for my experiment. I record the boiling point of the Isopropyl Alcohol and the melting point of powdered Acetamide with lab equipment such as the thermometer‚ capillary tube‚ beaker‚ test tube‚ and burner fuel
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and Purification of Solids Melting Points CH-337 Abstract: The purpose of this experiment was to find the eutectic point for the mixture of naphthalene and biphenyl. This was done by measuring the melting point of both pure substances and five mixtures of different ratios. The purpose of the second section was to identify an unknown sample by measuring its melting point and mixing it with two known substances and comparing them. The results suggest that the eutectic point is closest to the weight
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Separation Of a Sample Mixture By Liquid-Liquid Extraction Reading assignment: Techniques in Organic Chemistry 2nd ed pages 75-99. 3rd ed pages 113-140. Topics and Techniques i) identification of solvent layers of two immiscible solvents ii) partioning of a compound between two immiscible solvents and determination of KD iii) liquid-liquid extraction with aqueous acids and bases with organic solvents. iv) use of drying agents Introduction Liquid-liquid extraction is a method used for the
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from a Solid Mixture by Liquid-Liquid Extraction Introduction Liquid-liquid extraction is a technique used to separate chemical substances in order to purify or identify the various components of a mixture. Flavors‚ spices‚ perfumes‚ and medicines are just some of the everyday things that are extracted from plants and other natural sources [1]. The basic principle used to carry out this separation is the mixing of two liquids that are immiscible with each other. This creates layers of liquid‚ which
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experiment was to investigate the effects of salt type and concentrations on the rate of heating and the boiling point. Then from this data make a conclusion which salt type and concentration is the most energy efficient at heating water to its boiling point. It was hypothesised that highest concentration of MgCl2 was going to be the most energy efficient at heating the solution to its boiling point. This is because MgCl2 has the lowest specific heat capacity thus will use the least amount of energy
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