Oxidation of Borneol to Camphor Objectives: The purpose of this experiment was to use oxidation to convert (1S)-(-)-borneol into (1S)-(-)-camphor‚ which was done via the use of reagents such as glacial acetic acid and sodium hypochlorite and laboratory techniques learned in previous labs. Afterward‚ the final desired product was obtained‚ and to characterize and ensure the purity of the product‚ further lab techniques were implemented. Overall Reaction: 0 out of 10 Oxidation Reaction:. Mechanism:
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Title: The Green Oxidation of Borneol to Camphor Date Conducted: February 8‚ 2012 April 27‚ 2012 Abstract: The goal of this experiment was to perform a Green Oxidation of Borneol to Camphor‚ without the use of Chromium synthesis since it is toxic to the environment. Reagent Table: |Chemical Name |Amount used |Molecular weight |Concentration |Density g/mL |BP °C |MP °C |Chemical Formula
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reactions can be carried out in lab‚ or they can occur naturally via oxidants or reductants—substances that have the ability to oxidize or reduce other substances‚ respectively. Theory‚ Reactions‚ and Mechanisms In this lab‚ Borneol will be oxidized to camphor in a common reaction known as the Jones Oxidation Reaction. It is true that oxidation reactions subtract electrons‚ lowering its oxidation state. However in organic chemistry‚ a more detailed explanation of the oxidation reaction is
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Borneol; An Oxidation-Reduction Scheme Nicolas Gibson Lab Time: Tuesday 11:30 am Abstract: In this experiment‚ the main objective was to synthesize a ketone from borneol via an oxidation reaction and secondly‚ to produce a secondary alcohol from camphor via a reduction reaction. Therefore‚ the hypothesis of this lab is that camphor will be produced in the oxidation reaction and isoborneol will be the product of the reduction reaction because of steric hindrance. For the oxidation
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Introduction: Borneol (FIGURE-1)‚ first reported and published in the Tang Bencao in 659 A.D.‚ is often used in drug treatment‚ especially in Chinese drugs. It is helpful in opening obstruction of orifices‚ heat syndromes and pain releasing (Dharmananda). Nowadays artificially synthesized borneol‚ a mixture of borneol and isoborneol (FIGURE-2)‚ becomes more popular than pure natural borneol because of the lower cost in drug production. However‚ isoborneol is more toxic than borneol and thus is not
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Title : reduction of camphor to isoborneol Hend Altajjar Date: 01\30\2015 disk no. 116 lab report experiment procedure I scaled up 0.120 g of camphor ‚ the I added 1.0 ml of methanol in a 10-ml Erlenmeyer flask. I stirred with a glass stirring rod until the camphor has dissolved. Then I
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by everyday pollution from houses‚ factories‚ cars‚ and etc. This is the concept of acid rain‚ which according to EPA.gov is a broad term referring to a mixture of wet and dry deposition from the atmosphere containing higher than normal amounts of nitric and sulfuric acids. Acid rain isn’t just rain‚ its forms like hail or snow‚ which is wet deposition‚ and smoke or dust‚ which is dry deposition. The effects of acid rain are quite terrifying bringing all types of problems to the Earth‚ for example
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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hypochlorite (NaOCl) in acetic acid mixture was used to oxidize emdo-borneol (an alcohol) to camphor (a ketone). The product would then be purified by sublimation and then be analyzed by Infrared spectroscopy and melting point test. Procedure and ObservationsPlease refer to the lab manual and the carbon copy attached. Data and CalculationsWeight of endo-borneol = 0.2013gNo of moles of endo-borneol = 0.2013g/154.25g mol-1 = 1. 305mmolSince one mole of endo-borneol should give one mole of camphorTheoretical
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Experiment 8: Synthesis of Adipic Acid Performed November 8th & 10th By Jennifer Seitz Organic Chemistry 344 Section 803 Fall 2011 Objective: The purpose of this experiment was to synthesize adipic acid from cyclohexanol via an oxidation reaction that was catalyzed by sulfuric acid. Purity of the product was assessed by measuring the melting point. Physical Properties/Structures: Name | Formula | Molecular Weight (g/mol) | Boiling Point (0C) | Melting Point(0C) | Density(g/mL)
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