THEORETICAL STUDY ON MICROWAVE ASSISTED BONDING OF POLYMER BASED MICROFLUIDIC DEVICES By KASI BALAMURUGAN MANI A thesis submitted in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE IN MECHANICAL ENGINEERING WASHINGTON STATE UNIVERSITY School of Mechanical and Materials Engineering May 2013 To the Faculty of Washington State University: The members of the Committee appointed to examine the thesis of KASI BALAMURUGAN MANI‚ find it satisfactory and recommend that it
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at different temperatures. It is also the process in which the solid to be crystallized is dissolved to either a hot solvent or a hot solvent mixture and is cooled in a solution.In this experiment‚ acetanilide‚ the crude product of acetylation of aniline and acetic anhydride‚ was used as the pure organic compound. Crude acetanilide underwent crystallization process using the preferred recrystallizing solvent‚ water. The crystallization process was when crude acetanilide was placed in hot water bath
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Recrystallization Abstract: Technical grade aniline was reacted with acetic anhydride to give acetanilide a dark brown color‚ due to the presence of impurities. Crystallization of the crude product from water was combined with decolorization with activated carbon‚ furnished pure acetanilide as white flakes‚ melting point 112-115°C‚ yield 70.3%. Experimental: 2 grams of technical grade aniline and 15ml water were placed in a 125ml Erlenmeyer flask. Then‚ 2.5ml of acetic anhydride was
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Synthesis of Acetanilide Reaction O NH2 + H3C C O O C CH3 O N C CH3 H + H3C O C OH Aniline Acetic anhydride Acetanilide Acetic acid Purpose: Acetanilide is a useful precursor to many pharmaceuticals such as acetaminophen and penicillin. Experimental Procedure. (Estimated time: 1.5 h.) Unless otherwise noted‚ all manipulations should be done in the chemical fume hood. Place 100 µL of aniline into a tared 10 X 75-mm test tube (standing in a small beaker or Erlenmeyer flask). Now add
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MATERIALS Sodium nitrite Conc‚ sulphuric acid aniline N‚N-dimethylaniline nitroaniline phenol naphthol pyridine pH paper beaker‚ test tubes graduated cylinder filter paper PROCEDURES A. Preparation of Diazonium Salt Since these are immediately reacted‚ they should be prepared in parallel fashion‚ i.e. one vessel per prospective reaction. Into each vessel‚ place 1 gram or NaNO2. At 0 C‚ add a solution of 50 mg aniline in 2 mL conc H2SO4. Agitate for 5 minutes and isolate the
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Introduction: For this lab‚ the main focused involved alkanes and hydrocarbons. Essentially‚ the free-radical chain of chlorination of 1-Chlorobutne. Free radical-chains occur because alkanes are chemically unreactive with most agents. However‚ the free-radical chain allows a pathway of certain functional groups like alkyl chloride or bromides. In addition‚ chlorine atoms can possibly be made from molecular chlorine under low to mild conditions with the usage of a catalytic amount of an initiator
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To get to aniline‚ tin metal acts as a reducing agent and is oxidized to SnCl4. The purification of crude aniline is done by distillation and extraction. Aniline can be converted to acetanilide by acetylation reaction using acetic anhydride with sodium acetate. This step protects the amine functional group from doing unwanted reactions
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by : Directorate of Education‚ Delhi SOME IMPORTANT REASONING BASED QUESTIONS OF ORGANIC CHEMISTRY 1. Chlorobenzene is less reactive than chloromethane. Ans. In chlorobenzene‚ each carbon atom of benzenering is sp2 hyridised and is electron withdrawing. Chlorine atom donates a lone pair of electron and acquire positive charge. The negative charge is delocalised on ortho and para position by resonance. C-Cl bond acquires partial double bond character and is 169 pm as compared to 17.0 pm in chloromethane
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Desquitado‚ John Carlos M. Drapesa‚ Arianne Valerie B. Escritor‚ Elisha Ellis R. Esteva Group 4 2B Medical Technology Organic Chemistry Laboratory ABSTRACT In this experiment‚ acetanilide was used as the pure organic compound. Acetylation of aniline and acetic anhydride yields the crude product or crude acetanilide. The crude acetanilide was purified by dissolving it in hot water and then the solution was cooled slowly by placing in an ice bath. The yielded crystals were pure acetanilide since
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1. List all Functional Groups 2. What is an alkane? List its properties. 3. Write the name and formula of simple alkanes 4. Consider this compound (CH3)2CHCH2C(CH3)3. Name this. a. redraw it clearing all brackets and parentheses. b. Find the longest chain. Check from all directions. If it is not horizontal‚ rewrite the compound that so that longest chain IS horizontal. c. Number the carbons of the longest chain backwards and forwards.
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