members were asked to prepare the water bath‚ ice bath and a fluted filter paper while others were tasked to weigh the filter papers in advance so that the experiment will flow smoothly. The formation of crude acetanilide was due to the acetylation of aniline and acetic anhydride. The recrystallizing solvent dissolved the acetic acetanilide and was heated in a water bath. Crystals started to form after cooling the solutions in an ice bath. Pure acetanilide was the product after the second crystrallization
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Recrystallization is a technique used to purify organic solids. This method involves dissolving of a solute in a solvent and inciting the solute to produce a precipitate from a solution. In this experiment‚ acetic anhydride was added to the mixture of 2mL aniline and 20mL of distilled water. The mixture was cooled in an ice bath and filtered through filter paper resulting to the crude acetanilide. The pure acetanilide was then produced by the filtered solution of crude acetanilide and recrystallizing solvent
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Activity 1 Preparation of Acetanilide Abstract Recrystallization is a common method of purifying organic substances through the difference in solubility at different temperature. In this experiment‚ acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The solution was cooled slowly in an ice bath as crystals form out. As the compound crystallizes from the solution‚ molecules of other compounds dissolved
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plus the poisonous chemicals necessarily handled in the production of dye stuffs. Prior to 1917 the making of aniline products in this country for use as dye stuffs amounted to next to nothing. Our company had‚ however‚ been making aniline products since 1907‚ and in no inconsiderable quantities‚ for use as explosives; so that while the dye industry is fairly new to us‚ the nature of aniline and a number of its allied products is fairly familiar. The first hazard we meet in the dye industry is from
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Recrystallization is the primary method for purifying solid organic compounds through the differences in solubility at different temperatures. In this experiment‚ a suitable solvent was first determined. Acetanilide was produced by acetylation of aniline with acetic anhydride. The crude acetanilide was dissolved in a solvent in a heating water bath. The hot solution was filtered and the filtrate‚ cooled slowly in an ice bath as crystals started forming out. As the compound crystallizes from the solution
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Answers to Questions: 1.) Arrangement of Reactivity: (fastest to slowest) - Phenol‚ Nitrophenol‚ Acetanilide‚ Benzene‚ Chlorobenzene‚ Aniline - A reaction has occurred if there’s a change in color. The nature of the substituent‚ whether electron-donating to the ring or electron-withdrawing from the ring‚ was responsible for the reactivity of the benzene. Aniline and acetanilide contain amine groups‚ which are electron-donating. Chlorobenzene contains chlorine‚ which is electron-withdrawing. Phenol
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addition of aniline as one of the steps. The first step involves the acylation of aniline with maleic anhydride to give maleanilic acid 1. I n the second step maleanilic acid undergoes the Michael addition of aniline and cyclization to yield I-phenyl-3-pl~enylaminopyrrolidine-2‚5dione 2 (Method A). Compound 2 can also he obtained in one step by using commercially available maleanilic acid (Merck) or‚ albeit in slightly lower overall yield‚ by refluxing maleic anhydride and aniline in 12molar
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Since mammals do not synthesize their own folic acid‚ PABA inhibitors such as sulfanilamide selectively kill bacteria without injuring the host (Figure 1). One of the most well-known preparation techniques of sulfanilamide is achieved by treating aniline with excess chlorosulfonic acid via replacement of hydrogen with a sulfonyl chloride group. This reagent forms sulfonic acid first before being converted into a sulfonyl chloride by the excess chlorosulfonic acid (Scheme 1). A key method of sulfanilamide
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SYNTHESIS OF 1-PHENYLAZO-2-NAPHTHOL ABSTRACT Amines are compounds composed of nitrogen atoms bearing alkyl or aromatic compounds. Amines undergo interesting reactions‚ one of which is with the reaction with nitrous acid producing an azo dye. In this study‚ the experiment focused on synthesizing an observing the physical properties of Sudan-1. Sudan-1 is of the most common dyes found in waxes‚ oils and in some food ingredients specifically curry and chilli powder. Furthermore‚ this study aimed to
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Organic Chemistry Experiment - Hydrocarbons Thursday‚ April 12‚ 2007 1:34 PM Purpose: To Identify an unknown Hydrocarbon Procedure: Procedure listed in handout "Organic Chemistry Experiment -- Hydrocarbons" Hazards: Open flame and hydrocarbons are flammable. Equations: 1. . 3. . 4. . 5. . Unknown #: 1B s-6 Hyd-3 (colorless liquid) Data/Observations: Test Bromine addition Alkane Mixture of hexane and dichloromethane was originally clear liquid. After adding 3 drops red color Br2/CH2Cl
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