Distilling a Mixture of Cyclohexane and Toluene Lab partner: Chemistry 211 2/08/12 Goal: The purpose of doing this experiment is to separate a sample of cyclohexane and toluene using simple miniscale distillation. The objectives will be to record boiling range and volumes (mL) of distillates that are acquired during the distillation process. It is expected that cyclohexane boils and distils before toluene. By gathering these measurements will allow us to determine refractive index
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3.3 Results and Discussion 3.3.1 Particle Size of Asphaltenes. DLS was utilized to obtain the hydrodynamic radius of asphaltenes in toluene‚ which could help understand the behaviors of asphaltenes in the bulk solutions and oil/water interfaces. Figure 1 shows the particle size distribution of asphaltenes under different concentrations at 23 ℃ and under 2000 mg/L at different temperatures. A summary of the average particle size under different concentration and temperature conditions is shown in
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We reached our goals through our experimentation. We tested the solubility of each of the starting and ending materials in water‚ HCl‚ NaOH‚ toluene‚ and acetone. We discovered that the starting materials would only dissolve in toluene. To make the soap‚ we obtained about 10 mL of vegetable oil and 10 g of lard and we placed them both in separate 250 mL beakers. While we were stirring the compounds‚ we also added 15 mL of 6 M NaOH drop by drop and 1 mL of glycerol. We then heated our solutions
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BroIn this experiment of the relative rates of free-radical chain bromination‚ we were expected to be able to determine the relative reactivates of the many types of hydrogen atoms involved toward bromine atoms. Bromination is defined to be a regioselective reaction meaning bromine has preference of making or breaking a bond over all other directions that it may have had available. In this case‚ Markovnikov’s rule is revealed to be the case in this situation that states that adding a protic acid
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Loreta Grazhees TA: Titas Friday 11:50 - 3:55 February 9‚ 2018 Nitration Of Toluene When reacting Toluene with (NO2+) the end goal is to generate an ortho-‚ para-‚ and/or meta-nitrotoluene. This lab will help guide you in the direction to predict the regioselectivity and activation vs. deactivating powers of the nitro-group. Gas Chromatography will be used to analyze compounds that can be vaporized without being decomposed. GC is also used to check the purity of a substance‚ and separating the
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Abstract The bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure and its mechanism. After the addition of bromine to trans-cinnamic acid‚ the product was identified by its melting point and infrared spectrum resulting in erythro-2‚3-Dibromo-3-phenylpropanoic acid after comparing similar properties. Introduction In this lab‚ the bromination of trans-cinnamic acid was completed to determine dibromide’s stereochemical structure‚ and from there determine
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Lab 3: Bromination of Acetanilide CHEM 2110 Hassan Alsaleh 0525970 Due date :11/02/2015 Q1: To find the limiting reagent we need to find the number of moles of acetanilide‚ and the number of moles of Bromine. Mass of Acetanilide used = 0.67g Molar mass of Acetanilide = 135.16g/mol[1] Number of moles of Acetanilide = (0.67g) / (135.16g/mol) = 0‚005 mols Volume of Bromine = 0.25ml Density of Bromine = 3.103 g/ml[2] Mass of Bromine = (0.25ml) X (3.103g/ml) = 0.78g Molar mass of Bromine
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Organic Chemistry I LAB EXAM: FINAL BROMINATION OF BENZENE SYNTHESIS AND PURIFICATION OF BROMOBENZENE: PROCEDURE DATA TABLE Chemical Boiling point C Melting Point C Density g/mL Solubility Benzene 80.1 5.5 0.88 Slightly in H2O Toluene 110.6 -93 0.87 Slightly in H2O Bromobenzene 155-156 -30.8 1.50 Insoluble Dibromobenzene 220.40 87.31 0.96 Insoluble MATERIALS: Graduated cylinder Weight scale Buchner funnel Filter flask Rubber stopper Hot plate Thermometer Conical funnel Various
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Hydrocinnamic acid underwent bromination using N-bromosuccinimide and AIBN. As one lab partner set up the reflux apparatus‚ the other measured the chemicals used in the lab experiment. 2.10 g of hydrocinnamic acid was used. It was observed as white and had a slight cinnamon smell. The amount of NBS was 2.49g and was measured in the fume hood. AIBN was measured at .030 g. 10 mL of acetic acid was also obtained. The reflux apparatus consisted of a 25 mL flask with a stir bar in a water bath. The chemicals
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LAB REPORT! EXPERIMENT#5‚6! MANPREET KAUR KHAIRA! LAB PARTNER: VIAN RAIES! The purpose of this lab exercise was to perform the bromination of (E)-1‚2-diphenylethene (trans-stilbene) by addition reaction in which bromine was added across the double bond to yield a vicinal dibromide. The next step was to perform a double elimination reaction by product gained to synthesize an alkyne‚ that is‚ 1‚2-diphenylacetylene. The two major techniques used in this lab were TLC analysis and UV-vis spectroscopy
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