Abstract – This multi-step synthesis uses aniline as the starting reagent to synthesize five compounds employing several reactions such as acetylation‚ diazo coupling‚ nitration‚ bromination‚ and hydrolysis. The isolated products were analyzed with TLC and spectral data that determined most products were pure while some had a few impurities indicated by GC‚ LC‚ and a wide melting point range was shown for products 2 and 3. The presence of water in product 2 and 7 was indicated by the IR. Acetanilide
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CHEM 3152-003 Experiment 2: Fractional Distillation and Gas Chromatography Introduction: The purpose of this experiment was to separate a mixture of ethyl acetate (EtOAc) and toluene by using the method of fractional distillation and to analyze the fractions using gas chromatography (GC). ethyl acetate toluene Distillation is a method known as separating or purifying a liquid or mixture by vaporization and condensation. In a simple distillation‚ the liquids being separated boil below 150 0C
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DISTILLATION- SEPARATION OF A MIXTURE Ronald Ogbu‚ Alex 27th Aug. 2013 Purpose: To separate mixture of acetone and toluene using simple‚ packed and unpacked distillation columns. Results and Discussion: There were three distillation setups: simple‚ unpacked and pack fractional. All three procedures had different distillation apparatus but the unknown mixture was the same for all. The unknown liquid in a 50 ml round bottom flask was heated in a heating mantle such that a
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hydrocarbons using properties and reactions. b) Study substitution and addition reactions. Equipments test tube rack (1) test tube holder (2) 100 mL beaker medium test tube (6) Materials cyclohexene toluene n-hexane conc. H2SO4 Br2/CCl4 or Br2/CH2Cl2 0.50 % KMnO4 10% NaOH 10% Na2CO3 unknowns hydrocarbons Discussion Hydrocarbons‚ compounds which contain only carbon and hydrogen‚ can be classified into several types‚ depending
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is a combination of the mixture. The addition of a fractionating column allows numerous small distillations to occur within the column as the vapour rises towards the condenser. This experiment will demonstrate the separate a 50:50 mixture of toluene and cyclohexane by two methods and will require two separate equipment setups - one with the fractionating column (fractional distillation) and condenser and one with only the condenser (simple distillation). The results will show the contrast between
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halogenation reaction. If the bromine reacted with the alkene the bromine would discolor from orange and turn clear. Experiment Part A) Solubility of Alkanes: 1 mL of nine solvents (water‚ methanol‚ n-butanol‚ ethylene‚ glycol‚ acetone‚ hexane‚ toluene‚ ethyl acetate‚ and dichloromethane.) was added to nine sample vials. Each vial then had 0.5 mL of the alkane decalin added to each one. The mixtures were stirred to determine if the materials dissolved. If the material was insoluble it was heated
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I. Abstract The experiment: Classification tests on Organic Compounds‚ allows the students to be familiarized with different classification tests used for identifying the different classes of organic compounds; examine unknown compounds using appropriate tests; and identify functional group of an organic compound based on the tests performed. Several organic compounds with different functional groups were tested to identify the functional groups present in the compound. n-heptane‚ pentene
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Procedure: 3 drops of phenol soln in test tube + 1 drop FeCl3 soln Aliphatic and Aromatic Hydrocarbons/ Alkenes Bromination in Light (Free Radical Bromination) (Reacts with alkanes) Reagent: Br2 in H2O Observation: decolorization‚ brown ( colorless Procedure: 2 drops of test compound in test tube+ 1 drop 0.05 M Br2 in H2O‚ shake well‚ record observations Bromination in Dark (Electrophilic Addition Halogenation) (Reacts with alkenes) Reagent: Br2 in H2O Observation: decolorization
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other to react twice with a Grignard followed by removal of the protecting group by acid hydrolysis to give final product (C2). Method: Ethyl acetoacetate (30.03g)‚ ethylene glycol (15.01g) and toluene-p-sulphonic acid (0.13g) were added to a 250 cm3 round bottomed flask‚ containing a stirrer bar and toluene (100 cm3)‚ fitted with a condenser and dean-stark head. Solution was heated strongly under reflux using a heater stirrer block for approximately one hour. During heating 4.5 cm3 of water was collected
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Department of Occupational Therapy‚ College of Rehabilitation Sciences University of Santo Tomas‚ Espaňa Street‚ Manila 1008 Date Submitted: February 2‚ 2011 Abstract: Organic compounds hexane‚ heptane‚ cyclohexane‚ cyclohexene‚ benzene‚ and toluene were subjected to different physical and chemical tests todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test for the presence of aromatic ring)‚ Bromine test (test for
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