between benzonitrile oxide and an alkene‚ and to test the regiochemistry of the reaction between benzonitrile oxide and styrene. 2. Plan: Each student in a group of three will work to create a reaction with the Benzonitrile Oxide with‚ cis-stilbene‚ trans-stilbene‚ or styrene in an Erlenmyer flask. With this Reaction solution thin layer chromatography will be performed using each reaction solution. The different reactions will then be compared by running co-spot TLC’s. An NMR of the crude products
Premium Thin layer chromatography Nuclear magnetic resonance Chemistry
the other‚ and they were both swirled to observe reactivity. Part three of the experiment involved placing 1 mL of dichloromethane in each of five sample vials followed by adding 5 drops each of cyclohexene‚ toluene‚ beta-pinene‚ camphene‚ and trans-stilbene to the vials and swirling each until dissolved. Then bromine solution was added to each vial and
Premium Chemistry Ethanol Oxygen
1. In table format‚ provide the Rf values you recorded for each of the 3 compounds in Part I. List compound on one axis of your table and solvent system on the other. If multiple spots were present for a compound‚ give Rf value for each component and state if the component was major or minor. | 100% hexane | 25% EtOAc in hexane | 10% EtOAc in hexane | Fluorene | 0.34 cm | 0.94 cm | 0.67 cm | 9 - fluorenol | 0.00 cm | 0.49 cm | 0.05 cm | 9 - fluorenone | 0.00 cm | 0.69 cm | 0.21 cm |
Premium Chromatography Gas chromatography Solvent
Bromination of Trans-Cinnamic Acid Christopher B. Martin CHEM 3411 1 Mechanism of Bromine Addition to Alkenes Understanding the chemical mechanism (order of bonds broken and made as well as intermediates formed) has a great value in chemical synthesis. The chemical mechanism of a reaction will influence the rate of the reaction‚ the stereochemistry of the product(s)‚ and the extent of possible undesired side reactions. Organic reaction mechanisms investigate the path towards a desired product
Premium Chemistry Chemical reaction Organic reaction
cyclohexanol was first converted to cyclohexene and water by simple distillation (product: 6.5395g‚ 79.75% recovery). The cyclohexene then underwent a bromination reaction by addition of concentrated HBr and a 30% H2O2 solution‚ followed by an extraction of the aqueous phase. This produced trans-1‚2-dibromocyclohexane (product: 12.8886g‚ 67.34% recovery). The trans-1‚2-dibromocyclohexane was reduced by zinc metal to cyclohexene. The reaction was conducted in water‚ first allowing the reaction to reflux and
Premium Chemistry
APPLICATIONS OF ORGANIC COMPOUNDS IN LASER TECHNOLOGY WHAT IS AN ORGANIC COMPOUND? An organic compound is any member of a large class of gaseous‚ liquid‚ or solid chemical compounds whose molecules contain carbon. Organic chemistry is the science concerned with all aspects of organic compounds. Organic synthesis is the methodology of their preparation. APPLICATIONS OF ORGANIC COMPOUNDS clothing of cotton‚ wool‚ silk‚ and synthetic fibres; common fuels‚ such as wood‚ coal‚ petroleum‚ and natural
Premium Laser Organic chemistry Carbon
Name all cyclics. 7. What is cis? trans? 8. Name these. C(CH3)3 C(CH3)3 CH3 CH3 9. Go from the name to the structure a. 2‚ 3‚ 4 –tri methyldecane b. 4- t-butyl- 3- ethyl-3 -1 propylnonane c. 1‚ 1 di- ethylcyclopentane d. cis – 1‚ 2- dimethylcyclopentane e. trans – 1‚ 3 – diethylcyclopentane 10. Write
Premium Methane
The percent yield of meso-1‚2-dibromo-1‚2-diphenylethane was calculated to be 66.36% and with a melting point of 235.1°C. Therefore‚ it can be concluded that this experiment was successfully conducted as the percent yield obtained is only 33.64% off from the equilibrium point‚ and because the melting point met the literature value. The percent yield for the product was less than 100%‚ indicating that were experimental errors‚ such as an undesirable side reaction‚ or more likely‚ an incomplete reaction
Premium Chemical reaction Chemistry Melting point
Properties and Reactions of Hydrocarbons Abstract Introduction Hydrocarbons are organic materials that contain only carbon and hydrogen atoms‚ these molecules can be saturated or unsaturated and acyclic‚ cyclic‚ or aromatic. In this experiment we used a variety of methods to examine the physical and chemical properties of hydrocarbons. The first experiment we tested a variety of solvents to see if they dissolved our alkane (Decalin). One would expect that non-polar solvents will dissolve
Premium Solvent Solubility
Unsaturated Hydrocarbons Unsaturated hydrocarbons Have fewer hydrogen atoms attached to the carbon chain than alkanes. Are alkenes with double bonds. Are alkynes with triple bonds. 1 Structure of Alkenes Alkenes (and alkynes) are unsaturated hydrocarbons Alkenes have one or more double bonds The two bonds in a double bond are different: - one bond is a sigma () bond; these are cylindrical in shape and are very strong - the other is a pi (π) bond; these involve sideways overlap of
Free Benzene Hydrocarbon Alkene