EXP-10 CHEM 233L SYNTHESIS OF p-BROMOANILINE Introduction: In this experiment‚ p-bromoaniline was synthesized in three steps starting from aniline. Since the amino group of aniline is a strong activator of aromatic ring‚ direct bromination is impractical (equation 1). In order to make a desired product‚ amino group needed to be protected as the acetamide which also maintained ortho and para position but slowed down the rate of reaction (equation 2). Slow reaction rate would increase
Premium Acetic acid Solvent
2 mL of 48% aqueous hydrobromic acid‚ and 150 mg of tetrabutylammonium bromide is heated under reflux. The organic chemicals that are used are volatile and can evaporate and get lost; therefore we heat the reaction mixture
Premium Chemistry Alcohol Hydrogen
Experiment 15 & 16: Preparation of 1-bromobutane‚ an SN2 reaction Preparation of 2-chloro-2-methylbutane‚ an SN1 reaction Introduction The purpose of this experiment is to synthesize 1-bromobutane from 1-butanol and sodium bromide. In order for this reaction to reach completion there are four major operations that need to be performed. The four major operations include refluxing‚ simple distillation‚ separation‚ and drying. To begin‚ in order for the compounds to react they will be dissolved
Premium Chemical reaction Ethanol Metabolism
Ozone Layer Depletion [ Language & Communication Skills ] Contents Abstract | 1 | Introduction | 2 | Findings: Factor of ozone depletion | 3 | Effect of ozone depletion | 4 | Solution of ozone layer | 5-6 | Conclusion | 7 | Recommendation | 8 | References | 9-10 | Appendices | 11-13 | Bibliography | 14 | Abstract Ozone is concentrated in the ozone layer ‚ which is located in the stratosphere. It plays an important role to protect humans and
Premium Ozone depletion
Bromobenzene undergoes no reaction for both SN1 and SN2. This is because bromobenzene is very stable‚ and contains allylic and vinyllic bromine‚ which is also very stable‚ and cannot be a good nucleophile. Bromocyclopentane reacts under SN1 and SN2‚ but it shows a faster reaction in AgNO3/ethanol reagent‚ that is SN1. This is because bromocyclopentane is secondary bromine‚ and have bigger steric strain‚ since it is a cyclic compound. The bigger steric in a molecule‚ the harder it is for the nucleophile
Free
todifferentiate their intrinsic physical properties and chemical properties in terms ofstructure and behaviour. Nitration test (test for the presence of aromatic ring)‚ Bromine test (test for the presence of unsaturation)‚ and Basic oxidation test (test for an alkyl substituted benzine) were done. We were given an unknown which we tested (Nitration‚Bromine‚ Basic oxidation) and found out that it was an aromatic unsaturated hydro carbon. Keywords: hydrocarbons‚ hexane/ cyclohexane‚ cyclohexene‚ naphthalene
Free Benzene Hydrocarbon
Grignard Synthesis of Triphenylmethanol Aim The aim of this experiment was to prepared Grignard reagent (phenylmagnesium bromide) from bromobenzene and magnesium‚ to use the reagent prepared to synthesise a tertiary alcohol (triphenylmethanol) by reacting reagent and ester (methyl benzoate)‚ and the product formed is analyse by infrared spectroscopy (IR)‚ melting point‚ thin layer chromatography (TLC)‚ gas chromatography mass spectrum (GCMS) and finally Nuclear Magnetic Resonance spectroscopy. Introduction
Premium Nucleophile Magnesium Alcohol
Anionic Exchange Ion Chromatography to Detect the Anions Concentrations in the water Samples Narendra Boppana‚ Nasser Ali‚ Martin Chavez‚ Sear Introduction: Ion Exchange Chromatography is a process where the ionic exchange occurs in between the stationary phase and the sample in the mobile phase‚ by using this ionic exchange phenomenon it is easy to separate the compounds. Ionic exchange depends on the electrical properties
Premium Ion Chemistry Atom
For many‚ the answer to cleaning pallets is to fumigate the pallets with methyl bromide‚ a pesticide that has restricted use due to its toxic nature‚ or they may choose to heat-treat each pallet. Methyl bromide is not only an environmental toxin‚ but is also a known neurotoxin and carcinogen causing symptoms such as fatigue and acute memory loss. Heat treated pallets are of course free from methyl bromide and its’ less than desirable side effects but exposure to outside elements will more easily
Premium Management Economics Marketing
cyclohexene—flammable and irritant (cyclohexene) Sulfuric acid—toxic and oxidizer (Sulfuric acid) phosphoric acid—corrosive (phosphoric acid) Results/Data: End product weighed 0.109g of cyclohexane and tested positive with bromine test Discussion: In order to perform this experiment‚ a distillation apparatus was assembled. 4.0mL of H3PO4 and 3.0mL of cyclohexanol was placed in the round-bottom flask as sell as 5 drops of H2SO4 and a magnetic stir bar. The flow of water
Premium Sulfuric acid Laboratory glassware Distillation