Title : reduction of camphor to isoborneol Hend Altajjar Date: 01\30\2015 disk no. 116 lab report experiment procedure I scaled up 0.120 g of camphor ‚ the I added 1.0 ml of methanol in a 10-ml Erlenmeyer flask. I stirred with a glass stirring rod until the camphor has dissolved. Then I
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borneol and isoborneol (FIGURE-2)‚ becomes more popular than pure natural borneol because of the lower cost in drug production. However‚ isoborneol is more toxic than borneol and thus is not favored regarding the safety issue of drugs. But how can we synthesize borneol in a way that gives more borneol than toxic isoborneol? An experiment of making borneol from camphor (FIGURE-3) is performed in two different methods‚ Sodium Borohydride Reduction and Meerwein-Ponndorf-Verley Reduction‚ to compare
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Experiment VI: Oxidation of Isoborneol with Bleach Purpose: In this experiment‚ Green chemical procedures were applied to oxidize isoborneol to camphor using bleach (NaOCl)‚ rather than the tradition chromium-based oxidizing reagents. The camphor was then purified using the process of sublimation. Procedure: Using a 50-mL Erlenmeyer flask‚ 1.316 g (8.5 mmol) isoborneol and 1.0 mL (17 mmol) glacial acetic acid were stirred vigorously with a magnetic stir plate. A volume of 1.7 mL NaOCl
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objective for the experiment was to perform a reduction reaction on the ketone group of camphor to the OH group on isoborneol. In order to successfully synthesis the reactant to the product‚ NaBH4 was used as the main reagent to reduce the carbonyl double bond. One believes the formation of isoborneol was successfully due to the product’s percent yield‚ IR‚ and melting point. During the lab‚ .077 grams of isoborneol was yielded from the camphor reduction. In result‚ .077 g compared to an theoretical
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Oxidation of Borneol to Camphor Objectives: The purpose of this experiment was to use oxidation to convert (1S)-(-)-borneol into (1S)-(-)-camphor‚ which was done via the use of reagents such as glacial acetic acid and sodium hypochlorite and laboratory techniques learned in previous labs. Afterward‚ the final desired product was obtained‚ and to characterize and ensure the purity of the product‚ further lab techniques were implemented. Overall Reaction: 0 out of 10 Oxidation Reaction:. Mechanism:
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Borneol; An Oxidation-Reduction Scheme Nicolas Gibson Lab Time: Tuesday 11:30 am Abstract: In this experiment‚ the main objective was to synthesize a ketone from borneol via an oxidation reaction and secondly‚ to produce a secondary alcohol from camphor via a reduction reaction. Therefore‚ the hypothesis of this lab is that camphor will be produced in the oxidation reaction and isoborneol will be the product of the reduction reaction because of steric hindrance. For the oxidation
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Title: The Green Oxidation of Borneol to Camphor Date Conducted: February 8‚ 2012 April 27‚ 2012 Abstract: The goal of this experiment was to perform a Green Oxidation of Borneol to Camphor‚ without the use of Chromium synthesis since it is toxic to the environment. Reagent Table: |Chemical Name |Amount used |Molecular weight |Concentration |Density g/mL |BP °C |MP °C |Chemical Formula
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WHAT IS HARM REDUCTION? Harm reduction is a set of practical strategies intended to reduce the negative consequences of high risk behavior such as over drinking or drug abuse. Harm reduction is a non judgmental approach that attempts to meet people where they are at with their drinking or drug abuse. Instead of demanding perfect abstinence‚ this pragmatic approach is supportive of anyone who wishes to minimize the harm associated with a high risk behavior such as drinking or drug abuse. Harm
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the international poverty line include; – Guatemala‚ – Guinea-Bissau‚ – India‚ – Kenya‚ – Lesotho‚ – Madagascar‚ – Nepal‚ – Niger‚ – Senegal‚ – and Zambia • Analysts have found a strong positive relationship between economic growth and poverty reduction. • For example‚ East Asia (excluding China)‚which contains the world’s fastest-growing economies‚ reduced the share of its population living in poverty from 23 percent in 1987 to less than 14 percent in 1993. But in Sub-Saharan Africa‚ where negative
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Mohammed N. M. Sayan ESL 0405 ESL Advanced Writing Date: February 13th‚ 2013 Dr. J. Parla Palumbo Topic: Crime Reduction Title: What can I do to reduce crime? Thousands of crimes happen all over the world and increase exponentially every year. According to Nations Master’s website‚ more than twelve million crimes committed in the United states last year. "Crime statistics." nationmaster.com. Rapid Intelligence‚ 2002. Web. 25 February 2013. All of these crimes have happened due to high poverty
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