Chemistry of Spices This page intentionally left blank Chemistry of Spices Edited by Villupanoor A. Parthasarathy Indian Institute of Spices Research Calicut‚ Kerala‚ India Bhageerathy Chempakam Indian Institute of Spices Research Calicut‚ Kerala‚ India and T. John Zachariah Indian Institute of Spices Research Calicut‚ Kerala‚ India CABI is a trading name of CAB International CABI Head Office Nosworthy Way Wallingford Oxfordshire OX10 8DE UK Tel: +44 (0)1491 832111 Fax:
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Introduction Flash-Column Chromatography is another useful technique used to separate and purify complex mixtures of compounds. In this experiment‚ TLC is used to determine the best solvent system for the column. Due to Flash-Column Chromatography1 being an inexpensive technique‚ many scientist use this process for drug and natural product purification. Method By using the information from Experiment 6B‚ the TLC solvent system used was 30% EtOAc: 70% Hex. Experiment 7 was broken into two parts‚
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by Laboratory Reagents‚ Legacy Product Code: S/0380/48‚ CAS Number:8047-15-2) were powdered and analyzed as potassium bromide (KBr) pellets using FTIR (Model-JASCO FT/IR 4100 LE‚ made in Japan; Range: 4000-400 cm-1) Prabhu et al. (2013). Gas Chromatography–Mass Spectrometry (GC–MS) analysis: Acid hydrolysis of saponin was carried out according to the method described by Metwally et al. (2012) with some modification. Saponin was hydrolyzed with 2 N HCL (6 hr at 100 o C) under reflux‚ the residue
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Post-Lab Report for Experiment 2: Cooperative Identification of an organic Solid October 6‚ 2013 Introduction: This experiment was focused on the cooperative identification of organic compound by its chemical properties such as: slow melting point‚ mixed melting point‚ Rf values in TLC experiment‚ IR spectrum analysis‚ and H NMR spectra. Such data can provide the the identity of functional groups and the identity of the compound itself. In this experiment
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XV. GIMNAZIJA International Baccalaureate Department Group 4 – Chemistry SL Lab no.2: Acid-base titration Student: Caterina Rende Dominis Teacher: Zrinka Toplićan Date: 19 November 2012 Data Collection and Processing (DCP) Aspect 1: Recording raw data Table 1 Table showing raw data collected from titration Known measurements 25 mL of diluted acid 0‚100 M of NaOH solution Measurement Number | V of alkali needed to neutralize acid /mL/ (±0.01 mL)
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OH-‚ or H20 is added. By using standard lab equipment‚ a lab pro diagnostic tool‚ and acidic and basic solutions‚ the pH can be found. By recording the pH while adding a base or an acid gradually to a buffer solution you can find the capacity of each buffer to resist drastic changes in pH. The best buffers will keep a solution from becoming either too acidic or basic with the addition of a strong base or acid. Introduction The objective of the Irresistible lab is to determine the capacity of each
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Chromatography of Food Dye Chem 180-DL3 Abstract: The goal of this experiment was to use different dyes to determine the Rf value. Chromatography is done to determine the presence of a mixture in a substance. In this experiment different dyes were used such as McCormick food coloring‚ M&M’s‚ Kool-Aid‚ and the dyes that came with the lab kit. Experiment and Observation: In this experiment a 50mL beaker was filled with luke warm water and a pinch of salt water was dissolved in it
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Chromatography is a process used to separate mixtures. The word chromatography is derived from the Greek words ‘khroma’ and ‘graphein’ meaning ‘color’ and ‘to write’ or to represent. Although there are a couple different types of chromatography‚ in each case a substance is placed onto or into a medium and a solvent is passed through the test substance. In chromatography science‚ the solvent is called the mobile phase or the carrier fluid and the medium is called the stationary phase. There are four
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Basic Terms • forensic (adj) 1. pertaining to‚ connected with‚ or used in court of law or public discussion and debate 2. adapted or suited to argumentation; rhetorical Forensic Chemistry • Forensic science (n.) – the application of science to criminal and civil laws. – Emphasizes the application of science to criminal and civil laws that are enforced by police agencies in a criminal justice system. • Adversarial system – owes its origins to individuals such as Bertillon‚ Galton‚ Lattes
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5.05 Mixtures and solutions Lab report Ink Chromatography Chromatography is also used to compare and describe chemical substances. The chromatographic sequence of sorbed substances is related to their atomic and molecular structures. A change in a chemical substance produced by a chemical or biological reaction often alters the solubility and migration rate. With this knowledge‚ alterations or changes can be detected in the substance. Chromatography serves mainly as a tool for the examination and
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