Separation and Qualitative Determination of Cations and Anions Instructor’s Guide Master Materials List (complete for 24 students working in pairs) Silver nitrate‚ AgNO3‚ 0.2 M‚ 100 mL* Silver nitrate‚ AgNO3‚ 0.1 M‚ 100 mL* Cupric nitrate‚ Cu(No3)2‚ .02 M‚ 100 mL* Zinc nitrate‚ Zn(NO3)2‚ 0.2 M‚ 100 mL* Ferric nitrate‚ Zn(NO3)2‚ 0.2 M‚ 100 mL* Hydrochloric acid‚ HCl‚ 6 M‚ 125 mL* Nitric acid‚ HNO3‚ 6 M‚ 125 mL* Ammonia‚ NH3‚ 6 M‚ 125 mL* Sulfuric acid‚ H2SO4‚ 6 M‚ 125 mL* Acetic acid
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Abstract The preparation of 7.7-dichlorobicyclo [4.1.0]heptane which is also known as 7‚7-dichloronorcarane was done by reacting cyclohexene ‚ chloroform and a base( 50% aqueous sodium hydroxide) with benzyl triethylammonium chloride. The latter being a water soluble phase transfer catalyst (PTC).reaction was performed at room temperature and was distilled at atmospheric pressure. The mechanism of action of the above mentioned PTC is described in the text along with the mechanism for the addition
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Objectives 1. To separate a mixture of an acid and a neutral compound into its component by extraction. 2. To determine the melting point and the yield of the benzoic acid and the unknown sample. 3. To determine the unknown sample whether is is Trimethylmethanol or 1‚2‚4‚5-Tetrachlorobenzene. Introduction Extraction is a process of transferring a solute from one solvent to another. It is usually used to separate one or more components from a mixture. Diethyl ether‚ dichloromethane
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Analysis of Soda Ash and Volumetric Analysis of a Carbonate-Bicarbonate Mixture Buti‚ Mary Daphne A. Department of Chemical Engineering‚ Faculty of Engineering University of Santo Tomas España‚ Manila Abstract Sodium carbonate (Na2CO3)‚ commonly known by trade name soda ash‚ is a white‚ anhydrous‚ powdered or granular material that is an essential raw material used in the manufacturing of glass‚ detergents‚ chemicals‚ and other industrial products. In this experiment‚ the percent alkalinity
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An investigation to show how the rate of reaction between hydrochloric acid and sodium thiosulphate is affected by the concentration of the acid Simple Procedure Place a conical flask on a piece of paper with a cross on it. Add hydrochloric acid and sodium thiosulphate‚ and record the amount of time taken for the cross to disappear through the solution from the top of the flask. Record this time and repeat this for different concentrations of hydrochloric acid. Fair Test The variables in
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Antiseptics Definition An antiseptic is a substance which inhibits the growth and development of microorganisms. For practical purposes‚ antiseptics are routinely thought of as topical agents‚ for application to skin‚ mucous membranes‚ and inanimate objects‚ although a formal definition includes agents which are used internally‚ such as the urinary tract antiseptics. Purpose Antiseptics are a diverse class of drugs which are applied to skin surfaces or mucous membranes for their anti-infective
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Sulfa Drugs: Preparation of Sulfanilamide Introduction The purpose of this experiment is to prepare sulfanilamide from p-Acetamidobenzenesulfonyl chloride. This will be done using reflux‚ vacuum filtration‚ and melting point determination. Experiment Scheme6 Figure 1. Reaction equation.6 A hot water bath was prepared in a fume hood using a 250-mL beaker. 2.5 g of p-acetamidobenzenesulfonyl chloride was placed into a 50 mL Erlenmeyer flask and 11 mL of dilute ammonium hydroxide solution
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Aim: To examine a number of different chemical reactions and determine if they are exothermic or endothermic. Apparatus: • Test tubes {Around 10-12 in number} • Test-tube rack • Spatula • Digital thermometer { ± 0.1° C} • Digital balance {± 0.01 g} • Measuring cylinder {± 0.5cm³} • Different chemicals Introduction/Theory: Exothermic reactions are those reactions that release energy in the form of heat. Endothermic reactions need to absorb energy in the form
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Lux Toilet Soap Susan Sanders Devry University Lux Toilet Soap A 1954 ad for Lux Toilet Soap states‚ “Luscious is the word for Greer Garson’s complexion and she keeps it that way with Lux Toilet Soap.” This statement is an example of how emotional appeal is used in the ad to grab the reader’s attention. The advertiser uses character appeal by including information about Garson’s success in the ad to make the reader want to use the product. Logical appeal is used when a refund is offered to
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Title: Flame Test Aim: To determine the cation in each of the unknown substance X‚ Y and Z by observing the flame colour of different metal compounds. Introduction: A distinctive feature of many s-block metals is their ability to produce flame colours. At temperature of a Bunsen flame‚ a compound will decompose to give gaseous atoms of its constituent elements. When an electron in the gaseous atom absorbs energy from the flame‚ it will move from an orbital with lower energy to
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