the substances physical properties can be shown. A salicylic acid-naphthalene mixture was mixed together with diethyl ether and saturated sodium bicarbonate. Two layers separated and were extracted after acidifying with HCl. This precipitated the crude salicylic acid. The left over mixture was combined with water and the two layers separated where crude naphthalene was recovered. Sublimation was used to purify the naphthalene. Sublimation is the process when a solid evaporates from a warm surface
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4-nitroaniline had a percent recovery of 18.67% and naphthalene had a percent recovery of 80%. Naphthalene had a relatively high percent recovery‚ and the loss of product can be explained by error inherent. The low percent recovery of 4-nitroaniline is mainly due to the fact that anhydrous sodium sulfate was accidently added to the flask. Therefore‚ some product was lost as the aqueous solution with the protonated 4-nitroaniline reacted with the drying agent. However‚ more errors to explain the results
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Resolving and Determining the Percentages of Naphthalene‚ NaCl and SiO2 in a Mixture with the use of Separation Techniques Castro‚ Sarleen G.* Cid‚ John Emmanuel V.‚ Clemente‚ Christian Joy G. Group 5‚ 1CHEM‚ Department of Chemistry‚ College of Science‚ University of Santo Tomas‚ España‚ Manila‚ 1015 August 24‚ 2012 Abstract A mixture can be homogenous or heterogenous‚ depending if the mixture has been uniform throughout the mixture or not. One of the objectives is to separate C10H8‚ NaCl and
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points of the liquid. The purpose of this experiment was to identify‚ separate and characterize liquids from a mixture. This experiment took two days to complete. On the first day‚ we examined the properties of the solution and prepared a heating curve. A certain amount of the liquid mixture was poured into a small flask fitted with a two-hole stopper. In the first hole there was a thermometer and in the second hole there was a rubber tube which was attached to a piece of glass. The flask was placed
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Purpose: In this lab‚ a mixture of naphthalene (C10H8)‚ common table salt (NaCl)‚ and sea sand (SiO2) will be separated using the separation techniques in order to demonstrate the properties of mixtures and their ability to be separated by physical means. INTRODUCTION: This lab was based on the separation of the components of a mixture. A mixture can be defined as a physical combination of two or more pure substances. Separation techniques are used to separate components that are not chemically
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Lab Demonstration of Selected Calculations from Choice I Determination of Kf for Naphthalene To determine the Kf for naphthalene‚ we need to find the difference in the freezing point of pure naphthalene and the solution of 1‚4-dichlorobenzene in naphthalene. Let’s say that we did this experiment‚ used 1.00 g 1‚4-dichlorobenzene in 10.00 g naphthalene‚ and found that the freezing temperature of pure naphthalene was 78.2°C‚ while that of the solution was 75.4°C. This gives us a Tf of 78.2°C - 75
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Chemical Equation Chemical Reaction: C10H8+ 12 O2 → CO2 + 4H2 O (Naphthalene) Combustion Introduction of the Product: Naphthalene is an organic compound with formula C10H8. It is the simplest polycyclic aromatic hydrocarbon‚ and is a white crystalline solid with a characteristic odor that is detectable at concentrations as low as 0.08 ppm by mass. As an aromatic hydrocarbon‚ naphthalene’s structure consists of a fused pair of benzene rings. It is best known as the
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mixture of salicylic acid and naphthalene. The first part of extraction will be to separate the salicylic acid from the naphthalene using diethyl ether and aqueous sodium bicarbonate. The naphthalene will reside in the ether and be the top layer‚ while the salicylic acid resides in the sodium bicarbonate bottom layer. The two solutions will be separated and a solid crude substance will be collected from both. Then the method of sublimation will purify the naphthalene and the recrystallization will
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Name: JOANNA CELESTE M. QUINTANA Date performed: NOV. 12‚ 2012 Section: C-1L Date submitted: NOV. 21‚ 2012 Group Number: 3 Exercise No. 2 COLLIGATIVE PROPERTIES (Full Report) I. INTRODUCTION Colligative properties In liquid solutions‚ particles are close together and the solute molecules or ions disrupt intermolecular forces between the solvent molecules‚ causing changes in those properties of the solvent that depend in intermolecular attraction
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this experiment is to determine the heat of combustion for naphthalene. This is the some basic bomb procedures. In this experiment‚ we us naphthalene as a fuel in bomb calorimeter which naphthalene powder is turned to pellet using pellet press. The fuel is burnt at constant volume condition in a high pressure container (the bomb). The whole bomb‚ pressurized with excess of oxygen. The mass of iron wire‚ ma =0.02g. The mass of naphthalene pellet with iron wire‚ mb =0.38g. The bomb is submerged in
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