This experiment was a Landolt Iodine clock reaction - Oxidation of Bisulphite by Iodate. It involved conducting three measured experiments. The first variable tested was concencentration. This was tested by conducting two experiments‚ each varying the concentration of either the NaHSO3 or KIO3. The varying of NaHSO3 involved using 0.1 Molar of KIO3 against decreasing concentrations of NaHSO3 (0.25 M‚ 0.125 M‚ 0.0625 M and 0.03125 M). When decreasing the concentration of KIO3‚ 0.25 M of NaHSO3 was
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There are three reactions in the iodine clock reaction. The first reaction is IO3-(aq) + 3 HSO3-3 SO4-(aq) + I-(aq)+ 3 H+(aq)‚ where the iodate ions become iodide ions1. The second reaction is 6 H+(aq) +IO3-(aq) + 5 I-(aq) 3 I2(aq) + 3 H2O(l) where the iodate ions become molecular iodine2. The third reaction involves molecular iodine becoming a dark blue starch;I2(aq) + starch blue-black complex3. These three reactions react in a sequence. In any reaction the concentration is exponentially related
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Colorimetry Introduction Absorption Spectroscopic methods of analysis rank among the most widespread and powerful tools for quantitative analysis. The use of a spectrophotometer to determine the extent of absorption of various wavelengths of visible light by a given solution is commonly known as colorimetry. This method is used to determine concentrations of various chemicals which can give colours either directly or after addition of some other chemicals. As stated by the Beer-Lambert Law
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temperature on the rate of the iodine clock reaction using ammonium persulfate Assessment criteria: Design Variables: Table 1.1: List of dependent and independent variables. S.No | Dependent variables | Independent variables | Controlled variables | 1. | Rate of reaction | Temperature | Concentration | 2. | - | - | Pressure | 3. | - | - | Volume | Hypothesis: The iodine clock reaction is an experiment
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SPECTROPHOTOMETRY Spectrophotometry is the quantitative measurement of the reflection or transmission properties of a material as a function of wavelength It involves with the use of a spectrophotometer. A spectrophotometer is a photometer that can measure intensity as a function of the light source wavelength. A spectrophotometer is commonly used for the measurement of transmittance or reflectance of solutions‚ transparent or opaque solids‚ such as polished glass‚ or gases. Principles
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In order to prepare the iodine solution titrant‚ exactly 50 mL of 0.01 M KIO3‚ exactly 20 mL of 10% KI solution‚ and exactly 25 mL of 0.3 M H2SO4 was transferred into a 100 mL volumetric flask using a volumetric pipette. The volumetric flask was then filled to the mark with distilled water. The flask was covered with Parafilm and inverted to mix. The next part of the experiment was to determine the Vitamin C in a solution of known concentration. Observations of the Vitamin C sample and the amount
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Report of redox titration--- Iodine titrated against sodium thiosulphate Objectives The objective of this experiment is to balance the equation for the reaction between sodium thiosulphate and iodine. Principle As the reaction between sodium thiosulphate and iodine is a redox reaction‚ so I make use of this to perform a redox titration‚ iodine titrated against sodium thiosulphate. From the experimental result‚ I can find out the number of mole of the two substances‚ hence I can calculate
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Introduction: In this lab you will observe the diffusion of a substance across a semi permeable membrane. Iodine is a known indicator for starch. An indicator is a substance that chances color in the presence of the substance it indicates. Watch as your teacher demonstrates how iodine changes in the presence of starch. **Prelab Observations: Describe what happened when iodine came into contact with starch. The cornstarch turned blue-black Procedure: 1. Fill a plastic baggie with
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acid (acidified water) Solution of Sodium thiosulfate Granular zinc Iodine crystals Zinc ion and iodine-iodide-triiodide ion in water Solid zinc iodide Mineral oil Silver nitrate Magnesium turnings 3M Hydrochloric acid (HCl) solution 2 boiling tubes 1 large tube (we used a small) Pipet Beakers (to hold tubes) Bunsen burner PART 1 Procedure Get a boiling tube and label it R (reactants). Weigh out 2g of granular zinc and 2 g of iodine crystals and add to boiling tube “R”. Get a large test tube and
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a titration. Introduction Redox titrations using sodium thiosulphate as a reducing agent is known as iodometric titration since it is used specifically to titrate iodine. The reaction involved is: I2 + 2Na2S2O3 I2 + 2S2O322NaI + Na2S4O6 2I- + S4O62- In this equation I2 has been reduced to I- :2S2O32I2 + 2e S4O62- + 2e 2I- The iodine/thiosulphate titration is a general method for determining the concentration of an oxidising agent solution. A known volume of an oxidising agent is added into an excess
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