The Grignard Reaction Abstract Through the use of the Grignard reaction‚ a carbon-carbon bond was formed‚ thereby resulting in the formation of triphenylmethanol from phenyl magnesium bromide and benzophenone. A recrystallization was performed to purify the Grignard product by dissolving the product in methanol. From here‚ a melting point range of 147.0 °C to 150.8 °C was obtained. The purified product yielded an IR spectrum with major peaks of 3471.82 cm-1‚ 3060.90 cm-1‚ 1597.38 cm-1‚ and 1489
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If pH > pI‚ then the protein will have a negative charge and if pH < pI‚ the protein will have a positive charge. Buffer I has a pH >5‚ meaning both proteins carry a negative charge and bind to the DEAE (a positively charged resin). (b) pH = pKa + log10(Base/Acid) [Base = mM of sodium acetate; Acid = mM of acetic acid] = 4.7 + log10 (40/40) = 4.7 In order for the catalase to elute from the column‚ it must have lost its negative charge and stopped binding to the DEAE. Lowering the pH
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observe how the change in solvent polarity affects the rate and to determine the kinetics of a solvolysis reaction. In this experiment‚ we used 1-chloro-1-phenylethane in acetone in one reaction with 50% ethanol-50% water and in another reaction with 40% ethanol-60% water. To monitor he rate of reaction‚ we would need the concentration of the alkyl chloride at the beginning of the reaction and at a time t‚ but since we did not determine the concentrations‚ we monitored the rate of formation of
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Experiment three was divided into three parts; the preparation of the solutions‚ the reaction between Hydrochloric Acid and Ammonium Hydroxide (part b)‚ and the formation of Magnesium Oxide (part c). 200 mL of deionized water were added to a beaker followed by the addition of 100 mL 6 M HCl‚ which reacted to make 300 mL of a 2 M HCl solution used for Part B. Next‚ 50 mL of deionized water were added to a separate beaker and then 100 mL 3 M NaOH were added to the beaker to form 150 mL of a 2 M NaOH
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A. Introduction Title: The effect of reading Shakespeare on reaction time Research Question: Does reading a passage of Shakespeare decrease a person’s reaction time while completing a puzzle? One day in class‚ I was reading an interesting article about how people who read and are exposed to Shakespeare and Wordsworth and other renowned writers have better brain activity‚ attention spans‚ and can have more moments of beneficial self-reflection. In the article‚ scientists and psychologists at Liverpool
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All chemical reactions are processed through energy exchanges. Chemical reactions either absorb energy or release energy into their surroundings. In thermodynamics‚ endothermic reactions absorb energy where exothermic reactions release energy. In this experiment‚ we will be observing the chemical reactions that occur when a specific liquid is combined with a specific solid. We will measure the temperature of the liquid before the solid is added. Then we will measure the temperature of the liquid
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CHEM111AC‚ Experiment#9 - Ionic Reactions Discussion/Error Analysis In the first part of this experiment‚ the student was presented with 7 unique and unidentified bottles of solutions labeled A-G and was expected to be able to analyze the 7 solutions through trial and error and mixing them with one another. For solution A: mixing A + B formed a precipitate‚ A + C generated heat‚ A + D gave no reaction‚ A + E gave no reaction‚ A + F gave no reaction‚ A + G formed a precipitate. For solution B: mixing
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Report of redox titration--- Iodine titrated against sodium thiosulphate Objectives The objective of this experiment is to balance the equation for the reaction between sodium thiosulphate and iodine. Principle As the reaction between sodium thiosulphate and iodine is a redox reaction‚ so I make use of this to perform a redox titration‚ iodine titrated against sodium thiosulphate. From the experimental result‚ I can find out the number of mole of the two substances‚ hence I can calculate
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Introduction‚ aim and hypothesis Chemical reactions are accompanied by the release or absorption of energy. Reactions which release energy are described as exothermic and those which absorb energy are endothermic. The energy released in chemical reactions was previously stored as chemical potential energy in the reactants; this stored energy is called enthalpy. The aim of this practical is to observe and classify chemical processes as endothermic or exothermic‚ based on the changes in temperature
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The SN2 reaction requires three qualities: a strong nucleophile‚ a good‚ unhindered leaving group‚ and a polar‚ aprotic solvent. For our reaction‚ we have all three bases covered. The nucleophile is an alkoxide‚ a deprotonated alcohol. Technically‚ because our alcohol is a phenol‚ the conjugate base is called a phenoxide. Phenol itself has a pKa of about 10‚ but our alcohol has more resonance opportunities‚ so the pKa is down around 8. This is sufficiently acidic for use of weak base like K2CO3 for
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