The Grignard Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was
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ineffective. In order to help resolve the crisis‚ antibiotics were found through screenings of soil microorganisms. However‚ soil microorganism’s antibiotics were depleted by the 1960s and their antibiotic effects were unable to be replicated through synthesis. In this experiment‚ the researchers developed numerous methods to cultivate uncultured organisms in their environment. The goal of this experiment was to find antimicrobials in the uncultured soil. Through this successful experiment‚ the researchers
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1. Aim To determine the percentage of aspirin in different commercial preparations and to find which is the best value for money 2. Hypothesis The greater the percentage of acetylsalicylic acid (ASA) in the tablet‚ more powerful and efficient the aspirin would be due to the way aspirin works in human’s body. Aspirin is often used to alleviate the pain‚ and the sensation of pain is mainly attributed to a chemical substance called prostaglandins‚ which is responsible to send a strong signal
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Lab #28 Conservation of Mass Ashleigh Bublinec Serena Contreras
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mL of unknown #12. The flask was then covered and had a hole poked through the foil. Next‚ it was placed into boiling water. After the liquid was fully evaporated it was taken out‚ wiped dry and‚ allowed to cool. Then the mass was measured. Then the lab station was cleaned and the waste properly disposed of.
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Tie-Dye Grignard Synthesis Abstract: 4-Bromo-N‚N-dimethylaniline underwent a Grignard reaction with diethyl carbonate to produce a type of the tie-dye chemical triarylmethane. This specific triarylmethane produces a vivid crystal violet color when dyed. The experiment was first heated under reflux to produce the necessary Grignard reagent as a grey liquid. It was then reacted with diethyl carbonate and hydrochloric acid to produce crystal violet. The resulting chemical was very absorbent to
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The structure and synthesis of TPC is outlined in Scheme 1. Briefly‚ the compound 1 was synthesized as per literature procedure. 2 was synthesized by reacting 1-methy pyrazole-4-boronic pinacol ester with 1 by suzuki-coupling‚ the final product TPC was synthesized by treating with malononitrile in the presence of piperidine as a base and ethanol as solvent. The detailed synthesis procedure given in the experimental section. The structure and purity of TPC was unambiguously confirmed by 1H and 13C
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follows a semi microscale technique even a small amount of lost product yields a great loss in the yield 4. These sources of error could be minimized by doing a larger reflux in order to increase the yield. However‚ as the purpose was to simply synthesis SnI4 in order to identify the stable oxidation states (the melting point range requires very little product) it would be advantageous to use the current method. This is due to the smaller quantity of materials needed for this type of reflux‚ thus
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Analysis: In this lab we measured the rate of respiration of germinating mung beans and germinating peas at room temperature and 10 degrees Celsius. The rates of respiration at room temperature were higher than the rates of respiration in cold water. The reaction rate of the germinating peas at room temperature was .0125 ml/min and the reaction rate of the peas at 10 degrees Celsius was .0095 ml/min. The same is true for the germinating mung beans. At room temperature the rate of reaction was .0105
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blue green dihydrate. Copper (II) Chloride is highly soluble in water and will produce a blue solution. solutioAluminum is the compound that has a chemical formula of Al. This is a silver solid that can be easily formed‚ machined‚ or cast. In this lab‚ we will be finding the limiting reactant between Copper(II) Chloride and Aluminum. The limiting reactant is‚ reactant is‚ the reactant in a chemical reactant that limit’s the amount of the product that can be formed. We will also need to find the molarity
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