CHEMISTRY 101.1 Intermediate Chemistry Laboratory I Institute of Chemistry University of the Philippines‚ Diliman I. Synthesis of Salicylic Acid Purpose: Part I of the experiment illustrates the base hydrolysis of an ester‚ methyl salicylate‚ to form salicylic acid through nucleophilic acyl substitution. Procedure: Dissolve 12 g NaOH in 70 mL water in a 150 mL round bottom flask. Add 5.0 mL methyl salicylate and reflux the reaction mixture at its boiling point for 15 minutes using a stirrer
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Abstract Introduction The acylation of the α carbon position of a carbonyl group is one of the greatest breakthroughs that has benefited chemists in organic synthesis particularly when in need of building a carbon skeleton of interest in a molecule. For one to be able perform this acylation technique‚ there are two mar approaches which are employable. The first method involves the deprotonation of the α-Carbon atom which has a pKa known to be ̴20 through the use of a strong base for instance
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2.2 Application of Cu2O nanopowder 2.2.1 Photocatalyst 2.2.2 Solar energy conversion 2.3 Powder formation 2.4 Gas phase 2.4.1 Inert Gas Condensation (IGC) or Gas Phase Condensation 2.4.2 Chemical Vapor Deposition 2.4.3 Laser ablation 2.4.4 Flame synthesis 2.5 Liquid phase 2.5.1 Solvent evaporation method 6 6 7 7 8 9 9 11 11 11 12 12 13 Page ii iii vii viii xii xiii 1 2 3 4 5 pdfMachine iii Is a pdf writer that produces quality PDF files with ease! Produce quality PDF files in seconds and preserve
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Protein synthesis is one of the most fundamental biological processes. To start off‚ a protein is made in a ribosome. There are many cellular mechanisms involved with protein synthesis. Before the process of protein synthesis can be described‚ a person must know what proteins are made out of. There are four basic levels of protein organization. The first is primary structure‚ followed by secondary structure‚ then tertiary structure‚ and the last level is quaternary structure. Once someone understands
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Jewellyn G. Diola; ladyjewellyndiola@yahoo.com Abstract Synthesis of 3‚4-dihydro-3-(p-methylphenyl)-1‚2-(2h)-benzoxazine involves the nucleophillic addition of the 1 °amine group upon the carbonyly group of the salicylaldehyde‚ the reduction of imine to amine and the addition of paraformaldehyde to proceed ring closure. The experiment prepared the product through Mannich reaction‚ a multicomponent condensation synthesis between ketone‚ aldehydes‚ enols and amines. Biosynthesis of benzoaxazines
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Protein synthesis is the process whereby proteins are produced‚ or synthesized‚ in living things according to "directions" given by DNA (deoxyribonucleic acid) and carried out by RNA (ribonucleic acid) and other proteins. As suggested earlier‚ this is an extraordinarily complex process that we do not attempt to discuss here. Following synthesis‚ proteins fold up into an essentially compact three-dimensional shape‚ which is their tertiary structure. DNA contains the instructions for a cell’s structure
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SYNTHESIS AND CHARACTERIZATION OF POLYANILINE/POLY (P-HYDROXYANILINE)/Fe3O4 MAGNETIC NANOCOMPOSITE M. R. SABOKTAKIN‚ A. M. MAHARRAMOV‚ M. A. RAMAZANOV Baku State University‚ Baku‚ Azarbaijan E-mail: mamed_r50@mail.ru Several composites have been studied for static dissipationand microwave absorbing materials based on polyaniline with metallic oxides. These composites which are conducting polymers have been widely used because of their lower density as well their good environmental stability as in
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Experiment #1: Synthesis of Salicylic Acid From Wintergreen Oil By: Asad Razzaq TA: Date: 18/01/2015 222/Lab Section 8 Introduction Salicylic acid‚ used in production of substances used worldwide such as commonly used analgesic drug aspirin(cite)‚ can be obtained from natural resources such as wintergreen oil or can be synthesized. Through a series of chemical reactions with cheap raw materials beginning with beginning with methyl salicylate and‚ it is a cheaper and more
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Vidallon‚ Mark Louis P. Date Performed: February 20‚ 2012 CHEM44.1 2L Date Submitted: March 12‚ 2012 MIXED-ALDOL CONDENSATION Synthesis of Cinnamaldehyde I. Introduction Cinnamaldehyde‚ cinnamic aldehyde or 3-phenyl-2-propenal is the major constituent of cinnamon oil‚ extracted from several species of Cinnamomum (C. verum‚ C. burmanii‚ C. cassia)‚ under the family Lauraceae‚ a group of evergreen trees. Cinnamon bark (particularly C. verum) yields 0.4-0.8% oil‚ which contains 60-80% cinnamaldehyde
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The hypothesis for this lab is if strawberry DNA is separated from other components‚ then when it is placed in a insoluble solution the DNA can eventually be isolated. DNA is deoxyribonucleic acid. Its a self replacing material present in all living organisms as the main constituent of chromosomes. It is the fundamental and distinctive characteristics of someone or something‚ especially when regarded as unchangeable. DNA extraction is the removal of deoxyribonucleic acid from the cells or viruses
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