Discussion: Extraction and crystallization- The purpose of this lab was to extract and crystallize compounds in a mixture using acids and bases. 1 gram of the unknown was dissolved into 30 mL of ethyl acetate. The mixture was then transferred to a separatory funnel. Using aqueous solutions of different pH we were able to separate organic acids‚ bases and neutral compounds from each other. Using three 10 mL portions of HCl‚ we reacted the HCl with the base in solution. This made it possible to
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Have you ever seen dry ice‚ well let me show you. To measure the evaporation rate it is important to know that a half pound of dry ice will be placed outside and timed. The same thing will happen but in a cool room. If the dry ice is -109.3°F then it will evaporate in any condition warmer. The hypotheses is that the dry ice in the outside will evaporation faster. It is important to understand this because if you are trying to store dry ice and you put it in a freezer it will still evaporate. So in
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As discussed above‚ during DSC analysis two types of FFW and NFW were observed in PS‚ PT‚ and MA samples. The low-temperature XRD technique was used in this study to define the boundary between the FFW and NFW in PS‚ PT‚ and MA samples more accurately. Dowell and co-workers [29] and Shallcross and Carpenter [30] have reported the low-temperature XRD studies on ice structures. The low-temperature XRD analysis has been used by the authors to study the properties of water in low-rank coals [16‚ 26]
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4.11 The Design of the Cold Slug Wells The cold material well is located on the movable template opposite to the main flow path or at the end of the runner to trap the cooler advancing front of the melt while allowing hot material to flow into the cavities. The cold well should be slightly larger diameter than the main channel. To pull the sprue out of the sprue bush it has a snatch or pull pin or sucker pin underneath. Ejector pin system can be designed in three different methods: however the undercut
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Building a Fire to Fight Nature Jack London’s title for the story "To Build a Fire" starts the reader off with a very basic idea; building a fire. Almost anyone can build a fire. All it takes is a match and some kindling. London’s story is about more then building a fire‚ though. This story is about a man’s belief in himself‚ self-confidence and even arrogance‚ to such an extent that he doesn’t recognize the power of nature around him. London’s story is more like a "Man against Nature" story. London’s
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ago. My wide spread use over the course of human existence is the very reason that no one knows who discovered me. I belong to the group of elements called the transition metal group. I have several oxidation states and I also have a very high melting point which is around 1337.33 Kelvin. That is very high‚ in Fahrenheit it is 1947.92 degrees and in Celsius it is 1064.18 degrees. I am also paramagnetic‚ which means that I have very weak attractions to magnetic forces and can only be attracted when
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repCHEMISTRY I - LABORATORY EXERCISE MANUAL LABORATORY EXERCISE 10: Melting Point and Boiling Point Determination This is a traditional lab. You’ll simply follow the step-by-step procedure‚ keeping records of your measurements and observations. Each student will write their own lab report‚ which should include the following: Name: Names of lab partners: Date of Experiment: Date Report Submitted TITLE: Purpose: A brief statement about what the experiment is designed to determine
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Contents 1. Introduction and literature review 1.1 Polypropylene 1.1.1 Polypropylene crystallization 1.2 Polymer degradation 1.3 Broadband dielectric 1.4 Solubility and the cohesive energy density 1.5 Literature review 2. Experimental method 2.1 Solubility of SN 1010 in various solvents 2.2 Calibration curve 2.3 Preparation of polymer/antioxidant mix for films 2.4 Soxhlet extraction 2.5 Broadband dielectric analysis of films 2.6 Broadband dielectric analysis of molten samples
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PREPARATION OF ASPIRIN AND DETERMINATION OF THE MELTING POINT Ferrer‚ Lara Melissa V. Faculty of Engineering University of Santo Tomas Manila‚ Philippines ABSTRACT This experiment involved three steps: synthesis of aspirin‚ isolation and purification‚ and the estimation of purity of the final product. The synthesis involved the reaction of salicylic acid and acetic anhydride in the presence of a catalyst‚ phosphoric acid‚ H3PO4. When the aspirin was prepared‚ it was isolated and filtered. The percentage
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Solid: Crystallization and Melting Point Section: A61 Laboratory Exercise #1 Purification of a Solid: Crystallization and Melting Point Introduction In this lab exercise‚ we will be learning experimental techniques using glassware and other apparatuses. In order to successfully complete this lab‚ we will use techniques 1.0‚ 1.1‚1.2‚2.0‚2.1‚2.2‚ and 2.3 that are described in the Lab Manuel. In addition‚ we will learn how to determine the melting point of a solid
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