Friedel-Crafts alkylation was performed by adding t-butyl alcohol to p-dimethoxybenzene in order to produce 1‚4-di-t-butyl-2‚5-dimethoxybenzene. This reaction yielded 0.009g of 1‚4-di-t-butyl-2‚5-dimethoxybenzene having a percent yield of 5%‚ and a melting point range of 54.8°C-56.9°C. Introduction This reaction is designed to put functional groups onto aromatic rings. This is done through an electrophilic aromatic substitution where a positive species is strong enough to pull electrons out of the ring
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A qualitative analysis experiment was conducted to determine the identity of an unknown aldehyde or ketone. The tests include a Tollens test‚ a Schiff test‚ an iodoform test‚ and a derivative melting point test. The data of the first three tests was inconclusive. The final derivative melting point test was utilized to successfully determine that the unknown was the ketone‚ Propiophenone. Introduction: Qualitative analysis is a method or series of methods used to determine the identity
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Khoa Kirk Hoang OCHEM 262 Lab: Exp 35- Oxidation + Reduction Tablular Data Pre-Weighted Flask | Product + Flask | Product | % Yield | 5.36g | 5.401g | 0.041g | 41% | (60-70% = Acceptable) Actual Melting Point | Experimental Melting Point | 212C | 199.8 | ------------------------------------------------- (10C-15C variations acceptable) Reasons %yield: A reason that our percent yield is lower then what is acceptable can be due to various reasons. First‚ the amount of product we
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Lab # 4 Crystallization Jonathan Odell Partners: Allyson Chiu Michelle Jung Regine Ong Day 1 Period 3 Experiment conducted: November 15‚ 2012 Submitted date: November 21‚ 2012 Introduction: In this lab‚ the students were separated into groups of four in which were given a test tube that was half full of hydrate sodium thiosulfate. The experiment’s purpose was to observe the reaction of the hydrate sodium thiosulfate in different situations‚ such as being shook over a period of time
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experiments 3.2 and 3.4 was to determine whether the melting/freezing or boiling point is a characteristic of the property of the substance. A characteristic property is a certain property (physical or chemical) that can determine or identify the substance. For example‚ density and magnetism are two characteristic properties that can distinguish objects from one another. In this case‚ we are figuring out whether the melting/freezing or boiling point of a substance will help us find out what the substance
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Casting Pattern » Mold » Pour » Cool » Remove » Inspect Types of Casting : Expendable Mold‚ Multiple Use Mold Sand Casting : Expendable Mold casting process uses sand as molding material Requirements • • • • • • Mold : single or multiple use Melting Process Pouring Technique Solidification Process Mold removal Clean‚ Finish‚ Inspection METAL CASTING PROCESSES Categories • Expendable mold processes - mold is sacrificed to remove part • Mold (Sand‚ Shell‚ Vacuum‚ Expanded Polystyrene‚ Investment
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first structure is a trans isomer and the second structure is a cis isomer. Trans isomers have a higher melting point than cis isomers. b) No we won’t be able to tell the difference between the two isomers. This is because they are enantiomers. Enantiomers have the same melting point. 8. Increased intermolecular hydrogen bonding does increase the melting point. It causes the boiling point to be elevated since the molecules are more attracted to each other and thus require more energy to break
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expected to compete with traditional petroleum-produced polymers. The production of Polyhydroxybutyrate is well known in the medical field as it is mainly used for surgical pins and internal suture due to its biocompatibility. It has a high melting point with about 175C‚ which makes the material compatible as containers with high temperature usage. These properties of being biodegradable meaning its products decompose naturally without surgery needed to remove‚ and biocompatible meaning the body
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Unit C2‚ C2.2.3 Covalent structures 1. This drill contains an electric motor. The diagram below shows the main parts of an electric motor. The carbon contacts are made of graphite. Springs push the contacts against the copper ring. The contacts conduct electricity to the copper ring. The copper ring rotates rapidly but does not stick or become worn because the graphite is soft and slippery. Graphite has properties which are ideal for making the contacts in an electric motor. Explain
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The literature value for the melting point range for Trans-9-(2-phenylethenyl)anthracene is 130-133 oC. The obtained range was lower than that at 120.3 to 123.8 oC. Because it is lower than the known value‚ this means the obtain product is not completely pure. Impurities in the compound can result in a decrease in the compounds melting point‚ which is observed here. The impurities could be 1-propanol due to an insufficient drying. If the experiment was performed again‚ the product would need to be
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