Results and Discussion – Expt. 3 (Crystallization) Name: Parts A and B: 1. Please comment on the relative purity of your recrystallized salicylic acid (Hint: You should use your empirical data to support your claim). -The Salicylic acid that I obtained had a melting point range around 157-158 degrees Celsius for Part A. For Part B the melting point range was 156-157.5 degree Celsius. Part B‚ I would say the sample is less pure because of the notion that impurities lower the melting point
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purpose of this lab is to synthesize Lidocaine from 2‚6-dimethylaniline‚ using diethyl amine‚ 2-chloroacetyl chloride‚ acetic acid‚ and toluene. The Lidocaine was made by adding 2‚6-dimethylaniline to 2-chloroacetyl chloride in acetic acid. Sodium acetate is added in order to make the compound soluble. The product is dried‚ then treated with diethyl amine and toluene. This is refluxed using a water-cooled reflux condenser. The vapor is condensed by the cold water as the compound is being heated. A separatory
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greater accuracy when estimating ∆Hvap. The table below lists values for ∆Hvap and boiling point (Tb) for water and four organic compounds. Liquid Formula ∆Hvap/KJ mol-1 Tb/K Trichloromethane CHCl3 +29.3 335 Hexane C6H14 +28.8 342 Cyclohexane C6H12 +30.1 354 Methylbenzene C7H8 +33.4 384 water H2O +40.6 373 2. Water has a high ∆Hvap value compared with the other substances in the above table. Use your knowledge of intermolecular forces to explain this observation. a) Ethanol
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the proper responses of wild type E. coli Lac Operon as a control group. Mutated strains of E. coli were placed in four test tubes‚ each containing a different substance (lactose‚ glucose‚ water and lactose and glucose). After a warm water bath‚ Sarkosyl detergent‚ toluene and ONPG were added to the tubes and incubated again. The data was qualified by observing the color change from clear to yellow to indicate the presence of lactase. The results showed that strain A produced no lactase under any circumstance an
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Effects to the water quality Oils consist of a complex mixture of hydrogen and carbon which is used for fuel‚ lubrication‚ plastics manufacturing‚ and many other purposes. These petroleum products get into water mainly by means of accidental spills from ships‚ tanker trucks‚ pipelines‚ and leaky underground storage tanks Petroleum products affect surface water‚ impairing water quality with hydrocarbons‚ salts‚ nutrients‚ a host of organic compounds‚ and various heavy metals. Immediately after
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Chapter 6 practice MULTIPLE CHOICE 1. The formula for acetic acid‚ CH3CO2H‚ is an example of a(n) a.|condensed formula.| b.|mathematical formula.| c.|structural formula.| d.|molecular formula.| ANS: A OBJ: Goal #3.1: Interpret‚ predict‚ and write formulas for ionic and molecular compounds 3. Which of the following statements are correct? 1.|Metals generally lose electrons to become cations.| 2.|Nonmetals generally gain electrons to become anions.| 3.|Group 2A metals
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color. The tube was shaken gently to bring about white solids at the bottom of the reaction tube. Diphenyl ether(2mL) was added and heated until the solid dissolved. The reaction tube was cooled again and had toluene(2mL) added then placed in ice. The product was vacuum filtered‚ washed with toluene‚ dried‚ and weighed. Tetraphenylnaphthalene. Tetraphenylcyclopentadienone(0.500g)‚ glyme(3mL)‚ and a boiling chip was added to a reaction tube. Isoamyl nitrite(0.35mL) was added via syringe to reaction tube
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water (50ml x 5) and 50% aqueous ethanol. The mixture was dried under vaccuum suction and the melting point was determined. Yield: 0.85g‚ 90.8% m.p-199.8-200.3ºC. A portion of the dimer (0.0305 g‚ 0.0514mmol) was quantitatively dissolved in 25ml of toluene. The solution was left for 60min until colorless. The UV-Vis spectra was recorded for the colorless sample. The solution was irradiated using a lamp resulting in a purple solution and the UV-Vis spectrum was retaken. UV (): 524.92nm ε colourless (45
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[19593 Organic Chemistry of the Tramition Elements. Part r. View Online 551 Downloaded by University of Washington on 01 February 2011 Published on 01 January 1959 on http://pubs.rsc.org | doi:10.1039/JR9590000551 113. The Organic Chemistry of the Transition Elements. Part I. Tricarbonylchromium Derivatives of Aromatic Compounds. By B. NICHOLLS M. C. WHITING. and Many aromatic compounds‚ ArH‚ displace carbon monoxide from chromium hexacarbonyl with the formation of complexes Cr(CO)
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Volatile Organic Compounds (VOCs) have become the greatest challenges to the preservation of the environment today. This group of chemicals is used in almost every sphere of life from industries‚ government institutions and domestically by both an ignorant and knowledgeable public. This paper aims to put to light examples of such compounds‚ look at the effect on the general populace and the environment and outline possible remedies to negative impacts. At the same time‚ it is important to look at
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