and Stephonya Williams EXPERIMENT TITLE: Oxidation: Cyclohexanone from Cyclohexanol by Hypochlorite Oxidation and Adipic Acid from Cyclohexanone DATE: 4/18/2014 INTRODUCTION: In experiment 4‚ alcohol is oxidized to a ketone with household bleach. The product is then isolated by steam distillation and is extracted into the distillate with ether. After the removal of ether‚ it leaves the product cyclohexanone. In experiment 6‚ cyclohexanone is oxidized by potassium permanganate. Manganese dioxide
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Currently operating commercial production processes for adipic acid depend on the production or purchase of KA oil (a mixture of cyclohexanone‚ the ketone or K component‚ and cyclohexanol‚ the alcohol or A component)‚ or of pure cyclohexanol‚ and its subsequent oxidation in solution to adipic acid using an excess of strong nitric acid. This report deals with KA oil/cyclohexanol production by various routes‚ followed by the common step of nitric acid oxidation. KA oil production from cyclohexane by
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Exercise DP.1: Estimating Pure Component Properties in Hysys Workshop Report Requirements: 1. Create a graph of the vapor pressure in psia of cyclohexanol‚ cyclohexanol and high boiler as a function of temperature from 50 to 450 F. Print and submit these graphs. 2. Compare the pure component critical properties ( Critical Temperature‚ Critical Pressure) given in the design problem statement against the values used by Hysys. ( To view properties of a component‚ View the Basis Environment
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Laboratory #6 Qualitative Tests for Carbonyls: Aldehydes vs. Ketones Introduction Various chemical tests identifying ketones and aldehydes are used in this experiment in order to identify an unknown carbonyl compound. The tests used are: 2‚4-dinitrophenylhydrazone test‚ Tollen’s Test‚ Benedict’s Test‚ Chromic Acid Test‚ aka Bordwell-Wellman Test‚ Schiff’s Test‚ and Iodoform Test. These classification tests provide results based on color change or formation of precipitation‚ which is then used
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first step involves the production of KA Oil (a mixture of cyclohexanone‚ the ketone and cyclohexanol‚ the alcohol component) and the second stage is its subsequent oxidation to adipic acid with an excess of strong nitric acid in the presence of copper and vanadium catalysts. Only 3-8 % conversion of cyclohexane is obtained in the first step. Recycling of the large amount of cyclohexane unreacted and separation of cyclohexanol and cyclohexanone from cyclohexane present major problems. In the second step
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following parts a) You should state what experiment was performed‚ and show any necessary reaction schemes. The reaction schemes should include molecular weights and any other important physical data for the reagents and products. Ex. Cyclohexanol was oxidized to cyclohexanone using sodium dichromate in the presence of sulfuric acid. * Note: you can download a free version of a structure editor from ACD labs‚ the PC version is called chemsketch‚ the Mac version is called marvinsketch. You should learn
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Lab #24- Preparation 4-Methylcyclohexene Introduction: The goals in this lab were to have a reaction occur with 4-methylcyclohexanol and an acid catalyst to form our product of 4-methylcyclohexene via an E1 reaction. This reaction is accomplished by removing the –OH group on 4-methylcyclohexanol via dehydration and to have a double bond form via a loss of a hydrogen on a β-Carbon. Many techniques and skills were developed in this lab. Among them were dehydration‚ isolation‚ drying
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Good Practice Guidance and Uncertainty Management in National Greenhouse Gas Inventories N2O EMISSIONS FROM ADIPIC ACID AND NITRIC ACID PRODUCTION A C K N O WL E D G E M E N T S This paper was written by Heike Mainhardt (ICF Incorporated) and reviewed by Dina Kruger (USEPA). ABSTRACT Nitrous oxide (N2O) is generated as a by-product during the production of adipic acid and nitric acid. The main use for adipic acid is as a component of nylon-6/6; thus production trends are closely correlated
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EXPERIMENT 4 LAB REPORT TITLE: PREPARATION OF CYCLOHEXENE FROM CYCLOHEXANOL Paula Kata Partners: Ilai Bula S11099863 Eremasi Matin Abstract This work looks at preparation of cyclohexene from cyclohexanol which involves as part of an elimination reaction. The required reagent of concentrated sulfuric acid as one of the catalyst and water which allow the mixing known as washing the cyclohexene with water
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Maureen Wilson Lab Title Preparation of cyclohexene from cyclohexanol Aim Preparation of an Alkene by dehydration of an alcohol in the presence of a catalyst. Calculate the percentage recovery of products. Test for purity and identification of products. Abstract Cyclohexene and cyclohexanol are both colourless aromatic compounds. The major difference between the two is the presence of the hydroxyl group present in cyclohexanol. This hydroxyl group can be removed by a process known as dehydration
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