CHOONG SHING YI CHOONG SHING YI Preparation and Recrystallization of Aspirin Preparation and Recrystallization of Aspirin Date of the experiment: 9 May 2013 Date of submission: 23 May 2012 Date of the experiment: 9 May 2013 Date of submission: 23 May 2012 Synopsis 1. General Objective: To familiarize with the preparation of some simple organic compound and purify the compound by recrystallization. Specific Objective: The experiment is carried
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Pollution in Coal Based DRI Summer Internship Project‚ 2012 Supervised by Susmita Dasgupta susmita.dasgupta@hotmail.com 1 DRI‚ or directly reduced iron is a method of producing solid iron from iron oxide 2 Iron from iron ore can be • In solid form In solid form‚ iron ore can be 1. DRI produced in coal based kilns 2. HBI produced in gas based kiln. 3. DRI does not need coking coal at all. • Or in molten form In molten form iron can be produced in the 1. Blast Furnace‚ needs coking coal. 2.
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M. Drapesa‚ Arianne Valerie B. Escritor‚ Elisha Ellis R. Esteva Group 4 2B Medical Technology Organic Chemistry Laboratory ABSTRACT In this experiment‚ acetanilide was used as the pure organic compound. Acetylation of aniline and acetic anhydride yields the crude product or crude acetanilide. The crude acetanilide was purified by dissolving it in hot water and then the solution was cooled slowly by placing in an ice bath. The yielded crystals were pure acetanilide since molecules of other
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the hydrate copper (II) sulfate and the anhydride we were able to determine the mass of water in the hydrate. This information was then used to determine the empirical formula of the hydrate‚ defined as a compound formed by the addition of water to another molecule. In the first trial‚ the mass of water in the hydrate was determined to be 0.41 g‚ while in the second trial the mass of water was 0.52 g. Moles of water associated with a single mole of anhydride were then calculated for both trials‚ giving
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The Influence of Hair Color on the Concentration Zinc and Copper in Boys’ Hair1 JOSÉ DOREA2 ANDSUELI ESSADO PEREIRA G. Nutrition Laboratory‚ Faculdade de Ciencias da Saude‚ Universidade de Brasilia‚ 70910 Brasilia DP‚ Brazil of ABSTRACT Head hair of 150 normal boys from Brazil ranging in age from 1 to 12 years was studied for the influence of color on concentrations of zinc and copper. Hair color was classified visually and also quantified by melanin concentra tion. Visual classification
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acetaminophen. p-aminophenol and acetic anhydride were used to create acetaminophen and acetic acid. The acetic acid mixed with acetaminophen created an impure sample‚ which was purified through the addition of a water/methanol solution. The percent recovery of acetaminophen from the impure sample to the pure sample was 76%. The melting point of the pure sample was 167C - 169C. Introduction: Formulation of acetaminophen involves treating an amine with an acid anhydride to give rise to an amide. In this
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Preparation of Acetylsalicylic Acid Abstract Acetylsalicylic acid was prepared using salicylic acid and acetic anhydride. As a result‚ a white‚ powdery substance was formed (0.1931g‚ percent yield 91.30%) and was defined by melting point (124.5 – 134.5°C) and observation of color change with ferric chloride. Introduction Acetylsalicylic acid (aspirin) is one of the most popular analgesic drugs on the market today. It also acts as an antipyretic and anti-inflammatory drug. Salicylic acid itself
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prepare the water bath‚ ice bath and a fluted filter paper while others were tasked to weigh the filter papers in advance so that the experiment will flow smoothly. The formation of crude acetanilide was due to the acetylation of aniline and acetic anhydride. The recrystallizing solvent dissolved the acetic acetanilide and was heated in a water bath. Crystals started to form after cooling the solutions in an ice bath. Pure acetanilide was the product after the second crystrallization which was obtained
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pomegranate juice was treated with Fomes fomentarius laccase at various enzyme concentrations (0.5–5 U/ mL)‚ temperatures (20–50C) and times (30–300 min). The effect of these enzymatic treatments on total phenol content and clarity of the juice were evaluated using a central composite design. The optimum treatment conditions were: enzyme concentration 5 U/mL; time 300 min; and temperature 20C. Their application led to a 40% reduction of total phenols but induced a threefold decrease of the juice clarity
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50-100 mg (immediate release tablets) every 4-6 hours as needed for pain. The maximum dose is 400 mg/day. To improve tolerance patients should be started at 25 mg/day‚ and doses may be increased by 25 mg every 3 days to reach 100 mg/day (25 mg 4 times daily). Thereafter‚ doses can be increased by 50 mg every 3 days to reach 200 mg day (50 mg 4 times daily). Tramadol may be taken with or without food. Recommended dose for extended release tablets is 100 mg daily which may be increased by 100 mg every
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