3/26/2012 Part A: Dehydration of 1-butanol & 2-Butanol/Part B: Dehydrobromination of 1-Bromobutane & 2-Bromobutane Abstract The objective of this experiment is to successfully perform a dehydration of 1-butanol and 2-butanol‚ also dehydrobromination of 1-bromobutane and 2-bromobutane to form the alkene products 1-butene‚ trans-2-butene‚ and cis-2-butene. The dehydration reactions react under and acid-catalysis which follows an E1 mechanism. It was found that dehydration of 1-butanol yielded
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Synthesis of 4‐methylcyclohexene via Dehydration of 4‐methylcyclohexanol Heston Allred TA: Christine Woolley Thursday 1:05-4 pm Laboratory Experiment #10 Abstract 4-methylcyclohexanol was synthesized to 4-methylcyclohexene using dehydration. 4-methylcyclohexanol was heated to reflux and the subsequent distillate (4-methylcyclohexe) was collected. It was then purified using sodium chloride to separate products and an anhydrous solid was then added and filtered
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22: 4-Methylcyclohexene Abstract: We treated 4-methylcyclohexanol with phosphoric acid‚ and after purification we produced the end product 4-methylcyclohexene. We determined we had a pure product based on the results of the tests with Br2 and KMnO4‚ as well as the IR absorbtion spectrum of the final product. Purpose: The purpose of this experiment is to obtain pure 4-methylcyclohexene by reacting 4-methylcyclohexanol and phosphoric acid. Through distillation‚ extraction
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the simple distillation method to produce 4-Methylcyclohexene and to gain experience using an IR spectroscopy to characterize the product of the reaction in favor of equilibrium. B. Results and Discussion: C. Experimental: 24 mL of 4-methylcyclohexanol‚ 5mL of phosphoric acid‚ and 1mL of concentrated sulfuric acid was added to a 250 mL round bottom flask and mixed thoroughly with a magnetic stirrer. A simple distillation set up was installed with a 250mL round bottom flask‚ jack‚ stirrer‚
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Introduction: The goals in this lab were to have a reaction occur with 4-methylcyclohexanol and an acid catalyst to form our product of 4-methylcyclohexene via an E1 reaction. This reaction is accomplished by removing the –OH group on 4-methylcyclohexanol via dehydration and to have a double bond form via a loss of a hydrogen on a β-Carbon. Many techniques and skills were developed in this lab. Among them were dehydration‚ isolation‚ drying‚ and distillation. We used all of these techniques to
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When 4-methylcyclohexanol was combined with the bromine solution‚ the mixture turned into a light yellow color versus 4-methylcyclohexene with the bromine solution being colorless; the initial color for 4-methylcyclohexanol was combined with the bromine solution was a light orange/brown color. The solution being colorless indicated a positive sign of a double bond
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distillation column‚ and 7 mL of the distillate was collected. The organic and aqueous layers were separated and the organic layer was dried with anhydrous sodium sulfate. The product was analyzed using GC. III. Conclusion: In this experiment‚ 2-methylcyclohexanol was mixed with phosphoric acid with heat‚ to produce 3 isomers in one solution. This solution was run through a GC to calculate the product distribution. One isomer was such a rarity that it did not register on the GC. 1-methylcyclohexene accounted
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CHM456 ORGANIC CHEMISTRY 1 LABORATORY Contact hours: 3 hours/week Laboratory textbook: Pavia‚ Lampman‚ Kriz and Engel‚ Introduction to Organic Laboratoy Techniques 3rd Edition (2011) ** Students MUST obtain a copy of the textbook Synopsis This is an organic chemistry practical course which reinforce the theory and concepts studied in Organic Chemistry 1 (CHM456). It covers the learning of simple laboratory techniques such as reflux‚ distillation‚ extraction‚ crystallization and melting point
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of alcohol after observing our data; hence our experiment was a success. There was no side reactions observed within our experimental calculations. It was very evident that borohydride did in fact reduce our initial mixture to an alcohol (2-methylcyclohexanol). In the beginning of the experiment we spilled some of the reacting solution containing borohydride but we were still able to receive a favorably good result when it came to looking at our final data analysis.
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Chapter 17—Alcohols and Phenols SHORT ANSWER Drawing Instructions: Draw structures corresponding to each of the given names. 1. Draw: cis-4-tert-butylcyclohexanol ANS: 2. Draw: 3-methyl-2-buten-1-ol ANS: 3. Draw: 2-phenyl-2-propanol ANS: 4. Draw: glycerol ANS: 5. Draw: 2‚ 4‚ 6-trinitrophenol ANS: IUPAC Naming Instructions: Provide proper IUPAC names. 6. Name: ANS: (E)-2-ethylbut-2-en-1-ol 7. Name: HOCH2CH2OH ANS:
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