Experiment # 3 Acetylsalicylic Acid Introduction: The purpose of this experiment is to create and isolate pure acetylsalicylic acid from the substances salicylic acid and acetic anhydride. Then one will find the melting point to determine purity. Procedure: Make a hot bath. Weigh some salicylic acid and place in conical vial. Add .480mL of acetic anhydride and a drop of concentrated phosphoric acid. Drop in a magnetic spin vane and attach air condenser to vial. Partially submerge it in
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solution of an acidic and organic compound and purify its respective acidic product through the techniques of an acid base extraction‚ recrystallization‚ and use of Melt Temp (melting point range). The reaction of an unknown acid (3-chlorobenzoic acid) with diethyl and sodium hydroxide was observed‚ and the solution naturally separated into an aqueous and organic solution. The mixture of acid and organic solution was created and then separated through the Hirsch funnel into separate beakers of an aqueous
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A carboxylic acid is an organic acid characterized by the presence of at least one carboxyl group. The general formula of a carboxylic acid is R-COOH‚ where R is some monovalent functional group. A carboxyl group (or carboxy) is a functional group consisting of a carbonyl (RR’C=O) and a hydroxyl (R-O-H)‚ which has the formula -C(=O)OH‚ usually written as -COOH or -CO2H. Carboxylic acids are Brønsted-Lowry acids because they are proton (H+) donors. They are the most common type of organic acid. Among
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8: Synthesis of Adipic Acid Performed November 8th & 10th By Jennifer Seitz Organic Chemistry 344 Section 803 Fall 2011 Objective: The purpose of this experiment was to synthesize adipic acid from cyclohexanol via an oxidation reaction that was catalyzed by sulfuric acid. Purity of the product was assessed by measuring the melting point. Physical Properties/Structures: Name | Formula | Molecular Weight (g/mol) | Boiling Point (0C) | Melting Point(0C) | Density(g/mL) | Hazards
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Polytechnic University of the Philippines College of Science Department of Food Technology MOISTURE DETERMINATION (Experiment no. 1) Bea Dessa T. Co Maybelle Tolete Ian Francia Glyceryl Pangan BSFT 3-1D FOTE ///????? Food Analysis Prof. Kennedy Bongon Introduction Moisture content is one of the most commonly measured properties of food materials. It is important to food scientists for a number of different reasons: Legal and Labeling Requirements. There are legal limits to
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Title:Extraction:Extraction with acid and alkaline Objective: 1. To recover benzoic acid and p-dichlorobenzene from its mixture using acid-alkaline extraction. 2. To determine the percentage recovery and melting point of benzoic acid and p-diclorobenzene. Apparatus:Separatory funnel(250mL)‚Buchner funnel‚beaker. Materials:Benzoic acid‚p-dichlorobenzene‚ether‚10% NaOH‚conc.HCl‚distilled water‚ anhydrous CaCl2. Introduction: Organic compounds in an aqueous mixture can be separated
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Suggested time allotment: 5 to 6 hours MODULE 2 ACIDS AND BASES In Module 1‚ you identified common properties of solutions using different methods. You learned how to report the amount of the components in a given volume of solution. You also found out that not all solutions are liquid. Some of them are solids and others are gases. Towards the end of the module‚ you investigated the factors that affect how fast a solid dissolves in water. Most of the solutions you studied in Module 1
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________________________ Internal Assessment Criteria Aspect 1 Aspect 2 Aspect 3 Total DCP CE Aim: The aim of this practical is to plot and investigate the pH titration curves for the titration of a strong acid with a strong base and of a weak acid with a strong base‚ and find Ka of the weak acid. Procedure: Part I 1. Pour 30 ml of the HCl solution of unknown concentration in a 100 ml beaker. 2. Add a stirring magnet. 3. Place the beaker on the magnetic heater and activate the rotating motor but not
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Ingredients of the Melting Pot When reflecting on a timeline of America‚ what is clear is that this nation has grown in many ways due to far-reaching ideas‚ movements‚ and historical events. Immigrants who decided to continue their lives in the United States remain as the key factor of keeping this country functioning at the prosperous rate that it is. Unfortunately‚ Immigration has always been a controversial matter in America. Nonetheless‚ the population of the United States’ composes of citizens
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necessary reaction schemes. The reaction schemes should include molecular weights and any other important physical data for the reagents and products. Ex. Cyclohexanol was oxidized to cyclohexanone using sodium dichromate in the presence of sulfuric acid. * Note: you can download a free version of a structure editor from ACD labs‚ the PC version is called chemsketch‚ the Mac version is called marvinsketch. You should learn how to draw structures using these programs. Lab reports should look professional
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