Organic Chemistry Lab EXPERIMENT #2 and #3 Extraction and Evaporation Recrystallization and Melting Point Measurement PURPOSE: 1. To the components of a simulated pharmaceutical preparation‚ Panacetin‚ and identifying the unknown component of the mixture through extraction and separation methods. 2. To learn how to purify by recrystallization‚ how to dry them and how to obtain a melting point. PRECAUTION: ACETANILIDE AND PHENACETIN ARE EYE AND SKIN IRRITANTS. Minimize contact with
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#1: THE PURITY AND PURIFICATION OF SOLIDS MELTING POINTS ABSTRACT Melting points of different mixtures of naphthalene and biphenyl were examined in this lab. Samples of these various mixtures were collected and tested by different individuals in the lab in order to find the eutectic point of biphenyl. Unknown substances were then tested using the mixture melting point method in order to determine their identities. INTRODUCTION The melting point of a solid is the temperature where the
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VI: Conclusion: The melting point of a compound is the temperature at which the solid is in equilibrium with its liquid. A solid compound changes to a liquid when the molecules acquire enough energy to overcome intermolecular forces holding them together in an crystalline lattice structure. The melting point range is defined as the span of temperature from the point at which the crystals first begin to liquefy to the point at which the entire sample is liquid. This data can be tabulated experimentally
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The experimental melting point range of the desired alkene product‚ trans-9-(2-phenylethenyl) anthracene‚ was found to be 132-134 ˚C‚ in comparison to the literature value melting point range of 130-132˚C‚1 it was slightly higher than expected. Overall‚ the experimental melting point range varied from the initial melting point temperature and maximum melting point temperature by 2˚C. As the experimental melting point had a small range of temperature variance and was above that of the literature value
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Determination of An Unknown Amino Acid From Titration Abstract Experiment 11 used a titration curve to determine the identity of an unknown amino acid. The initial pH of the solution was 1.96‚ and the pKa’s found experimentally were 2.0‚ 4.0‚ and 9.85. The accepted pKa values were found to be 2.10‚ 4.07‚ and 9.47. The molecular weight was calculated to be 176.3 while the accepted value was found to be 183.5. The identity of the unknown amino acid was established to be glutamic acid‚
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collection jar was weighed and recorded. In the first recrystallization‚ 1.0 gram of adipic acid without the use of decoloring charcoal was recrystallized. After securing the yielded sample in one of the weighed jars‚ the next recrystallization was performed. As previously done‚ 1.0 gram of adipic acid was recrystallized. However‚ .10 gram of the pelltized decoloring charcoal was added to the sample. The yielded adipic acid was also collected in one of the weighed jars Both samples were left without caps
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Experiment 5- Standardization of NaOH and determination of Molarity of an unknown Acid Objectives 1. Preparation and standardization of a 0.1M NaOH solution 2. To learn the technique of titration 3. Determination of the concentration of an unknown diprotic acid. Introduction Titration can be traced to the origins of volumetric analysis‚ which began in the late eighteenth century. Study of analytical chemistry began in France and the first burette was made by Francois Antoine Henri
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EXPERIMENT : DETERMINATION OF THE RELATIVE MOLECULAR MASS OF AMIDOSULPHURIC ACID DATA COLLECTION AND PROCESSING. QUANTITATIVE DATA Type equation here. Experiment | Burette reading / cm3 | Volume of solution used(±0.1 cm3) | | Initial reading(± 0.05 cm3) | Final reading(± 0.05 cm3) | | 1 | 0.00 | 24.70 | 24.7 | 2 | 18.20 | 48.00 | 29.8 | 3 | 6.00 | 33.00 | 27.0 | QUALITATIVE DATA 1. When amidosulphuric acid was diluted with
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DETERMINATION OF BOILING POINTS Introduction: The boiling point of a compound is the temperature at which it changes from a liquid to a gas. This is a physical property often used to identify substances or to check the purity of the compound. It is difficult‚ though‚ to find a boiling point. Usually‚ chemists can only obtain a boiling range of a 2 - 3oC accuracy. This is usually sufficient for most uses of the boiling point. Purpose: The purpose of this experiment is to determine the
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changes in temperature. The changes in temperature were to be used to find the amount of heat released or absorbed. EXPERIMENTAL Reference """""""""""your website with your information""""""" RESULTS Calculation Calculation for determination of q: q = ms∆T Hess’s Law-type calculation ΔH = ΔHproducts – ΔHreactants J = g x [ J / ( g x ° C ) ] x ° C Calculation for Heat Change q=60g(160g*4.4c) =(60g*4.18J)/4.4j =1104.56 Joules CLASS TABLE part I
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