Summary Purpose To purify the component (unknown) of Pancetin from last experiment and then compare its melt point to the two other possible substances. Theory Panacetin should be made up of about 50 percent of the unknown component that we previously separated out of Panacetin for testing. We suspect that this unknown compound is either acetanilide or phenacetin. From the solubility of acetaminophen and phenacetin‚ we could know both of them are relatively soluble in boiling water but insoluble
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is done by observing the melting point. This is important because if there is an impure substance the melting point would be depression and the melting range would be broader. By finding the melting point of a known substance one can then observe an unknown substance’s melting point to see if the points are the same and try to figure out the unknown. Experimental Section: The first known substance we used was Biphenyl. 68 degrees Celsius is the known melting point. We used the capillary method
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3.7.2.1.5 Urea test PRINCIPLE Urea is hydrolyzed in the presence of urease to produce ammonia and CO2. The ammonia produced combines with 2 – oxoglutarate and NADH in the presence of GLDH to yield glutamate and NAD. Urea + H2O + 2H+ 2NH4+ + CO2 NH4+ + 2-Oxoglutarate +NADH H2O +NAD+ + Glutamate The decrease in absorbance due to the decrease of NADH concentration in unit time is proportional to the urea concentration. Ammonia
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of Salicylic Acid and Potentiometric Determination of its Purity and Dissociation Constant ------------------------------------------------- Abstract The purpose of the study is to synthesize salicylic acid from the ester‚ methyl salicylate‚ and determine the acid’s dissociation constant and purity. The ester was converted to salicylic acid by base hydrolysis. The products were refluxed and recrystallized‚ to ensure maximum purity‚ and filtered‚ dried‚ and weighed. The melting point of the product
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Title : Expt.1 Determination of the enthalpy (heat) of reaction of a monobasic acid with sodium hydroxide Experiment no : 1 Experiment title : Determination of the enthalpy (heat) of reaction of a monobasic acid with sodium hydroxide Objectives: 1) To understand the enthalpy chemistry. 2) To determine the calorimeter constant. 3) To determine the enthalpy reaction of acid-base reactions. 4) To study the exothermic reaction. Apparatus and Materials : * Dewar flask
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Spectrophotometric determination of Ascorbic acid Concentration in an Unknown Solution Introduction: The naturally occurring organic compound with antioxidant properties is Ascorbic acid shortly referred as (AA). Normally the color of Ascorbic acid is white‚ but in some cases of impure samples it appears yellow in color. Ascorbic acid is solid in state. In water it dissolves well to give mildly acidic solutions. Ascorbic acid is one form ("vitamer") of vitamin C [1]. So‚ Ascorbic Acid (AA) in other
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Date Performed: September 9 ‚2011 SPECTROPHOTOMETRIC DETERMINATION OF THE ACID DISSOCIATION CONSTANT OF METHYL RED M.C. Caligagan ‚M.N.Q. Tolentino and M.Q. Clores Institute of Chemistry‚ College of Science University of the Philippines‚ Diliman‚ Quezon City‚ Philippines Received :September 21‚2011 ABSTRACT This experiment aims to determine the acid dissociation constant value of Methyl Red by means of spectrophotometry. Ten samples were spectrophotometrically analyzed under a UV-Vis
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Lab S: Acids and Bases: Titrations | Determining Equivalence Point and Molarity Susheel Palakurthi 11661148 Partners: Justin Mwakule‚ Andrew Farrell July 29‚ 2015 CHEM 123 L02 TA: Amelia Fitzsimmons Experiment conducted: July 22‚ 2015 Introduction Acids and bases is an important aspect in chemistry. A specific example of such is in the body‚ acids and bases have to be balanced in order to provide the optimal pH in the system for normal physiological processes. Anything digested by the body has
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Ngoc Pham Chem162B Lab #2: Trends in Periodic Table Date: 01/10/2011 Lab partner: Ian Bauer Result Section: Table I: The solubility of the alkaline earth metal ions | SO42- | CO32- | C2O42- | IO32- | Mg2+ | S | I | S | S | Ca2+ | I | S | S | I | Sr2+ | S | S | S | I | Ba2+ | I | I | I | S | Key: I- insoluble‚ S-soluble Table II: Color of water (Halide) and Halogen (Hexane) layers | Cl2 | Br2 | I2 | Hexane layer | Clear | orange | Pink | Water layer | Clear‚
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REPORTIntroductionWater is a liquid that freezes and also melts at 32*F (0*C). Melting and freezing points are temperatures when a solid substance turns to a liquid. Liquid is a substance that flows to fit its container.Water Water is a liquid that is odorless‚ colorless‚ and tasteless. Water freezes and melts at 32*F (0*C). As water freezes it expands by one-eleventh. The amount of pressure on the water when it is freezing changes the melting point. Water that reaches 40*F it is at its maximum density. The molecules
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