Raquel Johnson October 19‚ 2014 Solids: Recrystallization and Melting Points Organic Chemistry 2423 Lab Report: Recrystallization Abstract: The purpose of this lab was to purify an unknown compound by recrystallization. Taking an unknown compound and identifying it by purifying it from its impurities through the use of hot gravity filtration. Then to determine the unknown you were to take the melting point. An unknown compound was recrystallized from hot water to produce 0.99 grams (67% recovery)
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tell you what active ingerdediant you are dealing with‚ confirm it through recording IR spectrum and then compare to online. 9. Run a TLC plate of isolated against solution of known compount. Eluent used is ethyl acetate containing .5% acetic acid. Spot reference containing acetaminophen and
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light catalyzes the thiosulfate to decompose. Before standardizing the thiosulfate‚ a blank determination of KI was performed. Potassium iodide may sometimes contain iodate ions; therefore‚ this part was performed to detect any iodate ions. In the blank determination experiment‚ exactly 2.00 grams of KI was dissolved in 50 mL of distilled water and then acidify with 5 mL of 3M sulfuric acid. After the acid‚ 5 mL of starch was immediately added into the solution. The solution didn’t turn into a blue
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IB Chemistry Experiment 4 Composition of a Post-1983 Penny Lab Report Background: Through the use of percent composition one can easily find out how much of a certain element is in a compound or an item such as a post-1983 penny. The experiment will be using HCl a strong acid to dissolve all the zinc inside the outer copper shell. The reaction follows as such; Zn+2HCLZnCl2+H2‚ but there will be no reaction with copper. The portion that will be measured is the mass of copper left after all of
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practice balancing those reactions while determining the relative activity of the metals included in the lab. Materials: Apparatus Test-tube rack 4 test tubes (25 mm x 150 mm) 4 beakers (150 mL) Safety goggles Lab apron Plastic gloves Full face shield Reagents Zinc Magnesium Iron Copper 1M hydrochloric acid‚ HCl 1M sulphuric acid‚ H2SO4 1M acetic acid‚ HC2H3O2 1M phosphoric acid‚ H3PO4 Procedure: Please refer to Health Chemistry‚ Laboratory Experiments‚ page(s) 75-76.
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hydrogen groups from the carbons. Concentrated phosphoric acid was used as a catalyst to help move the reaction towards the products motioned above. To determine the successfulness of the experiment and the amount of product(s) recovered‚ IR spectroscopy‚ Gas Chromatography and percent yield calculations were used. Equations and Structures 6. References 1. "18. Dehydration of 2- Methylcyclohexanol." Organic Chemistry Lab 2040L. XU Chemistry‚ n.d. Web. 12 Feb. 2013. 2. "Material
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(ACETYLSALICYLIC ACID) Aim: The aim of this experiment was to react salicylic acid with ethanoic anhydride to produce Aspirin. CH3CO)2O + HOC6H4COOH → CH3CO2C6H4CO2H + CH3COOH i Mass: 5g Volume: 7.5 cm3 Mass: 6.52g RMM: 138g/mol RMM: 180g/mol Moles: 5/138 = 0.0362 RMM: 102g/mol Moles: 0.0362 OBSERVATIONS – First‚ Ethanoic acid was added to the salicylic acid which resulted in a cloudy solution. When adding a few drops of concentrated sulfuric acid‚ which acted as
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Theory: Esters are derived from carboxylic acids and alcohols with the presence of a catalyst. A carboxylic acid contains the -COOH group‚ and in an ester the hydrogen in this group is replaced by a hydrocarbon group of some kind. Sulfuric acid (H2SO4)is used as a catalyst for this reaction in order to accelerate the rate at which the product is formed. The general formula of an ester is RCOOR’ in which R is the alkyl group that comes from the carboxylic acid while R’ is the alkyl group that comes from
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Abstract: This report presents the reason why the ocean does not freeze in the winter. Since the ocean consists of salt water‚ an experiment was done to test the effect of freezing on salt water compared to pure water. The experiment was conducted three times in order to obtain accurate results and eliminate errors. In addition to the salt and pure water experiment‚ a variation of this experiment was created to test other options. In the variation experiment the effect of freezing on sugar water
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Example Lab Report Experiment 4 1. Judith Anthony‚” Strong Acid/Strong Base Titrations”‚ CHEM 1130‚ T.A-Joseph Kreft‚ Tuesday 8am‚Room 1871‚Donna Ellitnorpe. 2. Purpose of this experiment: The purpose of this experiment is to observe the neutralization reaction that occurs between strong acid and strong base solutions. The technique of titration is used to observe the acid content of the fluid in a car battery. 3. Procedure: Calculate the volume of 6.00 M NaoH that is needed
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